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Struktur und Dynamik Poster: Mi., 14:00–16:30 M-P149<br />

Improved growth of Fe/V-superlattices due to H-assistance<br />

Gregor Nowak 1 , Arndt Remhof 1 , Andreas Liebig 2 , Moreno Marcellini 2 ,<br />

Kurt Westerholt 1 , Björgvin Hjörvarsson 2 , Hartmut Zabel 1<br />

1 Institut für Experimentalphysik/Festkörperphysik, Ruhr-Universität Bochum, Germany<br />

– 2 Department of Physic, University Uppsala, Regementsvägen 1, 75121 Uppsala,<br />

Sweden<br />

We studied the influence of hydrogen on the growth of sputter deposited V single<br />

layers and on [Fe(2ML)/V(16ML)]×30 superlattices. We show that the high structral<br />

quality achieved previously [1] can be further improved by using hydrogen enriched Argon<br />

(pAr=7 mbar)as process gas during sputter deposition. At each chosen hydrogen<br />

pressure of up to 2×10 −6 mbar we prepared a series of samples at substrate temperatures<br />

between 270 ◦ C and 320 ◦ C. The structural characterization was carried out by<br />

x-ray diffraction at the wiggler beamline W1.1 at the Hamburg synchrotron laboratory<br />

(HASYLAB). Three trends are observed. The mosaicity decreases, the interface quality<br />

increases (Fig. 1), and the transport measurements of 240 ˚A thick V single layers<br />

grown in H-enriched sputter gas reveal a 53 % higher residual resistivity ratio of 14.2<br />

in comparison to V-layers grown without H-enrichment (Fig. 2). The residual resistivity<br />

ratio is a direct measure of the Cooper pairs coherence length which we could<br />

increase due to the H-enrichment by 25 % to 232 ˚A in V. The Cooper pair coherence<br />

length is mainly li<strong>mit</strong>ed by scattering on structural and chemical defects which could<br />

be reduced in the H-enrich sputter process. We attribute this effects to an increased<br />

surface mobility of the metal atoms in the presence of hydrogen during the sputtering<br />

process [2].<br />

This project was funded by the DFG under contract-Nr. RE 2203-1/1<br />

[1] P. Isberg et al., Vacuum, 48 (1997) 483.<br />

[2] Horch et al., Nature, 398 (1999) 132.<br />

Fig. 1: X-ray radial scans of the Fe/V<br />

superlattices.<br />

Fig. 2: Transport measurements for<br />

26 nm thick V single layers.

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