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Alkoxo and Aryloxo Derivatives of M
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1 Introduction In 1978 the book ent
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1 INTRODUCTION 2 Homometallic Alkox
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Homometallic Alkoxides 5 to complet
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Table 2.1 (Continued) Homometallic
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Table 2.1 (Continued) Homometallic
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Table 2.1 (Continued) Homometallic
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Table 2.1 (Continued) Homometallic
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Homometallic Alkoxides 15 reactivit
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Homometallic Alkoxides 17 By contra
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Homometallic Alkoxides 19 2.3 React
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Homometallic Alkoxides 21 has been
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Homometallic Alkoxides 23 obtain on
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y Evans and co-workers: 160,161 Hom
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Homometallic Alkoxides 27 The heter
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Homometallic Alkoxides 29 not conve
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Homometallic Alkoxides 31 In view o
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2.7.2 Steric Factors Homometallic A
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Homometallic Alkoxides 35 (b) When
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Homometallic Alkoxides 37 2.8 Trans
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Homometallic Alkoxides 39 with orga
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2.9.1.1 Alkoxides of Be, Mg, Ca, Sr
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MfN⊲SiMe3⊳2g2thfx C2HOR, Cpy !C
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Homometallic Alkoxides 45 2.10 Misc
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Zr⊲CH2Bu t ⊳4 C 4RfOH benzene !
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2.10.5 By Insertion of Oxygen into
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Homometallic Alkoxides 51 First hom
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O M R M OR M OR RO M (M = Tl; R = M
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Homometallic Alkoxides 55 3. Nuclea
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Homometallic Alkoxides 57 explain t
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Decomposition (%) 100 80 60 40 20 0
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Table 2.6 Volatilities of tetravale
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Homometallic Alkoxides 63 deduced t
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Table 2.10 Vapour pressure of Ti, Z
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Homometallic Alkoxides 67 Table 2.1
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3.2.10 Alkoxides of Later 3d Metals
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Homometallic Alkoxides 71 Table 2.1
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Homometallic Alkoxides 73 affected
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Homometallic Alkoxides 75 the range
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Homometallic Alkoxides 77 several c
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Table 2.20 (Continued) Homometallic
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Homometallic Alkoxides 81 In toluen
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Bu t O Bu t O Bu t O Th O O Bu O t
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Homometallic Alkoxides 85 1H NMR st
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Homometallic Alkoxides 87 septet wa
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Homometallic Alkoxides 89 experimen
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Table 2.21 1 H NMR spectra of Al4(O
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Homometallic Alkoxides 93 3.5 Elect
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Homometallic Alkoxides 95 ligand fi
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- Page 103 and 104: Homometallic Alkoxides 101 alkoxide
- Page 105 and 106: Homometallic Alkoxides 103 fragment
- Page 107 and 108: Homometallic Alkoxides 105 The mass
- Page 109 and 110: Homometallic Alkoxides 107 [Al⊲OP
- Page 111 and 112: Homometallic Alkoxides 109 Under ca
- Page 113 and 114: 4.3.2 Phenol-Alcohol Exchange React
- Page 115 and 116: 4.4 Reactions with Alkanolamines Ho
- Page 117 and 118: Homometallic Alkoxides 115 R D Pr i
- Page 119 and 120: Homometallic Alkoxides 117 La(OPr i
- Page 121 and 122: Homometallic Alkoxides 119 with the
- Page 123 and 124: Homometallic Alkoxides 121 about 1.
- Page 125 and 126: Homometallic Alkoxides 123 concentr
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- Page 131 and 132: OH Monofunctional bidentate HC N R
- Page 133 and 134: Homometallic Alkoxides 131 metal al
- Page 135 and 136: Homometallic Alkoxides 133 which yi
- Page 137 and 138: shown in Eq. (2.286): O Mo2(OEt)6 H
- Page 139 and 140: Homometallic Alkoxides 137 Phenyl i
- Page 141 and 142: Homometallic Alkoxides 139 The 1990
- Page 143 and 144: Eqs (2.312)-(2.315): where R D l-ad
- Page 145 and 146: Homometallic Alkoxides 143 On the b
- Page 147 and 148: Homometallic Alkoxides 145 The form
- Page 149: Homometallic Alkoxides 147 On furth
- Page 153 and 154: 4Mo2(OPr i )6 + 18CO (excess) Homom
- Page 155 and 156: isolobality of CR 0 and W⊲OR⊳3
- Page 157 and 158: W2(OR)8 (R = CH2Bu t ) + CO + H2C C
- Page 159 and 160: Homometallic Alkoxides 157 43. J.S.
- Page 161 and 162: Homometallic Alkoxides 159 122. P.N
- Page 163 and 164: Homometallic Alkoxides 161 201. A.
- Page 165 and 166: Homometallic Alkoxides 163 281. R.C
- Page 167 and 168: Homometallic Alkoxides 165 358. L.A
- Page 169 and 170: Homometallic Alkoxides 167 430. M.R
- Page 171 and 172: Homometallic Alkoxides 169 521. I.
- Page 173 and 174: Homometallic Alkoxides 171 N.I. Koz
- Page 175 and 176: Homometallic Alkoxides 173 694. R.C
- Page 177 and 178: Homometallic Alkoxides 175 786. R.C
- Page 179 and 180: Homometallic Alkoxides 177 876. J.
- Page 181 and 182: Homometallic Alkoxides 179 966. H.
- Page 183 and 184: Homometallic Alkoxides 181 1054. M.
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200 Alkoxo and Aryloxo Derivatives
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202 Alkoxo and Aryloxo Derivatives
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204 Alkoxo and Aryloxo Derivatives
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206 Alkoxo and Aryloxo Derivatives
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208 Alkoxo and Aryloxo Derivatives
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210 Alkoxo and Aryloxo Derivatives
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212 Alkoxo and Aryloxo Derivatives
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214 Alkoxo and Aryloxo Derivatives
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216 Alkoxo and Aryloxo Derivatives
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218 Alkoxo and Aryloxo Derivatives
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220 Alkoxo and Aryloxo Derivatives
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222 Alkoxo and Aryloxo Derivatives
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224 Alkoxo and Aryloxo Derivatives
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226 Alkoxo and Aryloxo Derivatives
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228 Alkoxo and Aryloxo Derivatives
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230 Alkoxo and Aryloxo Derivatives
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232 Alkoxo and Aryloxo Derivatives
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234 Alkoxo and Aryloxo Derivatives
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236 Table 4.1 (Continued) M-O Bond
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238 Alkoxo and Aryloxo Derivatives
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240 Alkoxo and Aryloxo Derivatives
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242 Alkoxo and Aryloxo Derivatives
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244 Table 4.3 Alkoxides of aluminiu
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246 Alkoxo and Aryloxo Derivatives
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248 Table 4.4 Alkoxides of germaniu
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250 Alkoxo and Aryloxo Derivatives
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252 Alkoxo and Aryloxo Derivatives
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254 Alkoxo and Aryloxo Derivatives
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256 Table 4.6 Alkoxides of scandium
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258 Alkoxo and Aryloxo Derivatives
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260 Alkoxo and Aryloxo Derivatives
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262 Alkoxo and Aryloxo Derivatives
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264 Table 4.7 Alkoxides of lanthani
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266 Alkoxo and Aryloxo Derivatives
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268 Alkoxo and Aryloxo Derivatives
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270 Table 4.8 (Continued) M-O Bond
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272 Alkoxo and Aryloxo Derivatives
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274 Alkoxo and Aryloxo Derivatives
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276 Table 4.9 Alkoxides of titanium
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278 Table 4.9 (Continued) Bond leng
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280 Alkoxo and Aryloxo Derivatives
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282 Alkoxo and Aryloxo Derivatives
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284 Alkoxo and Aryloxo Derivatives
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286 Alkoxo and Aryloxo Derivatives
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288 Alkoxo and Aryloxo Derivatives
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290 Alkoxo and Aryloxo Derivatives
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292 Alkoxo and Aryloxo Derivatives
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294 Alkoxo and Aryloxo Derivatives
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296 Alkoxo and Aryloxo Derivatives
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298 Alkoxo and Aryloxo Derivatives
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300 Table 4.11 Alkoxides of chromiu
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302 Table 4.11 (Continued) Metal M-
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304 Table 4.11 (Continued) M-O Bond
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306 Table 4.11 (Continued) M-O Bond
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308 Table 4.11 (Continued) M-O Bond
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310 Table 4.11 (Continued) M-O Bond
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312 Table 4.11 (Continued) M-O Bond
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314 Table 4.11 (Continued) M-O Bond
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316 Table 4.11 (Continued) Metal M-
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318 Table 4.11 (Continued) M-O Bond
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320 Alkoxo and Aryloxo Derivatives
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322 Table 4.12 Alkoxides of mangane
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324 Alkoxo and Aryloxo Derivatives
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326 Alkoxo and Aryloxo Derivatives
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328 Table 4.15 (Continued) M-O Bond
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330 Alkoxo and Aryloxo Derivatives
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332 Table 4.16 Alkoxides of zinc, c
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334 Alkoxo and Aryloxo Derivatives
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336 Alkoxo and Aryloxo Derivatives
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338 Alkoxo and Aryloxo Derivatives
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340 Table 4.17 (Continued) Coordina
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342 Table 4.17 (Continued) Coordina
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344 Table 4.17 (Continued) Coordina
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346 Alkoxo and Aryloxo Derivatives
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348 Table 4.18 Bimetallic alkoxides
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350 Table 4.18 (Continued) Coordina
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352 Table 4.18 (Continued) Coordina
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354 Table 4.19 Heterometallic alkox
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356 Alkoxo and Aryloxo Derivatives
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358 Table 4.20 Heterometallic alkox
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360 Table 4.20 (Continued) Coordina
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362 Table 4.21 Heterometallic alkox
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364 Alkoxo and Aryloxo Derivatives
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366 Table 4.22 (Continued) Coordina
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368 Alkoxo and Aryloxo Derivatives
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370 Alkoxo and Aryloxo Derivatives
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372 Alkoxo and Aryloxo Derivatives
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374 Alkoxo and Aryloxo Derivatives
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376 Alkoxo and Aryloxo Derivatives
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378 Alkoxo and Aryloxo Derivatives
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380 Alkoxo and Aryloxo Derivatives
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382 Alkoxo and Aryloxo Derivatives
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384 Alkoxo and Aryloxo Derivatives
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386 Alkoxo and Aryloxo Derivatives
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388 Alkoxo and Aryloxo Derivatives
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390 Alkoxo and Aryloxo Derivatives
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392 Alkoxo and Aryloxo Derivatives
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394 Table 5.2 Chemical shifts from
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396 Alkoxo and Aryloxo Derivatives
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398 Alkoxo and Aryloxo Derivatives
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400 Table 5.3 Scandium, yttrium, la
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402 Table 5.3 (continued) Metal Oxo
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404 Alkoxo and Aryloxo Derivatives
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406 Table 5.4 Titanium and zirconiu
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408 Alkoxo and Aryloxo Derivatives
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410 Alkoxo and Aryloxo Derivatives
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412 Alkoxo and Aryloxo Derivatives
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414 Table 5.5 (continued) Metal Oxo
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416 Alkoxo and Aryloxo Derivatives
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418 Alkoxo and Aryloxo Derivatives
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420 Table 5.6 Chromium sub-group me
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422 Table 5.6 (continued) Metal Oxo
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424 Table 5.6 (continued) Metal Oxo
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426 Alkoxo and Aryloxo Derivatives
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428 Alkoxo and Aryloxo Derivatives
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430 Alkoxo and Aryloxo Derivatives
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432 Alkoxo and Aryloxo Derivatives
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434 Table 5.9 (continued) Metal Oxo
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436 Alkoxo and Aryloxo Derivatives
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438 Alkoxo and Aryloxo Derivatives
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440 Alkoxo and Aryloxo Derivatives
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442 Alkoxo and Aryloxo Derivatives
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1 INTRODUCTION 6 Metal Aryloxides T
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Metal Aryloxides 447 or both of the
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R1 OH O R2 R3NH2 −H2O Scheme 6.3
- Page 451 and 452:
Cl S N N OH O Cl Me 3C NH HN OH HO
- Page 453 and 454:
N OH N OH Me 3C Me3C HO HO N N OH H
- Page 455 and 456:
Metal Aryloxides 455 2Ln C 3Hg⊲C6
- Page 457 and 458:
Metal Aryloxides 457 Mixed halo, ar
- Page 459 and 460:
product metal aryloxide 1e,1f (Eqs
- Page 461 and 462:
Metal Aryloxides 461 Eqs 6.39 and 6
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O Mg Mg OAr O Metal Aryloxides 463
- Page 465 and 466:
3.7 From Metal Hydrides Metal Arylo
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Metal Aryloxides 467 Two other impo
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Metal Aryloxides 469 Table 6.1 Meta
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Table 6.3 W-OAr distances for vario
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Metal Aryloxides 473 At first it is
- Page 475 and 476:
Zr−O distance (Å) V−O distance
- Page 477 and 478:
Metal Aryloxides 477 as expected ar
- Page 479 and 480:
Metal Aryloxides 479 whereas R D Me
- Page 481 and 482:
where OAr = O But But H3C H3C O Ta
- Page 483 and 484:
PPh 2 Ph P Pt OAr PPh2 where OAr =
- Page 485 and 486:
6 SURVEY OF METAL ARYLOXIDES 6.1 Sp
- Page 487 and 488:
487 Na2[V(O) 2(OAr) 2]2.4H2O.DMF 6-
- Page 489 and 490:
489 [Tc(O)(OAr)(di-OAr)] 8-quin 2.0
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491 [Ni3⊲OAr⊳6][ClO4].EtOH 8-qu
- Page 493 and 494:
493 [Pt(OAr⊳2](tcnq) sq. planar P
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495 [Al(OAr) 3].MeOH 8-quin 1.850 (
- Page 497 and 498:
497 [Sb(OAr) 2⊲S2COEt⊳] pentago
- Page 499 and 500:
499 [Tc(O)(OAr)(N-salicylideneDD-gl
- Page 501 and 502:
Metal Aryloxides 501 A contribution
- Page 503 and 504:
503 Table 6.8 Metal bi-phenolates B
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505 Table 6.9 Metal binaphtholates
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507 [TiCl2(di-OAr)]2 two tetrahedra
- Page 509 and 510:
Metal Aryloxides 509 co-workers hav
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511 [Li⊲ 2-OAr⊳]3 planar Li3O3
- Page 513 and 514:
513 Table 6.11 Sodium aryloxides Bo
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Table 6.12 Potassium aryloxides Met
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Table 6.15 Magnesium aryloxides Met
- Page 519 and 520:
519 Table 6.18 Barium aryloxides Bo
- Page 521 and 522:
521 Table 6.19 Group 3 metal and la
- Page 523 and 524:
523 [Me4N]La2Na2⊲ 4-OAr⊳⊲ 3-O
- Page 525 and 526:
525 [Nd⊲OC6H3Ph- 6-C6H5⊳⊲OC6H
- Page 527 and 528:
527 [⊲THF⊳Li⊲ 2-OAr⊳2Sm⊲C
- Page 529 and 530:
529 [Eu⊲ 2-OAr⊳4⊲OAr⊳2⊲ 3
- Page 531 and 532:
531 [Yb(OAr) 3⊲THF⊳2].THF squar
- Page 533 and 534:
Metal Aryloxides 533 carbon atoms a
- Page 535 and 536:
535 [Cp Ł Th(OAr)⊲CH2SiMe3⊳2]
- Page 537 and 538:
Metal Aryloxides 537 amido compound
- Page 539 and 540:
539 Table 6.21 Titanium aryloxides
- Page 541 and 542:
541 [Ti2⊲ 2-OAr⊳2(OAr) 2Cl4]2 e
- Page 543 and 544:
543 [Ti(OAr) 2⊲NMe2⊳2] tetrahed
- Page 545 and 546:
545 [Ti(OAr) 3Bu t ] tetrahedral Ti
- Page 547 and 548:
547 [⊲ArO⊳2Ti⊲ 2-ButNDCC4Et4C
- Page 549 and 550:
549 [Cp⊲C5H3Me-Pri-1,2)Ti(OAr)Cl]
- Page 551 and 552:
551 [CpTi(OAr) 2⊲HPPh⊳] OC6H3Pr
- Page 553 and 554:
553 [Ti⊲di-OAr⊳Cl2].THF 6-coord
- Page 555 and 556:
555 Table 6.22 Zirconium aryloxides
- Page 557 and 558:
557 [Zr(Ind-OAr) 2] 1-indenylphenox
- Page 559 and 560:
559 [Cp2Zr(OAr)] 18-electron Zr, tw
- Page 561 and 562:
Metal Aryloxides 561 The thermal st
- Page 563 and 564:
Metal Aryloxides 563 can only arise
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565 1.839 (2) 138 1.854 (2) 140 [(t
- Page 567 and 568:
567 [V(OAr) 3-N-Li(THF) 3] tetrahed
- Page 569 and 570:
569 [V(O)(di-OAr)] 6-coord. V, both
- Page 571 and 572:
571 cis,mer-[Nb(OAr) 2Cl3(THF)] dis
- Page 573 and 574:
573 [Nb⊲OC6H3Ph- 4-C6H7⊳⊲OAr
- Page 575 and 576:
575 Table 6.26 Tantalum aryloxides
- Page 577 and 578:
577 [(THF)(ArO) 3Ta⊲DNND⊳Ta(OAr
- Page 579 and 580:
579 [Ta(OAr) 2Cl2⊲CH2C6H5⊳] tbp
- Page 581 and 582:
581 [Ta(OAr) 2Cl⊲ 6-C6Me6⊳] OC6
- Page 583 and 584:
583 [Ta(OAr)⊲OC6H3Pri- 2-CMeDCH2
- Page 585 and 586:
585 [f(TMEDA)Na⊲ 2-OAr⊳2g2Cr] 4
- Page 587 and 588:
587 Table 6.28 Molybdenum aryloxide
- Page 589 and 590:
589 [Mo2⊲OAr⊳5⊲NMe2⊳⊲HNMe
- Page 591 and 592:
591 [Mo(Hdi-OAr) 2] 6-coord. Mo, on
- Page 593 and 594:
593 [W2⊲OAr⊳6⊲HNMe2⊳2] OC6F
- Page 595 and 596:
595 [W(OAr) 2⊲DNBu t ⊳2] OC6H3P
- Page 597 and 598:
597 [W(OC6H3Ph- 1-C6H4⊳2⊲PMePh2
- Page 599 and 600:
599 [W⊲OC6HPh3- 1-C6H4-c-C5H8C- O
- Page 601 and 602:
601 [⊲OC⊳3Mn⊲C4H4N⊳Mn⊲CO3
- Page 603 and 604:
603 Table 6.32 Simple aryloxides of
- Page 605 and 606:
605 Table 6.33 Simple aryloxides of
- Page 607 and 608:
607 [NEt4]3fFe6⊲ 4-S⊳4⊲OAr⊳
- Page 609 and 610:
609 [Ru(OAr) 2(CO)(py-CMeO-4)] cis-
- Page 611 and 612:
Table 6.35 Simple aryloxides of osm
- Page 613 and 614:
Metal Aryloxides 613 states, e.g. [
- Page 615 and 616:
Bu t O Bu t (6-I) Bu t Bu t O Metal
- Page 617 and 618:
6.2.10 Group 9 Metal Aryloxides Met
- Page 619 and 620:
Table 6.38 Simple aryloxides of iri
- Page 621 and 622:
Metal Aryloxides 621 Table 6.39 (Co
- Page 623 and 624:
623 [Pd(OAr)⊲C6H3fCH2NMe2g2-2,6)]
- Page 625 and 626:
Metal Aryloxides 625 Table 6.41 Sim
- Page 627 and 628:
627 Table 6.42 Simple aryloxides of
- Page 629 and 630:
629 [(RNC) 2Cu⊲ 2-OAr⊳2Cu(CNR)
- Page 631 and 632:
Metal Aryloxides 631 The two-coordi
- Page 633 and 634:
Table 6.45 (Continued) Metal Arylox
- Page 635 and 636:
Table 6.47 Simple aryloxides of mer
- Page 637 and 638:
637 Table 6.48 Aluminium aryloxides
- Page 639 and 640:
639 [⊲ArO⊳2Al⊲ -OAr⊳2Mg(THF
- Page 641 and 642:
641 [Al(OAr) 2⊲i-Bu⊳] trigonal
- Page 643 and 644:
643 [Al(OAr)Cl(Me)⊲NH2But⊳] OC6
- Page 645 and 646:
645 Table 6.49 Gallium aryloxides B
- Page 647 and 648:
647 Table 6.50 Indium aryloxides Bo
- Page 649 and 650:
Metal Aryloxides 649 Table 6.53 Tin
- Page 651 and 652:
651 Table 6.56 Bismuth aryloxides B
- Page 653 and 654:
REFERENCES Metal Aryloxides 653 1.
- Page 655 and 656:
Metal Aryloxides 655 56. Y. Nakayam
- Page 657 and 658:
Metal Aryloxides 657 123. T.W. Coff
- Page 659 and 660:
Metal Aryloxides 659 202. A. Bell,
- Page 661 and 662:
Metal Aryloxides 661 268. K. Ishiha
- Page 663 and 664:
Metal Aryloxides 663 341. B.S. Kali
- Page 665 and 666:
Metal Aryloxides 665 405. P.N. Rile
- Page 667 and 668:
Metal Aryloxides 667 483. Y. Hayash
- Page 669 and 670:
Metal Aryloxides 669 561. A.P. Shre
- Page 671 and 672:
672 Alkoxo and Aryloxo Derivatives
- Page 673 and 674:
674 Alkoxo and Aryloxo Derivatives
- Page 675 and 676:
676 Alkoxo and Aryloxo Derivatives
- Page 677 and 678:
678 Alkoxo and Aryloxo Derivatives
- Page 679 and 680:
680 Alkoxo and Aryloxo Derivatives
- Page 681 and 682:
682 Alkoxo and Aryloxo Derivatives
- Page 683 and 684:
684 Alkoxo and Aryloxo Derivatives
- Page 685 and 686:
686 Alkoxo and Aryloxo Derivatives
- Page 687 and 688:
688 Index alkoxometallate(IV) ligan
- Page 689 and 690:
690 Index cerium oxo-isopropoxide 3
- Page 691 and 692:
692 Index gas-phase photoelectron s
- Page 693 and 694:
694 Index lead tert-butoxide 386 Le
- Page 695 and 696:
696 Index metal-hydrogen bonds clea
- Page 697 and 698:
698 Index oxo-alkoxides 384, 385, 3
- Page 699 and 700:
700 Index sodium hydroxide 142 sodi
- Page 701 and 702:
702 Index titanium dichloride dieth
- Page 703:
704 Index X X-ray Absorption Near E