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Latest developments in petro2 - Restek's Chromatography Blog ...

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Application for CFC analysis: Impuritie <strong>in</strong> R134a<br />

Column<br />

Column<br />

:<br />

:<br />

30m<br />

30m<br />

x<br />

x<br />

0.53mm<br />

0.53mm<br />

Rt<br />

Rt<br />

Alum<strong>in</strong>a<br />

Alum<strong>in</strong>a<br />

–<br />

–<br />

CFC<br />

CFC<br />

Carrier<br />

Carrier<br />

gas<br />

gas<br />

:<br />

:<br />

He<br />

He<br />

Oven<br />

Oven<br />

:<br />

:<br />

80°C<br />

80°C<br />

for<br />

for<br />

6<br />

6<br />

m<strong>in</strong>.,<br />

m<strong>in</strong>.,<br />

10°C/m<strong>in</strong><br />

10°C/m<strong>in</strong><br />

to<br />

to<br />

140°C,<br />

140°C,<br />

140°C<br />

140°C<br />

hold<br />

hold<br />

for<br />

for<br />

2<br />

2<br />

m<strong>in</strong>.<br />

m<strong>in</strong>.<br />

Injection<br />

Injection<br />

:<br />

:<br />

gas<br />

gas<br />

sampl<strong>in</strong>g,<br />

sampl<strong>in</strong>g,<br />

500<br />

500<br />

ul<br />

ul<br />

1 R 115 = Chloropentafluoroethane<br />

2 R 12 = Dichlorodifluoromethane<br />

3 R 22 = Chlorodifluoromethane<br />

4 R 134a = 1,1,1,2 Tetrafluoroethane<br />

User User had had big big problems with with<br />

Conventional Al2O3 Al2O3 PLOT PLOT<br />

columns<br />

Ref: André Hähnel<br />

Westfalen AG<br />

1<br />

2<br />

3<br />

4<br />

Copyrights: Restek Corporation

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