chapter 2 palladium catalysts in suzuki cross- coupling reaction
chapter 2 palladium catalysts in suzuki cross- coupling reaction
chapter 2 palladium catalysts in suzuki cross- coupling reaction
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4.5. Leach<strong>in</strong>g Test<br />
After the <strong>reaction</strong>, catalyst was removed from <strong>reaction</strong> medium by filtration. The<br />
filtrate was concentrated by evaporat<strong>in</strong>g organic solvent. The filtrate was digested <strong>in</strong> the<br />
presence of H2O2 (Merck, 99%) and HNO3 (conc.). The filtrate was diluted to (1/50)<br />
and analyzed by The Inductively Coupled Plasma Mass Spectrometry (ICP-MS).<br />
(Standard solutions were prepared as 1, 2, 4, 8, 10, 20 ppb from standard stock<br />
solution).<br />
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