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3. FOOD ChEMISTRy & bIOTEChNOLOGy 3.1. Lectures

3. FOOD ChEMISTRy & bIOTEChNOLOGy 3.1. Lectures

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Chem. Listy, 102, s265–s1311 (2008) Food Chemistry & Biotechnology<br />

Table IV<br />

Concentration of methanolic hydrolysed extract from Melampyrum cristatum L. flowers<br />

Compound nr.<br />

The quantitative analyses are made after the method<br />

from Cynarae folium monography and Crategus folium cum<br />

flore monography by FR IX and FR X.<br />

REFEREnCES<br />

1. Vlase L., Radu L., Fodorea C., Leucuţa S., Gocanj S.:<br />

Liq. Chromatogr. Related Technol. 28, 3109 (2005).<br />

2. Fodorea C. S., Vlase L, Leucuţa S., Tămaş M.: Clujul<br />

Medical, 4, 923 (2003).<br />

<strong>3.</strong> Suciu S., Vlase L., Fodorea C. S., Tămaş M., Leucuţa S.:<br />

Revista de Medicină şi Farmacie 50, 52 (2004).<br />

4. Suciu S., Vlase L., Fodorea C. S., Tămaş M., Leucuţa S.:<br />

Clujul Medical 3, 604, (2004).<br />

Identification Confirmation Concentration The quantity<br />

UV MS in extract [μg ml –1 ] in vegetable drug [mg g –1 ]<br />

Quercetol 14 yes yes 2.659 0.01330<br />

Luteolina 16 yes yes 11.122 0.05561<br />

Kaempferol 17 yes yes 1.642 0.00821<br />

Apigenina 18 yes yes 1<strong>3.</strong>479 0.06740<br />

Fig. 4. Mass spectrum of methanolic hydrolysed extract from<br />

Melampyrum cristatum l. flowers<br />

Table. V<br />

The apigenin and luteolin concentration obtained by TLC<br />

Test<br />

M.cristatum<br />

flowers<br />

M.cristatum<br />

leaves<br />

Apigenina Luteolina<br />

Area c [mg ml –1 ] Area c [mg ml –1 ]<br />

21,474.6 0.82 102,25<strong>3.</strong>9 0.74<br />

18,528.3 0.71 107,944.8 0.78<br />

Table VI<br />

The concentration found in rutozid and hiperozid by Melampyrum<br />

cristatum L.flowers and leaves<br />

Melampyrum cristatum<br />

leaves flowers<br />

Rutozid % 1.850 % 1.750 %<br />

Hiperozid % 0.43125 % 0.71875 %<br />

s741<br />

Fig. 5. Densitogram by Melampyrum cristatum flowers<br />

Fig. 6. Densitogram by Melampyrum cristatum leaves

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