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De-oiling of Raw Lecithin by High Pressure Extraction ... - ISSF 2012

De-oiling of Raw Lecithin by High Pressure Extraction ... - ISSF 2012

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CONCLUSIONS<br />

A green process for processing <strong>of</strong> the highly viscous raw lecithin was developed from laboratory scale up to<br />

industrial plant scale. The main advantages using supercritical CO2 instead conventional solvents (which<br />

contaminate lecithin with organic solvents which can not be easily removed) are presented.<br />

Examples on selective extraction and further fractionation <strong>of</strong> components <strong>of</strong> lecithin from raw lecithin are<br />

presented. Fundamentals, like phase equilibrium data for the system oil/SCF as well as mass transfer data will be<br />

given in the presentation. Mechanical design <strong>of</strong> industrial-scale equipment, influence <strong>of</strong> process parameters on<br />

lecithin particle size and particle size distribution, particle shape, modeling <strong>of</strong> extraction procedure <strong>of</strong> the process<br />

will be presented.<br />

REFERENCES<br />

[1] HORROCKS, L. A., in: SZUHAJ, B.F., (Ed.), <strong>Lecithin</strong>s: Sources, Manufacture and Uses, American Oil<br />

Chemists Society, Champaign, IL, 1989<br />

[2] SCHNEIDER, M., in: SZUHAJ, B. F., (Ed.), <strong>Lecithin</strong>s: Sources, Manufacture and Uses, American Oil<br />

Chemists Society, Champaign, IL, 1989<br />

[3] MONTANARI, L., FANTOZZI, P., SCHNEIDER, J.M., KING, J.W., J. Supercrit. Fluids, Vol. 14, 1999, p.<br />

87<br />

[4] LIST, G.R., KING, J.W., JOHNSON, J.L., MOUNTS, T.L., J. Am. Oil Chem. Soc., Vol. 70, 1993, p. 473<br />

[5] TEMELLI, F., J. Food Sci., Vol. 57, 1992, p. 440<br />

[6] PETER, S., in: KING, J.W., LIST, G.R., (Eds.) Supercritical Fluid Technology in Oil and Lipid Chemistry,<br />

AOCS Press, Champaign, 1996, p. 82<br />

[7] BRUNNER, G., PETER, S., Sep. Sci. Tech., Vol. 17, 1982,p. 199<br />

[8] STAHL, E., QUIRIN, K.W., Fette Seifen Anstrichmittel, Vol. 87, 1985, p. 219<br />

[9] PETER, S., WEIDNER, E., TIEGS, C., EP 0156374, 1985<br />

[10] WEIDNER, E., ZHANG, Z., CZECH, B., PETER, S., Fat Sci. Technol., Vol. 95, 1993, p. 347<br />

[11] PETER, S., WEIDNER, E., JAKOB, H., Chem. Ing. Tech., Vol. 59, 1987, p. 59<br />

[12] BEN-NASR, H., KRIEGEL, E., REIMANN, K., DE 4010400, 1991<br />

[13] ROSOLIA, F., DE 3936031, 1990<br />

[14] HEIDELAS, J., Agro Food Industry Hi-Tech, Vol. 8, 1997, p. 9

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