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__________________________________________________________________ANEXOSOONHHOOA53. Espectro de RMN de 13 C (75,45 MHz, CDCl 3 , TMS) da (R)-N-(3-oxo-tetradecanoil)-HSL sintética.OONHHOOA54. Espectro de RMN de 13 C DEPT 135 e 90º (75,45 MHz, CDCl 3 , TMS) da (R)-N-(3-oxo-tetradecanoil)-HSL sintética.221
__________________________________________________________________ANEXOS1a b c de23A55. Avaliação semi-quantitativa da atividade antimicrobiana de N-heptanoil-HSL contraS. aureus (1), B. subtillis (2) e B. cereus (3). Legenda: a. branco (água/DMSO 20%); b.controle positivo (cloranfenicol); c. racemato; d. enantiômero(S); e. enantiômero (R).222
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VDEDICATÓRIADEDICO ESTE TRABALHO
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VIIIBraga, Dr. José Augusto R. Rod
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XPOMINI, A. M. ; CABEÇA, L. F. ; C
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XIIde cadeia longa. Realizou-se tam
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XIVacyl-HSLs. We have also studied
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XVINBNOEODPpmR fRMNROERLUSTDSAMTMST
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XVIII3.3.4.2. Síntese da (S)-N-(2E
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XX5.4.10. Co-injeções das acil-HS
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PARTE EXPERIMENTAL5. PARTE EXPERIME
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PARTE EXPERIMENTAL• Espectroscopi
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PARTE EXPERIMENTAL5.1.2. Meios de c
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PARTE EXPERIMENTAL5.1.4. Cepas bact
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PARTE EXPERIMENTAL(S)-N-heptanoil-h
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PARTE EXPERIMENTAL(R)-(+)-N-heptano
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PARTE EXPERIMENTAL5.3. Avaliação
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PARTE EXPERIMENTALhexano, diclorome
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PARTE EXPERIMENTAL4,47 (t, 1H, J 9,
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PARTE EXPERIMENTAL13' 11' 9' 7' 5'O
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PARTE EXPERIMENTALHinton contendo o
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PARTE EXPERIMENTALno caso dos meios
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PARTE EXPERIMENTAL(S)-N-tetradecano
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PARTE EXPERIMENTALAs acil-HSLs fora
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PARTE EXPERIMENTAL5% (2 x 6 mL), bi
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PARTE EXPERIMENTAL13'12'11'10'9'8'7
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PARTE EXPERIMENTALsinais sobreposto
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PARTE EXPERIMENTALóleo e ferveu-se
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PARTE EXPERIMENTALRMN de 13 C (75,4
Page 175 and 176: PARTE EXPERIMENTAL(S)-(2E)-N-dodece
Page 177 and 178: PARTE EXPERIMENTAL(S)-3-oxo-(7Z)-N-
Page 179 and 180: PARTE EXPERIMENTAL5.4.9.3. Obtenç
Page 181 and 182: PARTE EXPERIMENTALIV (KBr): 3318, 3
Page 183 and 184: PARTE EXPERIMENTALisotermicamente a
Page 185 and 186: PARTE EXPERIMENTALprocedimento, por
Page 187 and 188: REFERÊNCIAS BIBLIOGRÁFICAS6. REFE
Page 189 and 190: REFERÊNCIAS BIBLIOGRÁFICASClusia
Page 191 and 192: REFERÊNCIAS BIBLIOGRÁFICASENGEBRE
Page 193 and 194: REFERÊNCIAS BIBLIOGRÁFICASLAMBAIS
Page 195 and 196: REFERÊNCIAS BIBLIOGRÁFICASusing l
Page 197 and 198: REFERÊNCIAS BIBLIOGRÁFICASXylella
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