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(12) PATENT APPLICATION PUBLICATION (21) Application No.6302/DELNP/2008 A<br />

(19) INDIA<br />

(22) Date <strong>of</strong> filing <strong>of</strong> Application :18/07/2008 (43) Publication Date : 24/10/2008<br />

(54) Title <strong>of</strong> the invention : "PROCESS FOR PRODUCING BISPHENOL A"<br />

(51) International classification :C07 37/20 (71)Name <strong>of</strong> Applicant :<br />

(31) Priority Document No :2006-01638 1)MITSUBISHI CHEMICAL CORPORATION<br />

(32) Priority Date :25/01/2006<br />

Address <strong>of</strong> Applicant :14-1 SHIBA 4-CHOME MINATO-KU<br />

(33) Name <strong>of</strong> priority country :Japan<br />

TOKYO JAPAN. Japan<br />

(86) International Application No :PCT/JP2007/000027 (72)Name <strong>of</strong> Inventor :<br />

Filing Date<br />

:24/01/2007<br />

1)NAGAOKA, MICHIHIRO<br />

(87) International Publication No :WO 2007/086239 2)TANAKA, TATSUO<br />

(61) Patent <strong>of</strong> Addition to Application<br />

Number<br />

Filing Date<br />

:NA<br />

:NA<br />

3)KIMURA, HIROAKI<br />

4)HAYASHI, HIDETO<br />

5)NAKAJIMA,IWAO<br />

(62) Divisional to Application Number :NA<br />

Filing Date<br />

:NA<br />

(57) Abstract :<br />

There is provided a process for producing bisplenol (BPA) which includes steps <strong>of</strong> treating a <strong>part</strong> <strong>of</strong> a mother liquor obtained in the<br />

process for production <strong>of</strong> bisphenol A to remove impurities there<strong>from</strong> <strong>and</strong> then feeding again the thus treated mother liquor to the<br />

reaction system, which is capable <strong>of</strong> preventing a BPA production catalyst used therein <strong>from</strong> being deteriorated in catalytic activity.<br />

The process for producing bisphenol A according to the present invention includes a reaction step <strong>of</strong> reacting acetone <strong>and</strong> phenol (PL)<br />

to obtain a reaction mixture containing BPA <strong>and</strong> PL; a low-boiling component separation step <strong>of</strong> separating a BPA-containing<br />

component <strong>from</strong> the reaction mixture; a BPA separation step <strong>of</strong> separating the BPA-containing component into a material flow<br />

containing BPA as a main component <strong>and</strong> a mother liquor containing PL <strong>and</strong> reaction impurities as main components; a light<br />

component separation step <strong>of</strong> subjecting at least a <strong>part</strong> <strong>of</strong> the mother liquor to heat treatment <strong>and</strong> distillation in the presence <strong>of</strong> an<br />

alkali to separate the mother liquor into a light component <strong>and</strong> a heavy component; <strong>and</strong> a recombination reaction step <strong>of</strong> treating the<br />

thus separated light component in the presence <strong>of</strong> a catalyst to allow PL <strong>and</strong> isopropenyl phenol contained in the light component to be<br />

recombined with each other <strong>and</strong> converted into bisphenol A, in which a content <strong>of</strong> isopropyl phenol in a reactdoil out ionoit ined in the<br />

reaction step is controlled to not more than 4% by weight.<br />

No. <strong>of</strong> Pages : 55 No. <strong>of</strong> Claims : 9<br />

The Patent Office Journal 24/10/2008 25810

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