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Dionex Instrument Integration for Empower - Installation Guide

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<strong>Installation</strong> <strong>Guide</strong><br />

<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong><br />

<strong>for</strong> <strong>Empower</strong><br />

Version<br />

1.10b<br />

March 2011<br />

© <strong>Dionex</strong>


<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong> <strong>Installation</strong> <strong>Guide</strong><br />

Table of Contents<br />

1 OVERVIEW ........... ................................................................................... 1<br />

2 SYSTEM REQUIREMENTS / COMPATIBILITY ...................................... 2<br />

2.1 Supported <strong>Empower</strong> Workstations .............................................. ....................... 2<br />

2.2 Supported Chromatography <strong>Instrument</strong>s and Drivers .............. ....................... 2<br />

2 .3 PC Requirements ........................................................................... ....................... 5<br />

2 .4 Supported Operating Systems ..................................................... ....................... 5<br />

2.4.1 Windows Security Updates ................................................. ....................... 5<br />

2.4.2 About Virtualization ............................................................. ....................... 6<br />

2 .5 Miscellaneous Requirements ....................................................... ....................... 6<br />

2.5.1 Regional Settings ................................................................ ....................... 6<br />

2. 5.2 Windows User Management ............................................... ....................... 7<br />

2. 5.3 PC Power Management ...................................................... ....................... 7<br />

2. 5.4 Required MDAC Versions ................................................... ....................... 7<br />

2. 5.5 Microsoft .NET Framework ................................................. ....................... 8<br />

2. 5.6 Microsoft MSXML ............................................................... ....................... 8<br />

3 INSTALLATION AND CONFIGURATION ............................ ................... 9<br />

3 .1 Installing <strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong>..................................... ....................... 9<br />

3 .2 Hardware <strong>Installation</strong> .................................................................... ..................... 12<br />

3. 2.1 Connecting the <strong>Dionex</strong> <strong>Instrument</strong>s ................................... ..................... 12<br />

3.3 <strong>Instrument</strong> Configuration in <strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> and<br />

<strong>Empower</strong> . 13<br />

3. 3.1 Chromeleon Server Configuration ...................................... ..................... 13<br />

3. 3.2 <strong>Empower</strong> <strong>Instrument</strong> Configuration Device ........................ ..................... 15<br />

3.3.3 Creating New System in <strong>Empower</strong> ..................... 16<br />

TM ..................................<br />

3 .4 Configuring and Specifying Plates <strong>for</strong> Sample Sets .................. ..................... 17<br />

3.4.1 Manually Defining Plate Types ................................................................ 17<br />

3.4.2 Importing Plate Types .........................................................<br />

..................... 22<br />

3.5 Chromeleon <strong>Installation</strong> Qualification (IQ) ...................................................... 24<br />

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<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong> <strong>Installation</strong> <strong>Guide</strong><br />

1 Overview<br />

<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong> provides an interface <strong>for</strong> controlling a<br />

id chromatography instruments with the <strong>Empower</strong> TM range of <strong>Dionex</strong> liqu<br />

2 software<br />

(from Waters).<br />

Based on Chromeleon the <strong>Dionex</strong><br />

the C leon Server, the<br />

Chromeleon Server Configuration, Control Panels and the Program Editor.<br />

® technology it installs and uses certain portions of<br />

Chromeleon Chromatography Management System such as hrome<br />

This guide describes how to install and configure <strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong><br />

<strong>for</strong><br />

<strong>Empower</strong>.<br />

Tips: Be<strong>for</strong>e installing, read the ‘Readme.html’ file that is available on the<br />

<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong> software disc. The file may<br />

contain last-minute product in<strong>for</strong>mation and supplements this<br />

documentation.<br />

To learn more about <strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong><br />

please refer to the following accompanying documents:<br />

- Release Notes,<br />

- Quick Start <strong>Guide</strong><br />

<strong>Empower</strong> her countries.<br />

TM Software is a registered trademark of Waters in the USA and ot<br />

Microsoft and Windows are registered trademarks of Microsoft Corporation in the<br />

United States<br />

and/or other countries. Other company names and product names mentioned in this manual are<br />

trademarks or registered trademarks of their respective companies.<br />

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<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong> <strong>Installation</strong> <strong>Guide</strong><br />

2 System Requirements / Compatibility<br />

2.1 Supported <strong>Empower</strong> Workstations<br />

This release of <strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong> is designed <strong>for</strong> <strong>Empower</strong><br />

TM 32<br />

2 (Personal Workstation, Workgroup PCs, Enterprise Clients and LAC/E<br />

Acquisition Server), Feature Release 4 or Feature<br />

Release 5.<br />

2.2 Supported Chromatography <strong>Instrument</strong>s and<br />

Drivers<br />

<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong> facilitates the control of a wide range of<br />

<strong>Dionex</strong> chromatography instruments and drivers with <strong>Empower</strong> . This release<br />

tion, micro,<br />

TM<br />

supports the following instruments/drivers (including all Rapid Separa<br />

biocompatible and thermostatted variants):<br />

System Device Type Model Interface<br />

UltiMate 3000 Dual Analytical Pump, Ternary DGP-3600A USB<br />

UltiMate 3000 Dual Analytical Pump, Ternary,<br />

Biocompatible<br />

DGP-3600AB USB<br />

UltiMate 3000 Dual Nano/Cap/Mic Pump, Ternary DGP-3600M USB<br />

UltiMate 3000 Rapid Separation Dual<br />

Analytical<br />

Pump, Ternary<br />

DGP-3600RS USB<br />

UltiMate 3000 Dual Analytical Pump, Ternary<br />

(Second Generation)<br />

DGP-3600SD USB<br />

UltiMate 3000 Dual Micor Pump, Ternary<br />

(Second<br />

Generation), Biocompatible<br />

DGP-360 0BM USB<br />

UltiMate 3000 Analytical Pump, Binary HPG-3200A USB<br />

UltiMate 3000 Nano/Cap/Mic Pump, Binary HPG-320 0M USB<br />

UltiMate 3000 Semiprep Pump, Binary HPG-3200P USB<br />

UltiMate 3000 Rapid Separation Analytical<br />

Pump,<br />

Binary<br />

HPG-3200RS USB<br />

UltiMate 3000 Analytical Pump, Binary (Second<br />

generation)<br />

HPG-3200SD USB<br />

UltiMate 3000 Analytical Pump, Binary<br />

with<br />

solvent selector valves<br />

HPG-340 0A USB<br />

UltiMate 3000 Nano/Cap/Mic Pump, Binary with<br />

solvent selector valves<br />

HPG-3400M USB<br />

UltiMate 3000 Rapid Separation Analytical<br />

Pump,<br />

Binary with solvent selector valves<br />

HPG-3400RS USB<br />

UltiMate 3000 Analytical Pump, Binary with<br />

solvent selector valves (Second<br />

Generation)<br />

HPG-3400SD USB<br />

UltiMate 3000 Analytical Pump, Isocratic<br />

ISO-3100A USB<br />

UltiMate 3000 Analytical Pump, Isocratic (Second<br />

Generation)<br />

ISO-3100SD USB<br />

UltiMate 3000 Micro Pump, Isocratic (Second<br />

Generation), Biocompatible<br />

ISO-3100BM USB<br />

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<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong> <strong>Installation</strong> <strong>Guide</strong><br />

UltiMate 3000 Nano/Cap/Mic Pump, Ternary LPG-3300M USB<br />

UltiMate 3000 Analytical Pump, Quaternary LPG-3400A USB<br />

UltiMate 3000 Analytical Pump, Quaternary,<br />

Biocompatible<br />

LPG-340 0AB USB<br />

UltiMate 3000 Nano/Cap/Mic Pump, Quaternary LPG-3400M USB<br />

UltiMate 3000 Rapid Separation Analytical Pump,<br />

Quaternary<br />

LPG-3400RS USB<br />

UltiMate 3000 Analytical Pump, Quaternary (Second Generation)<br />

LPG-3400SD USB<br />

UltiMate 3000 Micro Pump, Quaternary (Second<br />

Generation), Biocompatible<br />

LPG-340 0BM USB<br />

UltiMate 3000 Nano/Cap Pump,<br />

Binary NCP-3200RS USB<br />

UltiMate 3000 Nano/Cap/Mic Pulled-Loop<br />

WP Autosampler<br />

WPS-3000PL USB<br />

UltiMate 3000 Nano/Cap/Mic Pulled-Loop<br />

WPS-3000PL USB<br />

WP Autosampler<br />

Micro Fraction<br />

Collection Option<br />

UltiMate 3000 Nano/Cap/Mic Pulled-Loop<br />

WP Autosampler, Biocompatible<br />

WPS-3000BPL USB<br />

UltiMate 3000 Nano/Cap/Mic Pulled-Loop<br />

WP Autosampler, Thermostatted<br />

WPS-3000TPL USB<br />

UltiMate 3000 Nano/Cap/Mic Pulled-Loop<br />

WP Autosampler, Thermost.,<br />

Biocomp.<br />

WPS-3000TBPL USB<br />

UltiMate 3000 Analytical Pulled-Loop<br />

WPS-3000TBPL USB<br />

WP Autosampler, Thermost.,<br />

Biocomp.<br />

Ana lytical<br />

UltiMate 3000 Split-Loop WP Autosampler WPS-3000SL USB<br />

UltiMate 3000 Split-Loop WP Autosampler,<br />

Thermost.<br />

WPS-3000TSL<br />

USB<br />

UltiMate 3000 Pulled-Loop WP Autosampler and<br />

Fraction Collector, Thermostatted<br />

WPS-3000TFC USB<br />

UltiMate 3000 Pulled-Loop WP Autosampler<br />

and<br />

Fraction<br />

Collector, Thermost.,<br />

Biocomp.<br />

WPS-3000TBFC USB<br />

UltiMate 3000 Rapid Separation Split-Loop WP<br />

Autosampler<br />

WPS- 3000RS USB<br />

UltiMate 3000 Rapid Separation Split-Loop<br />

WP<br />

Autosampler,<br />

Thermost.<br />

WPS-3000TRS<br />

USB<br />

UltiMate 3000 Rapid Separation Pulled-Loop WP<br />

Autosampler<br />

WPS-3000PLRS USB<br />

UltiMate 3000 Rapid Separation Pulled-Loop WP<br />

Autosampler, Thermost.<br />

WPS-3000TPLRS USB<br />

UltiMate 3000 Nano/Cap/Mic LC Flow Manager FLM-3100 USB<br />

UltiMate 3000 Nano/Cap/Mic LC Flow Manager FLM-3200 USB<br />

UltiMate 3000 Nano/Cap/Mic LC Flow Manager FLM -3300 USB<br />

UltiMate 3000 Column Oven / Thermostat<br />

TCC-3000 USB<br />

UltiMate 3000 Column Oven / Thermostat TCC-3000SD (+<br />

user-installable<br />

UltiMate 3000 Rapid Separation Column Oven /<br />

Thermostat<br />

3<br />

valves)<br />

TCC-3000RS (+<br />

user-installable<br />

valves)<br />

USB<br />

USB


<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong> <strong>Installation</strong> <strong>Guide</strong><br />

UltiMate 3000 Column Oven / Thermostat TCC-3100 USB<br />

UltiMate 3000 Column Oven / Thermostat TCC-3200 USB<br />

UltiMate 3000 Column Oven / Thermostat TCC-3200B USB<br />

UltiMate 3000 Diode Array Detector DAD -3000 USB<br />

UltiMate 3000 Rapid Separation Diode Array<br />

Detector<br />

DAD- 3000RS USB<br />

UltiMate 3000 Multiple Wavelength Detector MWD-3000 USB<br />

UltiMate 3000 Rapid Separation Multiple<br />

Wavelength Detector<br />

MWD-3000RS USB<br />

UltiMate 3000 Variable Wavelength Detector VWD-3100 USB<br />

UltiMate 3000 Rapid Separation Variable<br />

Wavelength Detector<br />

VWD-3400RS UltiMate 3000 Autosampler<br />

Column Compartment ACC-3000 USB<br />

UltiMate 3000 Autosampler Column Compartment ACC-3000T USB<br />

UltiMate 3000 Pump, Loading Pump, Column<br />

Oven<br />

NCS-3500RS USB<br />

UltiMate 3000 Fluorescence Detector FLD-3100 USB<br />

UltiMate 3000 Fluorescence Detector FLD-3400RS USB<br />

ESA Charged Aerosol Detector Corona USB<br />

ESA Charged Aerosol Detector Coro na plus USB<br />

ESA Charged Aerosol Detector Corona utlra USB<br />

ESA Electrochemical Detector Coulo chem III USB<br />

ESA Isocratic Pump 584 and 582 RS232<br />

ESA Autosampler 542 RS232<br />

Miscellaneous<br />

Table 1<br />

Shared Relay and Inputs<br />

Remote Inject (Generic driver)<br />

Virtual Channel Driver (Generic driver)<br />

4<br />

USB


<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong> <strong>Installation</strong> <strong>Guide</strong><br />

2.3 PC Requirements<br />

The PC hardware that is needed <strong>for</strong> <strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong> is<br />

he requirements of the <strong>Empower</strong> TM basically determined by t<br />

software. For details,<br />

please refer to <strong>Empower</strong>’ s documentation.<br />

In addition, <strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> has the following requirements<br />

<strong>for</strong> the PC:<br />

• USB port / RS232 serial port / PCI slot (<strong>for</strong> in<strong>for</strong>mation about connecting<br />

<strong>Dionex</strong><br />

chromatography devices see the documentation of the device to be connected)<br />

• 2 GHz Dual Core processor<br />

• 2 GB RAM (total)<br />

Note: <strong>Dionex</strong> can only guarantee the correct operation of <strong>Dionex</strong> <strong>Instrument</strong><br />

<strong>Integration</strong> <strong>for</strong> <strong>Empower</strong> if both the above requirements and the hardware<br />

and software requirements of the <strong>Empower</strong> met.<br />

TM software are<br />

2.4 Supported Operating Systems<br />

The choice of operating system depends on both the requirements of the <strong>Empower</strong><br />

software (including Feature Releases) and the requirements of <strong>Dionex</strong><br />

<strong>Instrument</strong><br />

<strong>Integration</strong>.<br />

<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> itself is compatible<br />

with:<br />

• English version of Microsoft XP SP3<br />

® Windows ®<br />

• English version of Windows 2003 SP2 Server<br />

®<br />

Note: <strong>Dionex</strong><br />

<strong>Instrument</strong> <strong>Integration</strong> is NOT compatible with 64-bit versions of<br />

Windows.<br />

2.4.1 Windows Security Updates<br />

For optimum security, <strong>Dionex</strong> recommends that you keep your systems<br />

up to date<br />

with the latest security updates. Security updates rarely affect correctly<br />

functioning<br />

programs or change the specified behavior of the system. Most security updates<br />

affect only the handling of invalid input to operating system routines, e.g. so-called<br />

buffer overflows. The risk that a security update affects the correct<br />

operation of<br />

<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> is generally low.<br />

Since security updates should generally be installed as soon as possible to keep the<br />

"window of vulnerability" small, it would make no sense <strong>for</strong> the users to wait until<br />

<strong>Dionex</strong> per<strong>for</strong>ms an exhaustive <strong>for</strong>mal validation, which tests various combinations of<br />

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<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong> <strong>Installation</strong> <strong>Guide</strong><br />

systems and procedures. Instead, we recommend that users test the security updates<br />

briefly in the context of their own installation and operating procedures.<br />

<strong>Dionex</strong> recommends the following test procedure at minimum:<br />

– Install the security update and <strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> on a test<br />

PC<br />

– Run Chromeleon IQ (see Tips under section 3.5).<br />

– If desired, also per<strong>for</strong>m further PQ tests according to your needs.<br />

2.4.2<br />

Tips: <strong>Dionex</strong> will not <strong>for</strong>mally validate Windows security updates. <strong>Installation</strong><br />

and testing of security updates is the user’ s own responsibility.<br />

Should you find any compatibility problem during testing a Windows<br />

Security Update, please contact your <strong>Dionex</strong> support and service center<br />

<strong>for</strong> support. Although we will make reasonable ef<strong>for</strong>ts to solve such<br />

problems, we cannot guarantee compatibility with every security<br />

update.<br />

About Virtualization<br />

Virtualization techniques are usually not fully compatible<br />

with real-time operations<br />

and usage of multiple communication ports, which are essential <strong>for</strong> instrument<br />

control. For this reason, <strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> cannot (reliably)<br />

run on<br />

virtual machines. Communication with the instruments may not be established<br />

at all,<br />

or communication problems are likely to occur.<br />

2.5 Miscellaneous Requirements<br />

2.5.1 Regional Settings<br />

Caution: Make sure the decimal point (".") is used as a decimal<br />

symbol <strong>for</strong> all<br />

users including default user. Otherwise, some operations<br />

may fail.<br />

(If in doubt, open the Windows Control Panel and select<br />

Regional<br />

and Language Options. Click Customize…. On the Numbers tab<br />

page, verify that the decimal point is specified under Decimal<br />

symbol. Click OK and select Advanced tab of Regional<br />

and<br />

Language<br />

Options dialog. Ensure Apply all settings to the current<br />

user account and to the default user profile is selected and click<br />

OK (Figure 1)).<br />

6


<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong> <strong>Installation</strong> <strong>Guide</strong><br />

2.5.2 Windows User Management<br />

Figure 1 Regional and Language Options<br />

For proper interplay of <strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> and <strong>Empower</strong> the logged on<br />

Windows User must have certain privileges<br />

(“User” or “Power User” privileges are not sufficient).<br />

The logged on User must either<br />

be:<br />

• member of the “Chromeleon Operators” Local User<br />

Group<br />

(minimum requirement),<br />

or<br />

• a Windows Administrator.<br />

The “Chromeleon Operators” Group is automatically created during the <strong>Dionex</strong><br />

<strong>Instrument</strong><br />

<strong>Integration</strong> setup and all the current Windows users are automatically added<br />

to the Group.<br />

2.5.3 P C Power Management<br />

Caution: To avoid problems during instrument control, verify that<br />

the<br />

relevant PC Power Management features are disabled<br />

under<br />

Control Panel > Power Options and under Control Panel > System<br />

> Hardware > Device Manager > USB Controllers > USB Root<br />

Hub > Power Management.<br />

2.5.4 Required MDAC Versions<br />

<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> requires specific database interfaces that are provided<br />

with the Microsoft Data Access Components (MDAC). These are normally part of the<br />

supported Windows versions. The validated MDAC versions are:<br />

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<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong> <strong>Installation</strong> <strong>Guide</strong><br />

2.5.5<br />

MDAC Version<br />

2.8 SP1<br />

Tip: The Chromeleon<br />

IQ (see section 3.5) recognizes the following MDAC<br />

versions:<br />

2.5 (RTM - SP3), 2.6 (RTM - SP2), 2.7 (RTM - SP1) and MDAC<br />

2.8 (RTM and SP1) . Future MDAC versions may not be recognized<br />

correctly. If in doubt, check <strong>for</strong> the newest version of Microsoft's<br />

'Component Checker' tool on the Microsoft homepage. A version<br />

of this<br />

tool is also available on the CD:<br />

Other Tools\ODBC\Component_Check.exe.<br />

Microsoft .NET Framework<br />

<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> requires<br />

the Microsoft .NET Framework, Version 3.5<br />

SP1, or higher.<br />

If not already<br />

present on the target computer, the necessary files are automatically<br />

installed. In this case the installation events are logged in a file called<br />

DotNetInstall35.log in the \DxControl\IQ folder.<br />

The Chromeleon IQ (see section 3.5) checks whether .NET is properly installed. If not,<br />

an Error is issued.<br />

2.5.6 Microsoft MSXML<br />

<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> requires the Microsoft MSXML Version<br />

4 SP2, or<br />

higher.<br />

If not already present on the target computer, the necessary files are automatically<br />

installed. In this case the installation events are logged in a file called msxmlsetup.log in<br />

the \DxControl\IQ folder.<br />

The Chromeleon IQ (see section 3.5) checks whether MSXML is properly installed. If<br />

not, an Error is issued.<br />

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<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong> <strong>Installation</strong> <strong>Guide</strong><br />

3 <strong>Installation</strong> and Configuration<br />

Note: <strong>Empower</strong> TM 2 (relevant edition <strong>for</strong> customers configuration) software<br />

Feature Release 4 or 5 must be installed be<strong>for</strong>e installing <strong>Dionex</strong><br />

<strong>Instrument</strong> <strong>Integration</strong>.<br />

Note: <strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong> must be installed<br />

on all<br />

computers that are required to control an UltiMate 3000 and acquire and<br />

process data of an UltiMate 3000. This includes all personal, workgroup,<br />

client and LAC/E onfiguration it<br />

inal servers.<br />

32 computers. Depending on the network c<br />

may also be required to be installed on Citrix or other term<br />

Note: Do not connect <strong>Dionex</strong> instruments via USB to your PC until<br />

<strong>Dionex</strong><br />

<strong>Instrument</strong> <strong>Integration</strong> installation is finished, i.e., until the PC is<br />

rebooted and Chromeleon <strong>Installation</strong> Qualification (IQ) is completed<br />

and passed.<br />

No te: Ensure all <strong>Empower</strong> 2 programs, including the message center, are closed<br />

be<strong>for</strong>e beginning the installation. You may have to end the<br />

INSTRU~1.EXE process using the Task Manager<br />

in order to install<br />

<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong>.<br />

Caution : Make sure that the person per<strong>for</strong>ming the installation has full local<br />

administrator privileges. Otherwise, the installation will fail or be<br />

incomplete. After reboot, the administrator running the setup must<br />

login again so that the installation process can be completed<br />

correctly.<br />

Cauti on: Do not change the installation path, as this may cause various<br />

problems.<br />

Note: After <strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> is installed, the<br />

<strong>Dionex</strong><br />

<strong>Instrument</strong> <strong>Integration</strong> license is automatically<br />

selected on the<br />

License page in the Server Configuration program.<br />

3.1 Installing <strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong><br />

Description Setup Screenshots<br />

The <strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong><br />

Setup is launched.<br />

9


<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong> <strong>Installation</strong> <strong>Guide</strong><br />

Description Setup Screenshots<br />

Click ‘Next’ to accept Destination Location.<br />

Click ‘Next’ to accept Program Folder.<br />

Click ‘Next’ to start Copying Files.<br />

<strong>Installation</strong> progress is shown.<br />

Once status has reached its conclusion the user<br />

is notified that setup actions have been logged.<br />

Click ‘OK’.<br />

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<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong> <strong>Installation</strong> <strong>Guide</strong><br />

Description Setup Screenshots<br />

Once complete the Setup dialog prompts the<br />

installer to restart the computer. The installer<br />

clicks ‘Finish’.<br />

Computer is restarted and upon restart the<br />

installer logs in with administrative privileges<br />

and the installation process and IQ<br />

automatically run.<br />

Click ‘Yes’ to check the report <strong>for</strong> possible<br />

Errors and Warnings (Refer to section<br />

3.5 <strong>for</strong><br />

further details). After closing the IQ report<br />

the<br />

installation finishes.<br />

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3.2 Hardware <strong>Installation</strong><br />

3.2.1 Connecting the <strong>Dionex</strong> <strong>Instrument</strong>s<br />

Note: Do not connect <strong>Dionex</strong> instruments via USB to your PC until <strong>Dionex</strong><br />

<strong>Instrument</strong> <strong>Integration</strong> installation<br />

is finished, i.e., until the PC is<br />

rebooted and Chromeleon <strong>Installation</strong> Qualification (IQ) is completed<br />

and passed.<br />

After successful installation of <strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong>, connect<br />

all <strong>Dionex</strong><br />

instruments to your<br />

PC as described in the Operating Instructions of the<br />

instrument(s).<br />

For each USB connected instrument, follow the Found New Hardware<br />

Wizard as<br />

described in the Operating Instructions of the instrument(s) (Figure 2).<br />

Figure 2 Found New Hardware Wizard<br />

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3.3 <strong>Instrument</strong> Configuration in <strong>Dionex</strong> <strong>Instrument</strong><br />

<strong>Integration</strong> and <strong>Empower</strong><br />

Note: Only two Timebases can be controlled by <strong>Empower</strong><br />

TM .<br />

TM<br />

To control <strong>Dionex</strong> instruments by <strong>Empower</strong> via <strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong>:<br />

• First the corresponding <strong>Dionex</strong> instrument modules<br />

must be added to the<br />

Chromeleon Server Configuration (section 3.3.1).<br />

• <strong>Empower</strong> <strong>Instrument</strong> Configuration device must be also added<br />

to the newly created<br />

timebase in Chromeleon Server Configuration<br />

(section 3.3.2).<br />

• Newly created system must then be added to <strong>Empower</strong> Configuration<br />

System node (section 3.3.3).<br />

3.3.1 Chromeleon Server Configuration<br />

Manager<br />

1. In the Server Configuration program, right-click on the Server name<br />

(Figure 3a)<br />

and select Add Timebase from the context menu (Figure 3b). Enter<br />

a unique<br />

Timebase name (Figure 3c) in the dialog that opens, do not select<br />

the “Create<br />

Folder Structure <strong>for</strong> Your Data” option and click OK (Figure 3d).<br />

a<br />

b c<br />

Figure 3 Adding a Timebase<br />

2. Add all <strong>Dionex</strong> device drivers <strong>for</strong> modules that you need to configure <strong>for</strong> your<br />

Timebase by right-clicking on the Timebase and selecting Add Device…<br />

from<br />

the context menu.<br />

Most devices are connected via a USB interface. The USB address is then used<br />

by Chromeleon to detect a device. The USB address typically contains the serial<br />

number of the instrument. This allows two or more identical modules to be<br />

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present (e.g. two pumps). Click browse (Figure 4a) and double click on the USB<br />

number (Figure 4b).<br />

Figure 4 Assigning Module USB Address<br />

Only the USB addresses of corresponding devices are shown; <strong>for</strong> example,<br />

when<br />

adding UV detectors only the addresses from the UV detectors<br />

are shown.<br />

Caution: In general, you should accept the default device and signal names<br />

on all of the configuration pages. Changed names may cause<br />

problems with control via Panels. (Changing the names<br />

is only<br />

necessary, when you have more than one device of the<br />

same kind,<br />

e.g. two UV detectors. In this case, duplicate names would<br />

cause a<br />

conflict.<br />

In such situations, Chromeleon provides appropriate error<br />

messages.)<br />

Tips: Do not add any devices that are not supported by <strong>Dionex</strong> <strong>Instrument</strong><br />

<strong>Integration</strong>. For a list of supported instruments, refer to section<br />

2.2.<br />

If you want<br />

to record UV signals or other digital data channels, make sure<br />

the channels you want to record are activated in the Server<br />

Configuration.<br />

Note, that there can be interdependencies between the devices.<br />

Because<br />

of this, you may have to revisit some of the dialogs during the installation.<br />

Typical examples are:<br />

- a flow splitter can be assigned to a micro pump,<br />

- a pump can be assigned to an autosampler <strong>for</strong> inject synchronization,<br />

- a WPS-3000(T)SL autosampler can be assigned to a pump <strong>for</strong> purging.<br />

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If you use a DAD-3000RS or an MWD-3000RS, set the number of<br />

spectra buffers to a value >= 5000. To do so, right-click on the Server<br />

name, select Properties… and click on the Advanced tab. Enter a Spectra<br />

buffer 5000.<br />

3. Ad d Sharable Devices (such as the UCI-100 interface) and Generic Drivers (such<br />

as the Integrator Driver), as necessary.<br />

4. Click File and Save <strong>Installation</strong> to save the current configuration.<br />

3.3.2 <strong>Empower</strong> <strong>Instrument</strong> Configuration Device<br />

1. In the Server Configuration program, right-click<br />

on a Timebase and select Add<br />

Device… from the context menu. Select <strong>Empower</strong> within <strong>Dionex</strong> Manufacturers<br />

group of Add device to timebase dialog. Select <strong>Empower</strong> <strong>Instrument</strong><br />

Configuration device and click OK (Figure 5).<br />

Figure 5 <strong>Empower</strong> <strong>Instrument</strong> Configuration Device<br />

Note: The <strong>Empower</strong> <strong>Instrument</strong> Configuration<br />

device automatically configures<br />

settings in the Waters DHCP Server.<br />

2. The <strong>Empower</strong> <strong>Instrument</strong> Configuration dialog box appears stating that the<br />

Timebase has been made available in <strong>Empower</strong> (Figure 6).<br />

Figure 6 Waters DHCP Server Settings Updated<br />

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3. Click OK and select File from Menu and Save <strong>Installation</strong> to save the current<br />

configuration.<br />

3.3.3 Creating New System in <strong>Empower</strong> TM<br />

1. Click Configure<br />

System in <strong>Empower</strong> Pro dialog (Figure 7).<br />

Figure 7 <strong>Empower</strong> Pro Dialog<br />

Note: The <strong>Empower</strong> <strong>Instrument</strong> Configuration device automatically configures<br />

settings in the Waters DHCP Server.<br />

2. Right-click Systems and select New then Chromatographic System<br />

to start the<br />

New Chromatographic System Wizard ( Figure 8).<br />

Figure 8 <strong>Empower</strong> Configuration Manager Systems<br />

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3. Create new system and select required <strong>Dionex</strong> Timebase at System Selection<br />

(Figure 9).<br />

Figure 9 <strong>Empower</strong> System Selection<br />

4. Follow Wizard to completion setting relevant Access Controls and System Name<br />

and ensure that new system is added to Systems View Table of Configuration<br />

Manager.<br />

3.4 Configuring and Specifying Plates <strong>for</strong> Sample<br />

Sets<br />

Note: In <strong>Empower</strong> TM when creating sample set methods the autosampler<br />

plates<br />

(trays) have to be defined.<br />

No the <strong>for</strong>mat<br />

xample position RA1 will be referenced as R:A,1<br />

in <strong>Empower</strong> TM te: When defining the autosampler vial position in <strong>Empower</strong>TM<br />

will differ slightly. For e<br />

.<br />

Note: Refer to Quick Start <strong>Guide</strong> section<br />

3.3.1 <strong>for</strong> further details on how to<br />

define Plates <strong>for</strong> a Sample<br />

Set Method.<br />

3.4.1 Manually Defining Plate Types<br />

The following two examples describe how to register sample trays used in <strong>Dionex</strong><br />

autosamplers based on 1.8/2.0 mL sample tray (40 vials per tray) and 5mL wash vials.<br />

Caution: <strong>Dionex</strong> recommends using the exact naming convention and settings<br />

<strong>for</strong> autosampler plates (trays) as described in Table<br />

2.<br />

1. Right-click Plate Types in Configuration Manager and select New then Plate<br />

Type to start the New Chromatographic System Wizard (Figure 10).<br />

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Figure 10 <strong>Empower</strong> Configuration Manager Plate Types<br />

2. Select Plate tab of New Plate Type dialog and enter Plate Type name<br />

“<strong>Dionex</strong><br />

40 Standard Vials, 2mL” and set <strong>for</strong>mat as XY ( Figure 11).<br />

Figure 11 <strong>Empower</strong> New Plate Type Dialog Plate Tab<br />

3. Select Rows and Columns tab and specify number of rows and columns in tray.<br />

For our example 1.8/2.0 mL, 40 vial sample tray the number of rows are “5” and<br />

the number of columns are “8” (Figure 12).<br />

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Figure 12 <strong>Empower</strong> New Plate Type Dialog Rows and Columns Tab<br />

Note: Further geometric settings <strong>for</strong> the 1.8/2.0 mL sample tray (40 vials<br />

per tray) are not required and can be left as default values.<br />

4. Right-click Plate Types in Configuration Manager and select New<br />

then Plate<br />

Type to start the New Chromatographic System Wizard (Figure 13).<br />

Figure 13 <strong>Empower</strong> Configuration Manager Plate Types<br />

5. Select Plate tab of New Plate Type dialog and enter Plate Type name “<strong>Dionex</strong> 5<br />

Wash Vials” and set <strong>for</strong>mat as XY (Figure 14).<br />

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Figure 14 <strong>Empower</strong> New Plate Type Dialog Plate Tab<br />

6. Select Rows and Columns tab and specify number of rows and columns in tray.<br />

For our example 5mL, autosampler wash vials the number of rows are “1” and<br />

the number of columns are “5” (Figure 15).<br />

Figure 15 <strong>Empower</strong> New Plate Type Dialog Rows and Columns Tab<br />

7. Select Referencing tab and set Scheme referencing to “Sequential” (Figure 16).<br />

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Figure 16 <strong>Empower</strong> New Plate Type Dialog Referencing<br />

8. Plate Types <strong>for</strong> all supported <strong>Dionex</strong> Autosampler Trays should be created as<br />

described in steps 1 to 7 of section 3.4.1 and with naming convention<br />

and settings<br />

in Table 2 below.<br />

Tray Plate Type Na me Well<br />

Size<br />

40 Stan<br />

Vials<br />

dard<br />

Format Referencing<br />

Scheme<br />

<strong>Dionex</strong><br />

40<br />

Standard Vials,<br />

2mL<br />

Default XY XY<br />

96 Wells <strong>Dionex</strong> 96 Wells Default XY XY<br />

384 Wells <strong>Dionex</strong> 384 Wells 4 XY<br />

96 Deep Wells<br />

<strong>Dionex</strong> 96 Deep<br />

Wells<br />

384 Deep <strong>Dionex</strong> 384 Deep<br />

Wells Wells<br />

72 Micro Vials<br />

24 Deep Wells<br />

5 Wash Vials<br />

<strong>Dionex</strong> 72 Micro<br />

Vials, 1.2mL<br />

<strong>Dionex</strong> 24 Deep<br />

Wells<br />

<strong>Dionex</strong> 5 Wash<br />

Vials<br />

XY<br />

Default XY XY<br />

4 XY XY<br />

Default<br />

Default<br />

XY XY<br />

XY XY<br />

Default XY Sequential<br />

Table 2<br />

21<br />

Rows<br />

[Spacing]<br />

5<br />

[Default]<br />

8<br />

[Default]<br />

16<br />

[4.5]<br />

8<br />

[Default]<br />

16<br />

[4.5]<br />

6<br />

[Default]<br />

4<br />

[Default]<br />

1<br />

[Default]<br />

Columns<br />

[Spacing]<br />

8<br />

[Default]<br />

12<br />

[Default]<br />

24<br />

[4.5]<br />

12<br />

[Default]<br />

24<br />

[4.5]<br />

12<br />

[Default]<br />

6<br />

[Default]<br />

5<br />

[Default]


<strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> <strong>for</strong> <strong>Empower</strong> <strong>Installation</strong> <strong>Guide</strong><br />

3.4.2 Importing Plate Types<br />

Note: The following steps relate to Feature Release 5 of Waters <strong>Empower</strong> TM<br />

2.<br />

1. Select Plate Types in Configuration Manager.<br />

2. Right -click in the right pane where the plate types are listed, and click Import<br />

from Text (Figure 17).<br />

Figure 17 FR5 Plate Types Configuration<br />

3. In the Import Plate Type from Text File dialog box, click Browse to locate the<br />

<strong>Dionex</strong> autosampler files. They can be found in the <strong>Dionex</strong> <strong>Instrument</strong><br />

<strong>Integration</strong><br />

installation directory (typically under C:\DxControl\<strong>Empower</strong>\Plate<br />

Types) or on the disc under Additional Documents\Plate Types. Select a file and<br />

click Open.<br />

Note: You can select only one file at a time.<br />

4. Type a name (refer to Table 2) <strong>for</strong> this plate type in the New Plate Type Name<br />

box (Figure 18).<br />

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5 . Repeat steps 2 to 4 <strong>for</strong> all plate types.<br />

Figure 18 Import Plate Type<br />

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3.5 Chromeleon <strong>Installation</strong> Qualification (IQ)<br />

The Chromeleon <strong>Installation</strong> Qualification (IQ) compares current in<strong>for</strong>mation about<br />

the installed files with a reference list supplied by <strong>Dionex</strong> during the setup. It<br />

generates a report that can be read using the Windows<br />

Notepad or any other word<br />

processor. If the in<strong>for</strong>mation is identical, successful installation of the software is<br />

confirmed. When there are differences, a Note, Warning, or Error<br />

message appears<br />

indicating the following:<br />

Note: No action is required. The file date is different. The note appears only<br />

because<br />

the file was compared to the file in the list supplied with the<br />

setup. The difference should not impair <strong>Dionex</strong> <strong>Instrument</strong><br />

<strong>Integration</strong><br />

functionality.<br />

Warning: Usually, no action is required. If a problem occurs nevertheless,<br />

contact<br />

<strong>Dionex</strong> Service. A warning appears when<br />

the file size or the version<br />

differs from the expected size or version. For example, this<br />

may happen<br />

if newer versions of system files have been installed during<br />

the<br />

installation of other programs and if <strong>Dionex</strong> <strong>Instrument</strong> <strong>Integration</strong> uses<br />

these files as well. It is unlikely that such an update impairs<br />

<strong>Dionex</strong><br />

<strong>Instrument</strong> <strong>Integration</strong> functionality. The warning facilitates<br />

troubleshooting, just in case a problem occurs.<br />

Error: A vital file is missing. Please contact your <strong>Dionex</strong> representative.<br />

The Chromeleon IQ runs automatically at the end of the software installation<br />

process,<br />

and it should be run manually again at the end of the configuration<br />

process:<br />

1. Choose Start > All Programs > <strong>Dionex</strong> > DxControl > <strong>Installation</strong><br />

Qualification. The Chromeleon <strong>Installation</strong> Qualification program<br />

starts.<br />

2. Click Check <strong>Installation</strong>., Figure 19a<br />

3. A message appears: “Please stop other programs (including the Server<br />

Monitor)…”. Acknowledge<br />

this warning. However, <strong>for</strong> running a “Normal” IQ,<br />

no special action is needed.<br />

4.<br />

The Check <strong>Installation</strong> dialog opens.<br />

Accept the default settings: Check Mode = Normal, Report = Full (Figure 19b),<br />

and click Start (Figure 19c).<br />

5.<br />

Be patient. Checking the installation may take a couple of minutes.<br />

6. At the end, a message in<strong>for</strong>ms you about the results. Click Yes to<br />

view the report.<br />

7. Scroll to the end of the report to see the summary with the number of Errors<br />

and Warnings found, Figure 20a. If there are any Errors, the installation<br />

is<br />

corrupt and must be repeated. Notes and Warnings are generally acceptable,<br />

see above.<br />

8. You can use the Find function of your text editor to find quickly the location of<br />

any Warnings in the report.<br />

9. Close the report and Quit the <strong>Installation</strong> Qualification.<br />

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Tip: You can run the IQ at any time to check if your installation is intact.<br />

You can open the last “IQReport” at any time by choosing Start > All<br />

Programs > <strong>Dionex</strong> > DxControl > IQ Log Files > <strong>Installation</strong> Check.<br />

To learn more about the IQ tool, press F1 when the Chromeleon<br />

IQ<br />

window is open. This will launch the related Online Help topics.<br />

a.<br />

c.<br />

b. Use the<br />

default settings<br />

Figure 19 Starting the Chromeleon IQ<br />

manually<br />

Figure 20 The Summary of the IQ Report<br />

25

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