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UNIVERSITI PUTRA MALAYSIA<br />
FABRICATION AND CHARACTERIZATION<br />
OF SOME NiZn-BASED<br />
FERRITE MULTILAYER INDUCTORS<br />
(<strong>MLIS</strong>)<br />
LUCIA LIEW WOAN SHYAN<br />
FSAS 2000 45
FABRICATION AND CHARACTERIZATION<br />
OF SOME NiZn-BASED<br />
FERRITE MULTILAYER INDUCTORS<br />
(<strong>MLIS</strong>)<br />
LUCIA LIEW WOAN SHYAN<br />
MASTER OF SCIENCE<br />
UNIVERSITI PUTRA MALAYSIA<br />
2000
FABRICATION AND CHARACTERIZATION OF SOME NiZn-BASED<br />
FERRITE MULTILAYER INDUCTORS (<strong>MLIS</strong>)<br />
By<br />
LUCIA LIEW WOAN SHYAN<br />
Thesis Submitted in Fulfilment of the Requirements for the<br />
Degree of Master of Science in the Faculty of Science<br />
U niversiti <strong>Putra</strong> malaysia<br />
September 2000
DEDICATIONS<br />
To<br />
Dear Mom and Dad, brothers and sisters<br />
11
Abstract of thesis presented to the Senate of <strong>Universiti</strong> <strong>Putra</strong> <strong>Malaysia</strong> in<br />
fulfilment of the requirement for the degree of Master of Science<br />
FABRICATION AND CHARACTERIZATION OF SOME NiZn-BASED<br />
FERRITE MUL Tll,A YER INDUCTORS (<strong>MLIS</strong>)<br />
By<br />
LUCIA LIEW WOAN SHY AN<br />
September 2000<br />
Chairman: Associate Professor Mansor Hashim, Ph.D.<br />
Faculty: Institute of Advanced Technology<br />
The multilayer inductor is particularly important as a highly stable, easy to use<br />
and miniaturised component in electronic systems, such as radios, VCRs and<br />
computers. There were two main tasks in this research project, one was to<br />
make a proper preparation set-up, and the other was to measure the inductance<br />
and the reciprocal of the Q factor of the multilayer inductors produced. Layers<br />
of ferrite sheets were stacked together with silver layers in between by means<br />
of tape casting method. End metallization was applied to make contact with<br />
the inner conductors. Bulk and multilayered components of the same<br />
dimension were made to undergo parallel conventional sintering. The<br />
experimental work resulted in the complete construction of a tape-casting set<br />
up. The measured L values were in the range of 10-1 to lOS Henries and L fell<br />
rapidly with frequency from 1kHz to 30MHz. The energy was represented by<br />
111
lIQ ranged from 10- 3 to 10 and also fell rapidly within the same frequel\cy<br />
range.<br />
IV
Abstrak tesis yang dikemukakan kepada Senat <strong>Universiti</strong> <strong>Putra</strong> <strong>Malaysia</strong><br />
sebagai memenuhi keperluan untuk ijazah Master Sains.<br />
PEMBENTUKAN DAN PENCIRIAN INDUKTOR PELBAGAI<br />
LAPISAN (<strong>MLIS</strong>) }'ERIT NiZn<br />
Oleh<br />
LUCIA LIE\V \VOAN SHYAN<br />
September 2000<br />
Pengerusi: Profesor Madya Mansor Hashim, Ph.D.<br />
Fakulti: lnstitut Teknologi Maju<br />
lnduktor multi lapisan adalah penting terutamanya sebagai komponen<br />
berkestabilan tinggi, mudah digunakan dan bersaiz amat kecil dalam sistem<br />
elektronik seperti radio, VCR dan komputer. Ada dua objektif utama dalam<br />
kerja peyelidikan ini. Salah satu daripadanya ialah penyediaan satu set alat<br />
yang sesuai untuk pengeluaran komponen pelbagai Iapisan, manakala yang satu<br />
lagi ialah mengukur induktans dan salingan faktor Q induktor pelbagai lapisan<br />
yang dihasilkan. Lapisan ferit diletakkan berselang-seli dengan lapisan perak<br />
Hujung susunan ini dikemaskan dengan meletakkan lapisan perak untuk<br />
dijadikan konduktor. Toroid dan komponen pelbagai lapisan disinter bawah<br />
keadaan pembakaran selari. Kerja ujikaji ini menghasilkan suatu binaan<br />
lengkap peralatan tuangan-pita. Nilai L yang diukur berada dalam julat 10-1 ke<br />
10 ) henry dan L menyusut cepat dengan frckucnsi daripada 1 kHz to 30MHz.<br />
v
Kehilangan tenaga yang diwakili oleh l/Q berada dalam julat 10- 3 ke 10; ia<br />
juga menyusut cepat dengan frekuensi dalam julat yang sarna.<br />
VI
ACKNO\VLEDGEMENTS<br />
First of all, I would like to extend my deepest gratitude to God the Almighty,<br />
for giving me the strength, the faith, the wisdom, the confidence, the courage,<br />
and the helps needed to complete my thesis.<br />
Secondly, I would like to give my greatest appreciation to my dear supportive<br />
supervisor, PM Dr. Mansor Hashim, for his superb supervision, generosity,<br />
patience, endurance, and dedication throughout the whole of this project. Also<br />
not forgetting my supervisory committee members: Dr. Jumiah Bt Hassan and<br />
PM Dr. Salleh Bin Hj. Hamn, and Prof. Dr. Abdul Halim Shaari, the<br />
chairperson of the Examination Committee.<br />
I would also like to thank Dr. M. K Vidyadaran, Mr. Ho Oi Kuan, Miss Azilah<br />
Bt. Abdul Jalil,<br />
during my SEM session.<br />
Many thanks also for Khoon, San, Kak Ana, lab mates, and friends, especially<br />
Fanny, for their generous assistance and encouragement, and also the<br />
technicians, Mr. Nordin and Mr. Roslim, and the lab assistants Pak Mat Rasa.<br />
Finally, special thanks to my parents, brothers and sisters, especially Nancy<br />
who has helped a lot, and brothers and sisters in Christ, for praying earnestly<br />
forme.<br />
VII
I certify that an Examination Committee met on 28 September 2000 to conduct<br />
the final examination of Lucia Liew Woan Shyan on her Master of Science<br />
thesis entitled "Fabrication And Characterization Of Some NiZn-based Ferrite<br />
Multilayer Inductors (MLIs)" in accordance with <strong>Universiti</strong> Pertanian <strong>Malaysia</strong><br />
(Higher Degree) Act 1980 and <strong>Universiti</strong> Pertanian <strong>Malaysia</strong> (Higher Degree)<br />
Regulations 1981 . The Committee recommends that the candidate be awarded<br />
the relevant degree. Members of the Examination Committee are as follows:<br />
Abdul Halim Shaari, Ph. D<br />
Professor<br />
Faculty of Science and Environmental Studies<br />
<strong>Universiti</strong> <strong>Putra</strong> <strong>Malaysia</strong><br />
(Chairman)<br />
Mansor Bin Hashim, Ph.D<br />
Associate Professor<br />
Institute of Advanced Technology<br />
<strong>Universiti</strong> <strong>Putra</strong> <strong>Malaysia</strong><br />
(Member)<br />
Jumiah Bt Hassan, Ph. D<br />
Lecturer<br />
Faculty of Science and Environmental Studies<br />
<strong>Universiti</strong> <strong>Putra</strong> <strong>Malaysia</strong><br />
(Member)<br />
Salleh Bin Hj. Harun, Ph. D<br />
Associate Professor<br />
Faculty of Science and Environmental Studies<br />
<strong>Universiti</strong> <strong>Putra</strong> <strong>Malaysia</strong><br />
(Member)<br />
HAZALI-MOHA YIDIN, Ph. D<br />
Professor/Deputy Dean of Graduate School,<br />
<strong>Universiti</strong> <strong>Putra</strong> <strong>Malaysia</strong><br />
Date: 2 8 NOV 2000<br />
viii
This thesis submitted to the Senate of <strong>Universiti</strong> <strong>Putra</strong> <strong>Malaysia</strong> has been accepted as<br />
fulfilment of the requirement for the degree of Master of Science.<br />
ix<br />
Date: 1 1 JAN 2001
1 hereby declare that the thesis is based on my original work except for<br />
quotations and citations which have been duly acknowledged. I also declare<br />
that it has not been previously or concurrently submitted for any other degree<br />
at UPM or other institutions.<br />
x<br />
LUCT<br />
Date: :2.3 - J' - ;WOO
TABLE OF CONTENTS<br />
Page<br />
DEDICATIONS ... ... ... ..... , ... ...... '" ., . ... .......... '" ... ... ... .... 11<br />
ABSTRACT ..... , ... ... ... ... . , ...... , ...... ... ....... '" ., ...... , '" ... .... 111<br />
ABSTRAK . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . v<br />
ACKNOWLEDGEMENTS ... . .... . ... .................. . . .. . ..... . . . ... VB<br />
APPROVAL SHEETS ... ... ... . . .... ... ... ... ...... ... .. . ............ . .... V1l1<br />
DECLARATION FORM ... ......... ........... . .... ... ... .. . ...... .. , ... x<br />
LIST OF TABLES ... ....... ... ... ... ... ... ....... ... ... ... ... ... ... ... .... XIV<br />
LIST OF FIGURES .... ... ........ ... .................. ......... ... ...... ... x"V<br />
LIST OF PLATES ..... .... ........... ... . ..... ...... . ..... ... ...... .. , .. XVll<br />
LIST OF SYMBOLS & ABBREVIATIONS ....... ... ...... .......... XVlll<br />
CHAPTER<br />
I INTRODUCTION<br />
Ferrites ., ............. ......... ....................... .... ,. 1<br />
Nickel Zinc Ferrite ... ... .. , ............ . , . ..... , ... ... .. 2<br />
Some Magnetic Parameters ............................. 2<br />
Mutilayer Inductor ............... ......... ......... ....... 4<br />
Objectives .. . .. . ... .... , ...... , '" ...... ... ........ , ... ... ... 5<br />
n LITERATURE REVIEW<br />
Intr� .............. ... ....... .. ...... ...... ...... .... 7<br />
"Some Aspects on Ni-Zn Ferrites ..... ... ................. 7<br />
Trend in Modem Technology .... , ... ... ... ... ... ... ... ... 9<br />
Multilayer Components ........ ............... ... ......... 10<br />
Configurations and Parameters ... ... ... . ,. ... ... ... ... .... 12<br />
ill SOME BASIC THEORY<br />
Electromagnetic ..... ...... ...... .. , ......... ... . , .... .. , 15<br />
Definition for B . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. . . ... 15<br />
Magnetic Field Due to Current .. . . .. ... ..... . .. , ... . .. .. . 16<br />
Current-flow Direction of the Magnetic Field... ... ... .... 17<br />
Inductance ... ... ... ...... ...... ... .... ,. ... ... ... ... ... ..... 19<br />
Power/Energy Relationships for Inductors... . . . ... ... 23<br />
Magnetic Flux Density Tn A Multilayer Inductor .... 24<br />
Crystal Structure ofNi-Zn Ferrites ... ...... ...... ........ 26<br />
Ionic Charge Balance and Crystal Structure ...... '" .... 27<br />
Site Preferences of the Ions .. . . . . . . . . . . . . .. . . . . . . . . . . . . . . . . . 28<br />
Xl
Interactions Between Magnetic Moments On the<br />
Site I..attice .................. ......... ... .................. ... 29<br />
The Magnetic Properties ofFerrites . . .. . . . .. . . . . .. . . . . .. . 31<br />
Intrinsic Properties ... . ....... . . . . '" ...... '" . .. .. 31<br />
Extrinsic Properties ....... .. ... ... . .. ... ... ... . . . 34<br />
Effect of Grain Size and Porosity on Permeability .... . 39<br />
Tape Casting . . . . . . . . . . . . . . . . . .. . . . .. . . .. . . . . . . . . ... . .. . . . . .. 41<br />
Tape Casting Process ........................ ......... ..... 42<br />
Skin Depth ... . .... . ...... . ..... . .. ... .. . ......... .. . . .... .... , 45<br />
IV SOME BASIC CONSIDERATION ON MULTILAYER<br />
V METHODOLOGY<br />
Introduction ............... ... ...... . ..... .................. 46<br />
Deflocculant . . . . . . . . , ... ... ...... ...... ... ... ......... ... .. , 47<br />
Sur factant ..... , ... ... ... . .. ... ... ... ... ... ... .. . .. . ... ... .. . 47<br />
Binder ..... ....... ......... ......... ...... ...... .......... .... 49<br />
Pla sticize r... ... ...... ... ...... ...... ...... ......... ... ... ..... 50<br />
Lubricant .. . . . ... . . . , ... ... ... .. . ... ... . .. ... ... ... ... ... ... . 51<br />
VISCOSIty . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53<br />
Num ber of Layer s ..... , ..... , '" ... .... , ..... , .... '" ... . 53<br />
Wet Laye r Thickne ss ...... ..... , ......... ...... . " ... ..... 54<br />
Control of Cast Defects ... . .... . . . ..... . . . .. . ..... ... .. , ... 54<br />
Introduction .. .... . .. ..... .. . . . . , .... , . ... '" ... ... ... ... .. 56<br />
Experiments ......... ........................... ......... .. 59<br />
Two Stage-milling .................. .. , ..... , ... 60<br />
Weighing . . . . .. . .. . .. . . ,. ... ... ... ... ... ... ....... 60<br />
Mixing . . . . .. . . . . . . . . . . . . . . . . . . . .. . . ... . ... . . . . ,. ... 61 .<br />
Pre-smtenng . .... . ...... '" ... ... ... ... ... ... ... ... 62<br />
Add ition of ZnO , Bi 62<br />
Crushing and Sieving . . .. . . . . . . . . . . . . ... . ..... . . . 63<br />
Forming ..... . . .. . ..... . .. . .. ...................... 64<br />
Sinte ring ........ . ... ... ... .............. , ... ... ... 66<br />
VI RESULTS AND DISCUSSION<br />
Introduction ' " ... ........ ... ... ... .. . ... ... ... ...... ... .... 68<br />
Experimental Set-up .. . ... ...... ... ....... ,. ... ... ... .. . . 68<br />
Rheology of Slurry . . . . . . . . . . . . . .. . .. . . .... . . . . . , '" .. . ...<br />
Electrical Analysis of Inductance and Loss Factor<br />
69<br />
l/Q . . . . . , '" .. , ... ... .... ,. '" .,. ... ... ... ... ... .... ..... 70<br />
Microstructure Analysis . ... . . .. . .. . . . . . . . . .. . ..... . ... . . . 80<br />
Xli<br />
xii
VII CONCLlJSION AND SUGGESTIONS<br />
Conclusions<br />
Suggestions<br />
BffiLIOGRAPHY . . . . . . . . . . . . . . . . . . . . . ... .. . . . .. . . . . . . . . . . .. . . . . . .. . . . . . . . ... . 90<br />
APPENDIX A . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 94<br />
APPENDIX B . . .. . .. ........ ... . . . .... ..... . . . . . .. . . ... .. . . . .. .. . . . ... . . . . . . . 97<br />
APPENDIX C '" .. , ......... ... ............... '" ...... ......... '" ... ... ... . 98<br />
VITA '" ... '" ........ , ... '" ........... ...................... ......... '" '" .... 99<br />
xiii<br />
87<br />
88
Table<br />
LIST OF TABLES<br />
Page<br />
2. 1 Some dimentions of multilayer induct ors manufactured<br />
by AEM ,Tn c. ...... ... ... ... ... ... ... ... ... ... ...... ...... ... ... ...... 12<br />
2.2 Some Feat ures of Multilayer In duct ors Man ufact ured<br />
by AEM,ln c. ... ... . . . ... ............... ...... ... ... ......... ... ...... 13<br />
2.3 Some Diment ions of Multilay er Inductors Manufact ured<br />
by TO KO . . 13<br />
2.4 Some Features of Mut itay er In duct ors Manufact ured<br />
by TO KO .. 13<br />
2.5 Som e Dim entions of Multilay er Inducto rs Manu factu red<br />
by TRIGONCO MPO NEN 14<br />
2.6 Some Feat ures of Multilay er In ducto rs Ma nu factu red<br />
by TRIGON CO MPON ENTS... ... ... .............. . ...... ...... 14<br />
3.1 Site Pr eferenc e and Ma gnetic Moment for Som e Metal Ion s.. . 29<br />
4.1 Some Comm on Plas ticiz er ..... . ..... . ... . . . '" .. , ... ...... ... ..... , 51<br />
4.2 Comm on Lu bricants . . . .. , .............. ...... ......... ... ... ... ... .. 53<br />
S. l Stag e I of the Two Stag e-miling ... .<br />
...... . _ _ . .... _ _ . . . . . . _ _ . ..... 60<br />
5.2 Sta ge IT of the Two Sta ge-millin g ........... , ............ ...... . ,. 60<br />
XlV
LIST OF FIGlJRES<br />
Figure Page<br />
3.1 Magnetic Field Pattern of a Single and Long-straight Wire... . .. . 16<br />
3.2 Magnetic Field Pattern of a Current Flowing Through a<br />
Planal Round-turn . .. . . , '" ... '" ......... .. , '" .. , ............ .. , ... ... . 17<br />
3.3 Magnetic Field Pattern of a Long-solenoidal Wire... ... ... ... ... .. 18<br />
3.4 The Magnetic Field, B, set up by a Current i in a solenoid ... '" .... 20<br />
3.5 Circuit Symbol For An Inductor, Along With Associated<br />
Reference Direction For Current and Voltage .... , ............ , ... ... 22<br />
3.6 Construction of A Multilayer Inductor... ... ... ... .................. 25<br />
3.7 Current Flow Along AB Direction in Fig 3.6... ... ... ... ... ... ..... 25<br />
3.8 Magnetic-flux Density Configuration of A Multilayer Inductor<br />
Cross-sectional Area ......... . , ...................... .. , ... " . . .. ... ... 26<br />
3.9 Crystal Lattice of Spinel Structure ..... , .............. , ... ... ... ... ... 28<br />
3.10 Ferrimagnetism; (a) antiparallel alignment of moments of two<br />
sublattices, (b) the net magnetic moment of the lattice. .. . . . . . . ... . . . 30<br />
3.11 Magnetization Curve of a Material with Magnetic Anisotropy.... 32<br />
3.12 . Schematic of Continuous Tape Casting Apparatus ............ '" '" 44<br />
4.1 Structure of a surfactant molecule and its oriented<br />
adsorption at water-oil and water-air interface .... .. ......... ... '" .. , 49<br />
4.2 Molecular Structures of Hydrocarbon Chain and<br />
Fully Hydrolyzed Polyvinyl Alcohol ... ... ..... , '" ... ... ... ... ... ... 50<br />
5.1 HP16334A test Fixture ...... ...... ...... ... '" ... ... ... ... ... ... ... .... 58<br />
5.2 Experimental Flow Chart......... ............... ............... ........ 59<br />
6.1 Schematic of Tape Casting Apparatus... ... ... ... ... ... ... ... ... ... ... 69<br />
6.2 Graph Inductance, Lp, Versus Frequency of Sample<br />
102,202,302 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . '" '" ... ... 71<br />
xv
6.3 Graph Lp Versus Co-firing Temperatures of Sample 102,202,<br />
and 302 at Frequencies 10kHz, 50kHz, and 100kHz ........... , '" 71<br />
6.4 Graph Lp Versus Particle Size of Sample 102,202, and<br />
302 at Frequencies 10kHz, 50kHz, and 100kHz ... ...... . .. ... . ' . .. 72<br />
6.5 Graph lIQ Versus Frequency of Sample 102 ... . ,. '" .. , '" ......... 73<br />
6.6 Graph 1/Q Versus Frequency of Sample 202 ........... , . , . ' " .. , ... 74<br />
6.7 Graph lIQ Versus Frequency of Sample 302...... ...... ... ... ...... 74<br />
6.8 Graph lIQ Versus Frequency of Sample 102,202, and 302... ... . 75<br />
6.9 Graph lIQ Versus Co-firing Temperatures of Sample 102,202,<br />
and 302 at Frequencies 10kHz, 50kHz, and 100kHz ........ , .,. .... 76<br />
6.10 Graph l/Q Versus Particle Size of Sample 102, 202, and<br />
302 at Frequencies 10kHz, 50kHz, and 100kHz ... ......... '" ... . 76<br />
6.11 Graph Inductance, Lp Versus Frequency of Sample T002... ... . 78<br />
6.12 Graph l/Q Versus Frequency of Sample T002... ... ......... ....... 78<br />
6.13 SEM Photo Shows the Microstructure of Top Ferrite Layer Before<br />
Final Co-firing ... ... ... ...... ... ... '" ...... '" ... ... ... ... ... ... ... ... ... . 80<br />
6.14 (a), (b) and (c) Shows the SEM Microstructure of Ferrite Layer<br />
Co-fired at 620°C/8h ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... 80<br />
6.15 SEM Photo Shows the Microstructure of Ferrite Layer Co-fired<br />
at 600°C/8h ... '" ............... '" ... ...... ...... ...... '" ...... '" ... ..... 83<br />
6.16 (a), (b) SEM Photo Shows the Microstructure of Ferrite<br />
Layer Co-fired at 55 0°C/8h ............... ... '" ... ... ... ... ... ... ... ..... 83<br />
6.17 SEM Photo Shows the Imperfections Between Silver and<br />
Ferrite Layer. ........ ......... ......... ..... , ... ... ... .................. '" 85<br />
6.18 SEM Photo Shows the Silver End-termination of the Multilayer<br />
Inductor. .. ... . . . ... ... ... ... .. . ... ... ... ... ... .. . ... ... .. . ... ... ... ... ... . 85<br />
XVI
LIST OF PLATES<br />
�� h�<br />
5. 1 Electronic Analytical Balance . .. .. . .... .. .... , ............. '" ... ... .... 61<br />
5.2 Siever and Crusher. . . . . . . . . '" '" ..... , ... '" .. , ... '" '" ..... , ... '" ... .. 64<br />
5.3 Mould . . . . . . . . , . . . . . . . . . . . . ' " ' " . . . . . , . . , . . . . . . . . . . . . . . . . . . . . . . . . . . , .. , ..... 65<br />
5.4 Pressing Machine ... '" ... .. , .. , .. , ., ................ '" '" .... ,. '" ... ... 65<br />
5.5 Electric Furnace .. . . . , .. , '" .. , ... '" '" ............ '" ... ... ... ... ... ... ... 67<br />
xvii
A cross sectional area<br />
B induction<br />
Bs<br />
Di<br />
Do<br />
f<br />
h hour<br />
LIST OF SYMBOLS AND ABBREVIATIONS<br />
saturated induction<br />
inner diameter<br />
outer diameter<br />
frequency<br />
H applied field<br />
He<br />
HK<br />
coercive force<br />
saturated anisotropy field<br />
K anisotropy energy<br />
L inductance<br />
L/J length<br />
Ms<br />
saturation magnetisation<br />
N number of wire turns<br />
PYA polyvinyl alcohol<br />
Q quality factor<br />
RLF relative loss factort<br />
tan B loss tangent<br />
T thickness<br />
XVIII
W width<br />
XRD X-Ray Diffraction<br />
�<br />
�B<br />
J..1,)<br />
J..l<br />
J..li<br />
magnetic moment<br />
Bohr magneton<br />
permeabil ity of free space<br />
permeability<br />
initial permeability<br />
� ' real part of permeability<br />
J..l"<br />
p<br />
y<br />
imaginary part of permeability or magnetic loss<br />
resistivity<br />
Gyromagnetic ratio<br />
ill angular velocity<br />
a internal stress<br />
A magnetostriction<br />
XIX
CHAPTER I<br />
INTRODUCTION<br />
Ferrites<br />
Ferrites are magnetic ceramic materials, containing mostly iron which is derived<br />
from Fe 2+ O.Fe;+. 03 , and mix with other oxides and carbonates in powdered<br />
form, arranged in such a manner to produce spontaneous magnetisation (Gerald,<br />
1975� Standley, 1972� Crangle, 199 1). There are soft ferrites as wen as hard<br />
ferrites. Soft ferrites become magnetised by relatively low-strength magnetic<br />
field When the applied field is removed, they returned to a state of relatively low<br />
residual magnetism, whereas hard ferrites need high magnetising field and high<br />
remnant magnetism to become magnetised. Since the pioneering works of Snoek<br />
(1936) and Takei (1939), a very large number of studies have been published by<br />
other ferrite scientists, and have generated a wide range of technological<br />
applications (Snelling). In recent years, the rapid developements in the electronic<br />
and electric industries, have created even larger and dynamic changes on the<br />
demands for the uses of ferrites.<br />
Ferrites are ferrimagnetic materials which have domain structures and hysteresis<br />
loops, similar to those of ferromagnetic materials. They have three distinct<br />
crystal structures: the hexagonal magnetoplumbite, dodecahedral garnet and the<br />
spinel structure (Crangle, 1991� Standley, 1972). Hexagonal magnetoplumbite is<br />
a hard ferrite structure, dodecahedral garnet and the spinel are soft ferrite
structures. Soft ferrites are used for applications in which the material must be<br />
easily magnetised and demagnetised such as cores for power transformers, small<br />
electronic transfonners etc. On the other hand, hard magnetic materials are used<br />
for applications requiring pennanent magnets which do not demagnetise easily<br />
such as the pennanent magnets in loudspeakers, telephone receivers, and<br />
automotive starting motors. Anyway, it is the soft ferrites that are of concern in<br />
this research project.<br />
Nickel Zinc Ferrite<br />
The type of ferrite which is used in this research work is Nickel Zinc (NiZn)<br />
ferrite. It was developed for a wide range of applications where high<br />
penneability and low loss were the main requirements. NiZn ferrite is still one of<br />
the most important ferrites for such applications and constitutes a substantial<br />
portion of present day soft ferrite production. NiZn ferrites have been extensively<br />
used as core materials for large number of devices and electrical components such<br />
as inductors, transfonners, antenna rods etc.<br />
Some Magnetic Parameters<br />
One of the most important pammeters in magnetic materials evaluation is the<br />
permeability. Permeability is an extrinsic property and can be defines as ratio of<br />
induction, B to the magnetizing field H.<br />
2
B<br />
1-1=- H<br />
Permeability can also be written in complex form, where the real part f.l' showed<br />
the energy stored, expressing the component of B in phase with H and the<br />
imaginary part ll" indicating the energy dissipated, expressing the component of<br />
B out of phase with H.<br />
The permeability concept can be extended to include the losses. For time<br />
hannonic fields,<br />
H = Hoexp(joot)<br />
where 00 is the angular frequency and t is the time. The dissipation can be<br />
described as the phase difference between H and B, o. In the complex notation,<br />
the frequency dependency of permeability becomes<br />
ll(W) = B exp j(id +0)<br />
H exp(ja>t)<br />
which would give us, again,<br />
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where J.1" can actually be obtained from the relation<br />
ll" = �l' tan 0<br />
Permeability can not only be influenced by the chemical composition and<br />
crystal structure, but is also strongly dependent on microstructure, temperature,<br />
stress and time after demagnetization.<br />
Multilayer Inductors<br />
"Multi _" comes from the word "multiple" which means having many parts or<br />
elements, or a quantity which contains another quantity an exact number of times<br />
as we use in mathematics.<br />
Multilayer chip inductors were introduced in 1987 and soon became the inductive<br />
components of choice for many design engineers. For example, Toko, a Japanese<br />
company, introduced the first microminiature multilayer chip inductor LL2012 in<br />
the year 1992. And soon it became the inductive components of choice for many<br />
design engineers.<br />
Multilayer technology offers three advantages:<br />
I. Monolithic structure which is good for high reliability<br />
2. Magnetic shielding which is excellent for very high density applications<br />
3. Low mounting cost as multilayer (chip) inductors do not require winding<br />
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