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___________________________________________________RESULTADOS E DISCUSSÃOnatural foi identificada posteriormente através de técnicas espectroscópicas epor comparação com dados da literatura.ABONHOOCFigura 42. Cromatogramas de íons totais (CG-EM, IE, 70 eV): A. fraçãoacetato de etila do cultivo de M. mesophilicum; B. produto sintético (±)-Ndodecanoil-HSL;C. Co-injeção da fração acetato de etila com o produtosintético. Observe o incremento na abundância relativa da N-dodecanoil-HSLnatural.91
___________________________________________________RESULTADOS E DISCUSSÃOABONHOOCFigura 43. Cromatogramas de íons totais (CG-EM, IE, 70 eV): A. fração F22semi-purificada do cultivo de M. mesophilicum; B. produto sintético (±)-(2E)-N-dodecenoil-HSL; C. Co-injeção da fração F22 com o produto sintético.92
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VDEDICATÓRIADEDICO ESTE TRABALHO
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VIIIBraga, Dr. José Augusto R. Rod
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XPOMINI, A. M. ; CABEÇA, L. F. ; C
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XIIde cadeia longa. Realizou-se tam
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XIVacyl-HSLs. We have also studied
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XVINBNOEODPpmR fRMNROERLUSTDSAMTMST
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XVIII3.3.4.2. Síntese da (S)-N-(2E
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XX5.4.10. Co-injeções das acil-HS
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Page 137 and 138: PARTE EXPERIMENTAL5. PARTE EXPERIME
Page 139 and 140: PARTE EXPERIMENTAL• Espectroscopi
Page 141 and 142: PARTE EXPERIMENTAL5.1.2. Meios de c
Page 143 and 144: PARTE EXPERIMENTAL5.1.4. Cepas bact
Page 145 and 146: PARTE EXPERIMENTAL(S)-N-heptanoil-h
Page 147 and 148: PARTE EXPERIMENTAL(R)-(+)-N-heptano
Page 149 and 150: PARTE EXPERIMENTAL5.3. Avaliação
Page 151 and 152: PARTE EXPERIMENTALhexano, diclorome
Page 153 and 154: PARTE EXPERIMENTAL4,47 (t, 1H, J 9,
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PARTE EXPERIMENTAL13' 11' 9' 7' 5'O
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PARTE EXPERIMENTALHinton contendo o
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PARTE EXPERIMENTALno caso dos meios
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PARTE EXPERIMENTAL(S)-N-tetradecano
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PARTE EXPERIMENTALAs acil-HSLs fora
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PARTE EXPERIMENTAL5% (2 x 6 mL), bi
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PARTE EXPERIMENTAL13'12'11'10'9'8'7
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PARTE EXPERIMENTALsinais sobreposto
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PARTE EXPERIMENTALóleo e ferveu-se
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PARTE EXPERIMENTALRMN de 13 C (75,4
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PARTE EXPERIMENTAL(S)-(2E)-N-dodece
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PARTE EXPERIMENTAL(S)-3-oxo-(7Z)-N-
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PARTE EXPERIMENTAL5.4.9.3. Obtenç
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PARTE EXPERIMENTALIV (KBr): 3318, 3
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PARTE EXPERIMENTALisotermicamente a
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PARTE EXPERIMENTALprocedimento, por
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REFERÊNCIAS BIBLIOGRÁFICAS6. REFE
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REFERÊNCIAS BIBLIOGRÁFICASClusia
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REFERÊNCIAS BIBLIOGRÁFICASENGEBRE
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REFERÊNCIAS BIBLIOGRÁFICASLAMBAIS
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REFERÊNCIAS BIBLIOGRÁFICASusing l
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REFERÊNCIAS BIBLIOGRÁFICASXylella
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