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MBraun UNIlab Glovebox System

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ORNL<br />

<strong>MBraun</strong> <strong>UNIlab</strong><br />

<strong>Glovebox</strong> <strong>System</strong><br />

6<br />

Gloves<br />

Inner Antechamber<br />

Door<br />

5<br />

1<br />

Interactive<br />

Display<br />

4<br />

Pressure<br />

Gauge<br />

2<br />

Outer<br />

Antechamber<br />

Door<br />

3<br />

Antechambers


A<br />

B<br />

C<br />

D<br />

E<br />

F<br />

SETUP HAZARDS<br />

4<br />

Before proceeding, check the H20 and O2<br />

readings in the upperleft corner of the<br />

display and verify that the values are less<br />

than or equal to 0.1.<br />

If the values are not as<br />

indicated in A , please<br />

contact a LSM.<br />

To light the work area<br />

within the box, touch the<br />

“Boxlight” control on the<br />

panel.<br />

There are two antechambers on this<br />

model, a small forward chamber and<br />

a larger one toward the rear.<br />

To load materials into the box, first verify<br />

the pressure gauge on the chamber is<br />

reading 0, the inner door is closed, and<br />

the valve is in the closed position. 6<br />

Open the outer door by turning the knob<br />

in the center. Then slide the tray out and<br />

place materials on it. When the chaber is<br />

loaded, slide the tray back in and reseal<br />

the outer door.<br />

4<br />

1<br />

1<br />

2<br />

3<br />

G<br />

H<br />

I<br />

J<br />

K<br />

L<br />

Evacuate the small chamber by<br />

turning the valve to “evacuate”<br />

as indicated by the diagram<br />

below the pressure gauge.<br />

Once the pressure gauge has settled,<br />

allow 3 minutes for non-pourous and 12<br />

hours for pourous materials.<br />

Refill the chamber by turning the valve to<br />

“refill,” as indicated by the diagram. For<br />

non-porous materials, wait for the gauge<br />

to settle at the halfway point. For porous<br />

materials, wait for the gauge to settle at 0.<br />

For non-porous materials, repeat 2 more<br />

times with 3 minute evacuation cycles,<br />

refilling the chamber halfway then, finally<br />

to atmospheric pressure (0). For porous<br />

materials, repeat the procedure one more<br />

time, waiting another 12 hours for<br />

evacuation.<br />

Turn the valve to the “closed” position<br />

and open the inside antechamber door,<br />

slide the tray out, remove materials, then<br />

close the chamber.<br />

The procedure for the large<br />

antechamber is the same as for the<br />

small except the non-porous<br />

materials should have 5 minutes<br />

during evacuation instead of 3.<br />

4<br />

4<br />

6<br />

ELECTRICAL HAZARD<br />

This equipment is operated on a<br />

high voltage system and may<br />

remain charged after being<br />

powered off<br />

SUFFOCATION HAZARD<br />

There is a risk of asphyxiation when<br />

working with inert gasses.<br />

GENERAL HAZARDS<br />

Depending on the type of work being<br />

performed in the box, thermal,<br />

mechanical, electrical, and/or<br />

chemical hazards may be present.<br />

PREVENTION<br />

EYE PROTECTION<br />

Wear safety glasses while operating.<br />

PROTECTIVE GLOVES<br />

Wear appropriate gloves for heat and<br />

chemical usage.<br />

NON-SLIP, CLOSED SHOES<br />

Wear non-slip, closed shoes to avoid<br />

spills.<br />

READ MANUAL<br />

Become familiar with this guide<br />

before operating.<br />

For additional help contact the Lab<br />

Space Manager

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