Evaluation of the tensile stress-strain properties in the thickness ...
Evaluation of the tensile stress-strain properties in the thickness ...
Evaluation of the tensile stress-strain properties in the thickness ...
Create successful ePaper yourself
Turn your PDF publications into a flip-book with our unique Google optimized e-Paper software.
ned as <strong>the</strong> <strong>in</strong>tercept at zero force <strong>in</strong> a plot relat<strong>in</strong>g <strong>the</strong><br />
separation force to <strong>the</strong> s<strong>in</strong>gle handsheet grammage.<br />
Thickness def<strong>in</strong>ition <strong>of</strong> <strong>the</strong> constituents<br />
The comb<strong>in</strong>ed effect <strong>of</strong> adhesive penetration and nonrecoverable<br />
compression did not allow <strong>the</strong> direct<br />
evaluation <strong>of</strong> <strong>the</strong> <strong>thickness</strong> <strong>of</strong> <strong>the</strong> mix, t mix, and <strong>of</strong> <strong>the</strong><br />
<strong>thickness</strong> <strong>of</strong> <strong>the</strong> paper, t paper. An <strong>in</strong>direct assessment <strong>of</strong><br />
<strong>the</strong>se quantities was <strong>the</strong>refore necessary. The only measurable<br />
quantity was <strong>the</strong> sandwich <strong>thickness</strong>, t sandwich. This<br />
measurement, required ad hoc prepared test pieces.<br />
Alum<strong>in</strong>um sheets were placed between <strong>the</strong> platens and<br />
<strong>the</strong> adhesive so that <strong>the</strong> sandwich could be easily removed<br />
from <strong>the</strong> platens. The <strong>thickness</strong> <strong>of</strong> <strong>the</strong> sandwich<br />
could be determ<strong>in</strong>ed after remov<strong>in</strong>g <strong>the</strong> alum<strong>in</strong>um sheets<br />
from <strong>the</strong> sandwich. The <strong>thickness</strong> <strong>of</strong> <strong>the</strong> paper (see Fig 1<br />
for its geometrical def<strong>in</strong>ition) was calculated for each<br />
tested grammage as <strong>the</strong> difference between <strong>the</strong> <strong>thickness</strong><br />
<strong>of</strong> <strong>the</strong> handsheet after press<strong>in</strong>g and <strong>thickness</strong> <strong>of</strong> paper<br />
penetrated by <strong>the</strong> adhesive, Eqs (2)-(4). In Eq (2) <strong>the</strong><br />
penetration grammage and <strong>the</strong> density <strong>of</strong> <strong>the</strong> pressed<br />
handsheets for each grammage are used.<br />
Eq (2) can also be written us<strong>in</strong>g Eq (1) as<br />
⎛ 2w<br />
t = t ⎜1−<br />
paper handsheet ⎜<br />
⎝ w<br />
penetration<br />
handsheet<br />
The <strong>thickness</strong> <strong>of</strong> <strong>the</strong> mix could <strong>the</strong>n by calculated as<br />
t<br />
mix<br />
t − t<br />
=<br />
2<br />
sandwich paper<br />
Description <strong>of</strong> <strong>the</strong> test<strong>in</strong>g apparatus<br />
A schematic draw<strong>in</strong>g <strong>of</strong> <strong>the</strong> test<strong>in</strong>g apparatus is shown <strong>in</strong><br />
Fig 2. The rod was first screwed onto <strong>the</strong> test piece.<br />
Successively, <strong>the</strong> test piece and <strong>the</strong> rod were screwed<br />
onto <strong>the</strong> load cell. These actions were performed without<br />
subject<strong>in</strong>g <strong>the</strong> sandwich to undesired load<strong>in</strong>g. The rod<br />
was f<strong>in</strong>ally secured to <strong>the</strong> connector by <strong>the</strong> upper p<strong>in</strong>.<br />
Three sensors, fastened to <strong>the</strong> upper platen and displaced<br />
at 120 degrees from each o<strong>the</strong>r, measured <strong>the</strong><br />
displacement between <strong>the</strong> lower and <strong>the</strong> upper platen.<br />
The load<strong>in</strong>g was performed by means <strong>of</strong> a MTS servohydraulic<br />
test<strong>in</strong>g mach<strong>in</strong>e. The load was applied under<br />
displacement control <strong>in</strong> order to enable <strong>the</strong> measurement<br />
<strong>of</strong> <strong>the</strong> post-peak behavior <strong>of</strong> <strong>the</strong> material. The load was<br />
transferred to <strong>the</strong> rod via a universal jo<strong>in</strong>t system,<br />
consist<strong>in</strong>g <strong>of</strong> a connector, an upper and lower p<strong>in</strong>s<br />
cross<strong>in</strong>g each o<strong>the</strong>r. The po<strong>in</strong>t contact between <strong>the</strong> p<strong>in</strong>s<br />
avoided <strong>the</strong> bend<strong>in</strong>g moment caused by possible<br />
misalignments between <strong>the</strong> centre <strong>of</strong> <strong>the</strong> test piece and<br />
<strong>the</strong> po<strong>in</strong>t where <strong>the</strong> force is applied.<br />
The value <strong>of</strong> <strong>the</strong> Z-directional <strong>tensile</strong> strength obta<strong>in</strong>ed<br />
with <strong>the</strong> test<strong>in</strong>g apparatus was compared to <strong>the</strong> value<br />
obta<strong>in</strong>ed by a commercial apparatus follow<strong>in</strong>g SCAN<br />
P80:98. The latter method used tape to fasten <strong>the</strong> test<br />
pieces to <strong>the</strong> metal platens.<br />
⎞<br />
⎟<br />
⎠<br />
[2]<br />
[3]<br />
[4]<br />
Fig 2. A schematic draw<strong>in</strong>g <strong>of</strong> <strong>the</strong> test<strong>in</strong>g apparatus.<br />
Elaboration <strong>of</strong> <strong>the</strong> <strong>stress</strong>-<strong>stra<strong>in</strong></strong> data<br />
The data collected dur<strong>in</strong>g <strong>the</strong> experiments were <strong>the</strong><br />
displacements between <strong>the</strong> two platens measured by <strong>the</strong><br />
sensors and <strong>the</strong> correspond<strong>in</strong>g applied force measured by<br />
<strong>the</strong> load cell. The displacement at <strong>the</strong> centre <strong>of</strong> <strong>the</strong> test<br />
piece was calculated from <strong>the</strong> sensors measured displacements,<br />
as expla<strong>in</strong>ed <strong>in</strong> Appendix I. The displacement at<br />
<strong>the</strong> centre <strong>of</strong> <strong>the</strong> circular test piece, called δ sandwich, was<br />
taken as representative for <strong>the</strong> deformation <strong>of</strong> <strong>the</strong> whole<br />
sandwich. The elastic modulus <strong>of</strong> <strong>the</strong> sandwich was evaluated<br />
by a l<strong>in</strong>ear regression <strong>of</strong> <strong>the</strong> <strong>stress</strong>-<strong>stra<strong>in</strong></strong> curves.<br />
The <strong>thickness</strong> <strong>of</strong> <strong>the</strong> sandwich t, <strong>the</strong> <strong>in</strong>stantaneous force<br />
F and <strong>the</strong> tested area A were used for <strong>the</strong> determ<strong>in</strong>ation<br />
<strong>of</strong> <strong>the</strong> elastic modulus accord<strong>in</strong>g to Eq (5).<br />
E<br />
sandwich<br />
= δ<br />
F<br />
sandwich<br />
A t<br />
sandwich<br />
The displacement <strong>of</strong> <strong>the</strong> mix, δ mix, was determ<strong>in</strong>ed by<br />
assum<strong>in</strong>g a l<strong>in</strong>ear elastic behavior <strong>of</strong> <strong>the</strong> mix us<strong>in</strong>g Eq 6<br />
where <strong>the</strong> elastic modulus <strong>of</strong> <strong>the</strong> mix was obta<strong>in</strong>ed from<br />
<strong>the</strong> slope <strong>of</strong> <strong>the</strong> <strong>stress</strong>-<strong>stra<strong>in</strong></strong> curve <strong>of</strong> handsheets which<br />
were completely penetrated by <strong>the</strong> adhesive.<br />
The displacement <strong>of</strong> <strong>the</strong> paper was calculated as <strong>the</strong><br />
difference between <strong>the</strong> displacement <strong>of</strong> <strong>the</strong> sandwich and<br />
<strong>the</strong> displacement <strong>of</strong> <strong>the</strong> mix:<br />
Consequently <strong>the</strong> <strong>stra<strong>in</strong></strong> <strong>in</strong> paper was calculated as<br />
The value <strong>of</strong> <strong>the</strong> elastic modulus <strong>in</strong> <strong>the</strong> <strong>thickness</strong> direction<br />
<strong>of</strong> paper was determ<strong>in</strong>ed by comb<strong>in</strong><strong>in</strong>g <strong>the</strong> elastic<br />
[5]<br />
F<br />
δmix mix<br />
E A t = [6]<br />
mix<br />
δ = δ −2 δ<br />
paper sandwich mix<br />
[7]<br />
ε<br />
paper<br />
⎛<br />
δ<br />
δ<br />
⎜<br />
paper ⎝<br />
= =<br />
t<br />
paper<br />
sandwich<br />
F<br />
E A t − 2<br />
t paper<br />
mix<br />
Nordic Pulp and Paper Research Journal Vol 22 no. 1/2007 51<br />
mix<br />
⎞<br />
⎟<br />
⎠<br />
[8]