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174 Chapter 7
Table 7.3. Feeding molar ratios and amounts of the linkers used in the syntheses of the Ru-
DEMOF samples.
parent linker (H 3 BTC)
defect linker (5-X-ip)
Sample
H 3 BTC : (H 3 BTC + 5-XipH
2 )
mass
(mg)
5-X-ipH 2 : (H 3 BTC + 5-X-ipH 2 )
mass
(mg)
1a 90% 90.8
10% 9
1b 80% 80.7 20% 18
X = OH
1c 70% 71 30% 26
1d 50% 50.5 50% 43.7
2a 90% 90.8
10% 8
2b 80% 80.7 20% 16
X = H
2c 70% 71 30% 24
2d 50% 50.5 50% 40
3a 90% 90.8
10% 8.7
3b 80% 80.7 20% 17.4
X = NH 2
3c 70% 71 30% 26
3d 50% 50.5 50% 43.5
4a 90% 90.8
10% 12
4b 80% 80.7 X = Br
20% 24
4c 70% 71 30% 35.3