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QUANTIFICATION ET MORPHOLOGIE DE PHASES DE CLINKER PAR ANALYSE D'IMAGE.<br />

representative for the clinker as the 2000 points manually co<strong>un</strong>ted by the expert, which cover a<br />

larger analysis domain.<br />

For the analysis, two different magnifications were tested. The analysis of clinker 1 and 2<br />

used an examination field of 95µm*125µm for each image. The 50 fields of clinker 3 were taken<br />

with a less important magnification. Each image represents a field of 240µm*315µm. This<br />

corresponds to at least 40 crystals. The examination field is about six times bigger than in the case<br />

of clinker 1 and 2. The bigger field represents the clinker more correctly and the examination<br />

points are placed in a higher distance of 13µm.<br />

In the case of the reduced magnification, the dimensions (measured in picture elements)<br />

of each crystal in the image are less important. Thus, automatic colour and texture classification<br />

works with a local window of a smaller size. This decreases the performance of the automatic<br />

classification observed in Table 1. The difference between column a) and b) is more important<br />

for clinker 3 than for clinker 1 and 2.<br />

For the future, the solution will be either to increase the number of images with the<br />

bigger magnification to obtain a statistically significant sample or to increase the performance of<br />

the classification method to obtain good results with a less important magnification.<br />

2.7 CONCLUSIONS<br />

The object of this paper was the automatic quantitative determination of the phases of<br />

Portland cement clinker using a computer imaging system. The applied methods are based on<br />

advanced texture and colour analysis. The automatic segmentation of the phases takes advantage<br />

on the characteristics of local windows. The decision is made using data fusion from se<strong>par</strong>ated<br />

colour and texture classifications. The presented software determines the percentage of the main<br />

clinker phases.<br />

The proposed method gives access to the results manually obtained by the expert on<br />

different clinker types. The automatic phase segmentation between alite and belite gives good<br />

results. The system is integrated in a user interface, which makes the clinker analysis easy to be<br />

used even by a less experienced operator. The complete system can use the acquired images<br />

twice. Besides the use for the phase distribution analysis, the images can be used for the crystal<br />

size measurement.<br />

The automatic system is installed in the Lafarge laboratory in Viviers (France) and is used<br />

as a routine tool for the microscopic analysis. It permits to considerably reduce the time needed<br />

for the analysis of the different clinker samples. The system can replace the classical hard and<br />

tiring work and gives new possibilities to the clinker microscopy.<br />

The manual modification of wrong classed points is possible by the open and interactive<br />

software design by a simple mouse click. The corrections can be used to optimise the classifier.<br />

This can be made by adaptation of the <strong>par</strong>ameters used for the texture analysis or by amelioration<br />

of the learning database.<br />

In an additional developing state of the system, the automatic crystal measurement and<br />

form determination will be integrated. This could bring new information about the clinker and<br />

increase the performance of the quality control. Also, the determination of the minor phase<br />

WORLD CEMENT RESEARCH AND DEVELOPMENT 1998 107

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