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__________________________________________________________________ANEXOS242220Transmitância181614121083285O28552934ONHHOO1786171115411646101911735854000 3500 3000 2500 2000 1500 1000 500Número de onda (cm -1 )A21. Espectro no infravermelho (KBr) da (S)-N-(3-oxo-octanoil)-HSL sintética.OONHHOOA22. Espectro de RMN de 1 H (499,88 MHz, CDCl 3 , TMS) da (S)-N-(3-oxo-octanoil)-HSLsintética.205
__________________________________________________________________ANEXOSOONHHOOA23. Espectro de RMN de 13 C (125,69 MHz, CDCl 3 , TMS) da (S)-N-(3-oxo-octanoil)-HSLsintética.OONHHOOA24. Espectro de RMN de 13 C DEPT 135º e DEPT 90º (125,69 MHz, CDCl 3 , TMS) da (S)-N-(3-oxo-octanoil)-HSL sintética.206
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VDEDICATÓRIADEDICO ESTE TRABALHO
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VIIIBraga, Dr. José Augusto R. Rod
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XPOMINI, A. M. ; CABEÇA, L. F. ; C
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XIIde cadeia longa. Realizou-se tam
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XIVacyl-HSLs. We have also studied
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XVINBNOEODPpmR fRMNROERLUSTDSAMTMST
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XVIII3.3.4.2. Síntese da (S)-N-(2E
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XX5.4.10. Co-injeções das acil-HS
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PARTE EXPERIMENTAL5. PARTE EXPERIME
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PARTE EXPERIMENTAL• Espectroscopi
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PARTE EXPERIMENTAL5.1.2. Meios de c
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PARTE EXPERIMENTAL5.1.4. Cepas bact
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PARTE EXPERIMENTAL(S)-N-heptanoil-h
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PARTE EXPERIMENTAL(R)-(+)-N-heptano
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PARTE EXPERIMENTAL5.3. Avaliação
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PARTE EXPERIMENTALhexano, diclorome
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PARTE EXPERIMENTAL4,47 (t, 1H, J 9,
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PARTE EXPERIMENTAL13' 11' 9' 7' 5'O
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PARTE EXPERIMENTALHinton contendo o
Page 159 and 160: PARTE EXPERIMENTALno caso dos meios
Page 161 and 162: PARTE EXPERIMENTAL(S)-N-tetradecano
Page 163 and 164: PARTE EXPERIMENTALAs acil-HSLs fora
Page 165 and 166: PARTE EXPERIMENTAL5% (2 x 6 mL), bi
Page 167 and 168: PARTE EXPERIMENTAL13'12'11'10'9'8'7
Page 169 and 170: PARTE EXPERIMENTALsinais sobreposto
Page 171 and 172: PARTE EXPERIMENTALóleo e ferveu-se
Page 173 and 174: PARTE EXPERIMENTALRMN de 13 C (75,4
Page 175 and 176: PARTE EXPERIMENTAL(S)-(2E)-N-dodece
Page 177 and 178: PARTE EXPERIMENTAL(S)-3-oxo-(7Z)-N-
Page 179 and 180: PARTE EXPERIMENTAL5.4.9.3. Obtenç
Page 181 and 182: PARTE EXPERIMENTALIV (KBr): 3318, 3
Page 183 and 184: PARTE EXPERIMENTALisotermicamente a
Page 185 and 186: PARTE EXPERIMENTALprocedimento, por
Page 187 and 188: REFERÊNCIAS BIBLIOGRÁFICAS6. REFE
Page 189 and 190: REFERÊNCIAS BIBLIOGRÁFICASClusia
Page 191 and 192: REFERÊNCIAS BIBLIOGRÁFICASENGEBRE
Page 193 and 194: REFERÊNCIAS BIBLIOGRÁFICASLAMBAIS
Page 195 and 196: REFERÊNCIAS BIBLIOGRÁFICASusing l
Page 197 and 198: REFERÊNCIAS BIBLIOGRÁFICASXylella
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