Zborník príspevkov z vedeckej konferencie - Department of ...

1 st fraction
1.5
1.0
0.5
(x10,000,000)
1:TIC (1.00)
2.5 Inten.(x10,000)
185.102
0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0
2 nd fraction
1.50
1.25
1.00
0.75
0.50
0.25
1.5
1.0
0.5
0.0
(x10,000,000)
1:TIC (1.00)
0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0
Inten.(x10,000)
3 th fraction
1.5
1.0
0.5
2.0
1.5
1.0
0.5
0.0
227.107 384.182
280.977
450.264
847.939
705.777
755.133 895.225
655.563
186.109
545.736
1004.459
1038.537
(x10,000,000)
1:TIC (1.00)
Inten.(x10,000)
2.5
2.0
1.5
1.0
0.5
0.0
1190.750
1301.812
250 500 750 1000 1250 m/z
185.115
235.001
384.182
487.862
279.168
509.278
613.759
781.853
850.840
957.000
Inten.(x100)
4.5
4.0
3.5
3.0
2.5
2.0
1.5
1.0
0.5
250 500 750 1000 1250 m/z
311.221
406.206
14302.595
487.235
558.720 895.508
656.145 822.520
690.052
250 500 750 1000 1250 m/z
0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0
Fig.7: TIC traces (a), MS spectra (b) and deconvoluted MS spectrum (c) from HPLC/MS analysis of the fractions obtained
during the preparative ITP isolation of saliva sample spiked with lysozyme standard. For details, see Experimental.
1114.782
0.0
14200 14225 14250 14275 14300 14325 14350 14375 mass
Zborník príspevkov
z 18. medzinárodnej vedeckej konferencie
"Analytické metódy a zdravie loveka", ISBN 978-80-969435-7-9
- 131 -
c)
1209.565
b)
b)
a)
a)
b)
a)
hotel Falkensteiner, Bratislava
11. - 14. 10. 2010