Dames & Moore, 1999 - USDA Forest Service
Dames & Moore, 1999 - USDA Forest Service Dames & Moore, 1999 - USDA Forest Service
MEMORANDUM @ Date: December 8. 1998 To: Rik Langendoen, Project Manager From: Karen Mixon, QNQC Manager \b\ Subject: Summary Data Quality Review Holden Mine Remedial Investigation Phase Ill Lagoon Soil Sample Data, Fall 1998 Dames & Moore Job #17693-005-019 The summary data quality review of 13 soil samples collected from October 14 through 15, 1998 has been completed. The samples were analyzed at the Analytical Resources, Incorporated (ARI) laboratory in Seattle, Washington for metals by EPA Method 6010A, (cadmium, copper, and lead). In addition, samples were analyzed for total petroleum hydrocarbons (diesel and heavier than diesel range) by Washington State Department of Ecology TPH methods. The analyses were performed in accordance with the methods specified in €PA Test Methods for Evaluating Solid Waste, SW-846, January 1995, and Washington State Department of Ecology Total Petroleum Hydrocarbons Methods, April 1992. A validation package containing method associated QAIQC data and sample data was provided by the laboratory. The following samples are associated with laboratory work order ARI# Y964: Sample I.D. ARI Sample # Analvses Requested DMLG-4-2 DMLG-4-4 @ DMLG-2-2 Y964A Y964B Y964C Cadmium, Copper, Lead, VVTPH-D ext Cadmium, Copper, Lead, WTPH-D ext Archive DMLG-2-4 DMLG-1-surface Y964D Y964E Cadmium, Copper, Lead, WTPH-D ext Archive DMLG-5-2 Y 964 F Cadmium, Copper, Lead, VVTPH-D ext DMLG-1-2 Y964G Cadmium, Copper, Lead, WTPH-D ext DMLG-1-4 Y 964 H Cadmium, Copper, Lead, WTPH-D ext DMLG-3-2 Y9641 Cadmium, Copper, Lead, WTPH-D ext DMLG-3-4 Y964J Cadmium, Copper, Lead, WTPH-D ext DMLG-5-4 Y964K , Cadmium, Copper, Lead, WTPH-D ext DMLG-2-5 Y964L Archive DMLG-2-7 % Y964M Cadmium, Copper, Lead, WTPH-D ext 1 The following comments refer to ARl's performance in meeting quality control specifications described in the EPA documents "EPA Test Methods for Evaluating Solid Waste, SW-846", January 1995, "USEPA Contract Laboratory Program (CLP) National Functional Guidelines for Inorganic Data Review", February 1994, and 'USEPA Contract Laboratory Program (CLP) National Functional Guidelines for Organic Data Review", February 1994, and Washington State Department of Ecology Total Petroleum Hydrocarbons Methods, April 1992, and the Quality Assurance Project Plan (QAPP) prepared for the Phase Ill Remedial Investigation referenced in an addendum (August 28, 1998) to the Phase Ill Sampling and Analysis Plan. The report is divided into subsections based on type of analyses performed Metals Samples were prepared in the laboratory using EPA Method 3050. Samples were analyzed by ..:@ ICP (EPA Method 6010A). DAMES & MOORE
December 8, 1998 Lagoon Soil Samples, Fall 1998, Holdcn Mine Page 2 1. Holding Time - Acceptable 2. Initial Calibration - Acceptable 3. Continuing Calibration - Acceptable 4. Blanks Copper (3.2 to 4.0 uglL) was detected in calibration blanks (CCBs) associated with several of the sample analyses. As the copper concentration in the samples was substantially greater (100X) than the equivalent soil concentration detected in the CCB, data were not qualified. 5. ICP Interference Check (ICP analysis only) - Acceptable 6. Laboratory Control Sample - Acceptable 7. Laboratory Duplicate Sample - Acceptable 8. Field Duplicate A field duplicate was not collected. 9. Matrix Spike The matrix spike was performed on sample DMLG-4-2. The recoveries for cadmium (-21.4%), copper (-1550%), and lead (14.3%) were outside of the control limits (75-12596). The concentration of cadmium (150 mglkg), copper (17,500 mglkg), and lead (730 mglkg) in the sample exceeded the spiking concentration by greater than 4X. Data qualification was not required. 10. ICP Serial Dilution (ICP analysis only) - Acceptable 11. Detection Limits - Acceptable 12. Type of Review - Summary 13. Overall Assessment of Data The usefulness of the data is based on EPA guidance documents listed above. Upon consideration of the information presented above, the data are acceptable except where flagged with data qualifiers that modify the usefulness of the individual values. Orcaanic Analvses Select samples (as noted in the report introduction) were analyzed for TPH (diesel extended range) by the Washington State methods previously referenced. 1. Hold Time Samples DMLG-1-4, DMLG-2-7 %. DMLG-3-2, DMLG-3-4, and DMLG-5-4 were reextracted due to low surrogate recoveries. The surrogate recoveries were acceptable in the reextracts; however, the reextraction occurred ,6 days past the 14 day hold time for extraction. The reextract data was acceptable for site evaluation with qualification. The data are estimated and flagged "J" accordingly.
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MEMORANDUM<br />
@ Date: December 8. 1998<br />
To: Rik Langendoen, Project Manager<br />
From: Karen Mixon, QNQC Manager \b\<br />
Subject: Summary Data Quality Review<br />
Holden Mine Remedial Investigation Phase Ill<br />
Lagoon Soil Sample Data, Fall 1998<br />
<strong>Dames</strong> & <strong>Moore</strong> Job #17693-005-019<br />
The summary data quality review of 13 soil samples collected from October 14 through 15, 1998<br />
has been completed. The samples were analyzed at the Analytical Resources, Incorporated (ARI)<br />
laboratory in Seattle, Washington for metals by EPA Method 6010A, (cadmium, copper, and lead). In<br />
addition, samples were analyzed for total petroleum hydrocarbons (diesel and heavier than diesel range)<br />
by Washington State Department of Ecology TPH methods. The analyses were performed in accordance<br />
with the methods specified in €PA Test Methods for Evaluating Solid Waste, SW-846, January 1995,<br />
and Washington State Department of Ecology Total Petroleum Hydrocarbons Methods, April 1992. A<br />
validation package containing method associated QAIQC data and sample data was provided by the<br />
laboratory. The following samples are associated with laboratory work order ARI# Y964:<br />
Sample I.D. ARI Sample # Analvses Requested<br />
DMLG-4-2<br />
DMLG-4-4<br />
@ DMLG-2-2<br />
Y964A<br />
Y964B<br />
Y964C<br />
Cadmium, Copper, Lead, VVTPH-D ext<br />
Cadmium, Copper, Lead, WTPH-D ext<br />
Archive<br />
DMLG-2-4<br />
DMLG-1-surface<br />
Y964D<br />
Y964E<br />
Cadmium, Copper, Lead, WTPH-D ext<br />
Archive<br />
DMLG-5-2 Y 964 F Cadmium, Copper, Lead, VVTPH-D ext<br />
DMLG-1-2 Y964G Cadmium, Copper, Lead, WTPH-D ext<br />
DMLG-1-4 Y 964 H Cadmium, Copper, Lead, WTPH-D ext<br />
DMLG-3-2 Y9641 Cadmium, Copper, Lead, WTPH-D ext<br />
DMLG-3-4 Y964J Cadmium, Copper, Lead, WTPH-D ext<br />
DMLG-5-4 Y964K , Cadmium, Copper, Lead, WTPH-D ext<br />
DMLG-2-5 Y964L Archive<br />
DMLG-2-7 % Y964M Cadmium, Copper, Lead, WTPH-D ext<br />
1<br />
The following comments refer to ARl's performance in meeting quality control specifications<br />
described in the EPA documents "EPA Test Methods for Evaluating Solid Waste, SW-846", January<br />
1995, "USEPA Contract Laboratory Program (CLP) National Functional Guidelines for Inorganic Data<br />
Review", February 1994, and 'USEPA Contract Laboratory Program (CLP) National Functional<br />
Guidelines for Organic Data Review", February 1994, and Washington State Department of Ecology<br />
Total Petroleum Hydrocarbons Methods, April 1992, and the Quality Assurance Project Plan (QAPP)<br />
prepared for the Phase Ill Remedial Investigation referenced in an addendum (August 28, 1998) to the<br />
Phase Ill Sampling and Analysis Plan.<br />
The report is divided into subsections based on type of analyses performed<br />
Metals<br />
Samples were prepared in the laboratory using EPA Method 3050. Samples were analyzed by<br />
..:@ ICP (EPA Method 6010A).<br />
DAMES & MOORE