chapter 2 palladium catalysts in suzuki cross- coupling reaction
chapter 2 palladium catalysts in suzuki cross- coupling reaction
chapter 2 palladium catalysts in suzuki cross- coupling reaction
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2-Acetylbiphenyl: 1 H NMR (400 MHz, CDCl3) δ: 7.57-7.49 (m, 4H); 7.45-7.38<br />
(m, 3H); 7.37-7.33 (m, 2H); 2.01-1.99 (s, 3H); 13 C NMR (100 MHz, CDCl3) δ: 205.0,<br />
141.2, 140.9, 140.8, 130.9, 130.5, 129.1, 128.9, 128.1, 127.7, 30.6; MS: 196 (M + ), 181,<br />
152.<br />
4-Methylbiphenyl: 1 H NMR (400 MHz, CDCl3) δ: 7.67-7.26 (m, 9H); 2.49-<br />
2.41 (m, 3H); 13 C NMR (100 MHz, CDCl3) δ: 141.5, 138.7, 137.3, 129.8, 129.0, 127.3,<br />
127.3, 21.4; MS: 168 (M + ), 152.<br />
4-Phenylanil<strong>in</strong>e: 1 H NMR (400 MHz, CDCl3) δ: 7.62-7.59 (d, 2H); 7.49-7.44<br />
(m, 4H); 7.35-7.31 (m, 1H); 6.79-6.77 (m, 2H); 3.71 (s, 2H); 13 C NMR (100 MHz,<br />
CDCl3) δ: 146.2, 141.5, 131.8, 128.9, 128.3, 126.7, 126.5, 115.7; MS: 169 (M + ).<br />
50
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