Small Particle HPLC Columns - Cp-Analytica
Small Particle HPLC Columns - Cp-Analytica
Small Particle HPLC Columns - Cp-Analytica
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Anti-Diabetic, Anti-Ulcerative, Bronchodilator, Corticosteroids<br />
Anti-Diabetic Glyburide (Glybenclamide) on Ultra IBD<br />
1<br />
2<br />
Peak List:<br />
1. unknown<br />
2. glyburide<br />
Sample:<br />
Inj.: 1µL<br />
Conc.: 500mg/mL<br />
Solvent: water:methanol:acetone<br />
(1:1:2, v/v)<br />
Column: Ultra IBD<br />
Cat. #: 9175565<br />
Dimensions: 150 x 4.6mm<br />
<strong>Particle</strong> size: 5µm<br />
Pore size: 100Å<br />
Conditions:<br />
Mobile phase: water with<br />
0.1% (v/v) acetic acid:<br />
acetonitrile (95:05, v/v)<br />
Flow rate: 1.0mL/min.<br />
Temp.: 27°C<br />
Det.: UV @ 254nm<br />
0 1 2 3 4 5 min.<br />
LC_0069<br />
Bronchodilator Albuterol on Allure® Basix<br />
Peak List:<br />
1. albuterol<br />
Sample:<br />
Inj.: 2.5µL<br />
Conc.: 1.1mg/mL<br />
Solvent: methanol:water<br />
(30:70)<br />
Column: Allure ® Basix<br />
Cat. #: 9161565<br />
Dimensions: 150 x 4.6mm<br />
<strong>Particle</strong> size: 5µm<br />
Pore size: 60Å<br />
Conditions:<br />
Mobile phase: 10mM ammonium<br />
formate, pH 2.5:<br />
acetonitrile<br />
(20:80, v/v)<br />
Flow rate: 1.2mL/min.<br />
Temp.: 25°C<br />
Det.: UV @ 225nm<br />
0 1 2 3 4 5 min.<br />
LC_0089<br />
1<br />
Anti-Ulcerative Cimetidine on Ultra IBD (LC/MS)<br />
Peak List:<br />
1. cimetidine<br />
Sample:<br />
Inj.: 5µL<br />
Conc.: 10µg/mL<br />
Solvent: mobile phase<br />
Phone: 800-356-1688 or 814-353-1300<br />
www.restek.com<br />
1<br />
Column: Ultra IBD<br />
Cat. #: 9175552<br />
Dimensions: 50 x 2.1mm<br />
<strong>Particle</strong> size: 5µm<br />
Pore size: 100Å<br />
Conditions:<br />
Mobile phase: water:acetonitrile<br />
(20:80, v/v)<br />
Flow: 0.2 mL/min.<br />
Column temp.: ambient<br />
Det.: PE/Sciex API 150 EX<br />
Interface: turbo ion spray<br />
Ion mode: positive<br />
Ion spray voltage: 4800V<br />
Temp.: 350°C<br />
Orifice: 10V<br />
Ring: 100V<br />
Auxiliary gas: 6000cc/min.<br />
0 0.2 0.4 0.6 0.8 1.0 1.2 1.4 1.6 1.8 min.<br />
LC_0115<br />
Corticosteroids on Pinnacle II Cyano<br />
(Reversed Phase)<br />
Peak List: Conc. (mg/mL)<br />
1. cortisone 0.1<br />
2. corticosterone 0.5<br />
3. cortisone acetate 0.7<br />
Sample:<br />
Inj.: 5.0µL<br />
Solvent: methanol<br />
Column: Pinnacle II Cyano<br />
Cat. #: 9216565<br />
Dimensions: 150 x 4.6mm<br />
<strong>Particle</strong> size: 5µm<br />
Pore size: 110Å<br />
Conditions:<br />
Mobile phase: water:methanol<br />
(65:35, v/v)<br />
Flow: 1.0mL/min.<br />
Temp.: 30°C<br />
Det.: UV @ 254nm<br />
Pressure: 133 bar<br />
1<br />
0 1 2 3 4 5 6 7 8 9 min.<br />
LC_0186<br />
2<br />
3<br />
91<br />
<strong>HPLC</strong> APPLICATIONS | PHARMACEUTICAL
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