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___________________________________________________RESULTADOS E DISCUSSÃOAm/z 154m/z 143 (McLafferty)ONHHOOm/z 181Bm/z 156m/z 143 (McLafferty)ONHHOOm/z 102Cm/z 156m/z 143 (McLafferty)ONHOOm/z 102Figura 29. Espectros de massas da A. (S)-N-(2E)-dodecenoil-HSL, B. (S)-Ndodecanoil-HSLe C. N-tridecanoil-HSL.59
___________________________________________________RESULTADOS E DISCUSSÃOAm/z 156m/z 143 (McLafferty)ONHHOOm/z 208 (-H)m/z 101, 102 (+H)Bm/z 156m/z 143 (McLafferty)ONHHOOm/z 101, 102 (+H)Cm/z 143 (McLafferty)ONHHOOm/z 236m/z 206 (-H)m/z 169 (Mclafferty)m/z 101, 102 (+H)Figura 30. Espectros de massas da A. (S)-N-(7Z)-tetradecenoil-HSL; B. (S)-N-tetradecanoil-HSL; C. (S)-N-(2E,7Z)-tetradecadienil-HSL.Como mostrado acima, as acil-HSLs estavam presentes em uma fraçãocomplexa e de massa reduzida (8,0 mg) dificultando o isolamento e acaracterização estrutural de todas estas substâncias por ressonância magnéticanuclear e espectroscopia no infravermelho. Decidiu-se, portanto, realizar acaracterização destes metabólitos por CG-EM, utilizando derivados obtidos60
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VDEDICATÓRIADEDICO ESTE TRABALHO
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VIIIBraga, Dr. José Augusto R. Rod
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XPOMINI, A. M. ; CABEÇA, L. F. ; C
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XIIde cadeia longa. Realizou-se tam
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XIVacyl-HSLs. We have also studied
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XVINBNOEODPpmR fRMNROERLUSTDSAMTMST
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XVIII3.3.4.2. Síntese da (S)-N-(2E
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XX5.4.10. Co-injeções das acil-HS
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PARTE EXPERIMENTAL5. PARTE EXPERIME
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PARTE EXPERIMENTAL• Espectroscopi
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PARTE EXPERIMENTAL5.1.2. Meios de c
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PARTE EXPERIMENTAL5.1.4. Cepas bact
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PARTE EXPERIMENTAL(S)-N-heptanoil-h
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PARTE EXPERIMENTAL(R)-(+)-N-heptano
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PARTE EXPERIMENTAL5.3. Avaliação
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PARTE EXPERIMENTALhexano, diclorome
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PARTE EXPERIMENTAL4,47 (t, 1H, J 9,
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PARTE EXPERIMENTAL13' 11' 9' 7' 5'O
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PARTE EXPERIMENTALHinton contendo o
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PARTE EXPERIMENTALno caso dos meios
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PARTE EXPERIMENTAL(S)-N-tetradecano
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PARTE EXPERIMENTALAs acil-HSLs fora
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PARTE EXPERIMENTAL5% (2 x 6 mL), bi
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PARTE EXPERIMENTAL13'12'11'10'9'8'7
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PARTE EXPERIMENTALsinais sobreposto
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PARTE EXPERIMENTALóleo e ferveu-se
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PARTE EXPERIMENTALRMN de 13 C (75,4
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PARTE EXPERIMENTAL(S)-(2E)-N-dodece
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PARTE EXPERIMENTAL(S)-3-oxo-(7Z)-N-
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PARTE EXPERIMENTAL5.4.9.3. Obtenç
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PARTE EXPERIMENTALIV (KBr): 3318, 3
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PARTE EXPERIMENTALisotermicamente a
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PARTE EXPERIMENTALprocedimento, por
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REFERÊNCIAS BIBLIOGRÁFICAS6. REFE
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REFERÊNCIAS BIBLIOGRÁFICASClusia
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REFERÊNCIAS BIBLIOGRÁFICASENGEBRE
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REFERÊNCIAS BIBLIOGRÁFICASLAMBAIS
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REFERÊNCIAS BIBLIOGRÁFICASusing l
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REFERÊNCIAS BIBLIOGRÁFICASXylella
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