22.09.2015 Views

Neutron Scattering

Neutron Scattering - JuSER - Forschungszentrum Jülich

Neutron Scattering - JuSER - Forschungszentrum Jülich

SHOW MORE
SHOW LESS

You also want an ePaper? Increase the reach of your titles

YUMPU automatically turns print PDFs into web optimized ePapers that Google loves.

Fig. 4 .3 .4 probably represents the first verification of the spin-flip and non-spin flip<br />

scattering from a spin-incoherent scatterer . The example is Vanadium a typical material<br />

used for absolute calibrations of neutron measurements . The scattering above the<br />

background level shows nearly the ideal intensity ratio 2 :1 for spin-flip to non-spin-flip<br />

intensities . In particular, hydrogenous materials have large spin incoherent cross sections .<br />

Figure 4 .8 : Nuclear-spin incoherent scattering from vanadium obtained by rocking the<br />

analyzer crystal through the clastic position . The flipper off data are proportional te the<br />

(++) cross section and the flipper on data are proportional to the (-) cross section . In<br />

contrast to magnetic scattering the result is independent of the neutron polarization with<br />

respect to the scattering vector Q .[7]<br />

We recall that for a magnetic system the spin-flip and non-spin flip scattering should<br />

depend on the polarization of the neutron with respect to Q . This field dependence is<br />

illustrated in Fig . 4 .9 showing the paramagnetic scattering from MnF 2 . In general, we<br />

expect that the final polarization to vary between 0 and -PZ,,tit2al . It is obvious that<br />

this scattering can be distinguished from spin-incoherent scattering . Indeed, one can<br />

easily verify that the difference between the spin-flip scatterings with polarization P I~ Q<br />

and P L Q is proportional te the (para-)magnetic scattering only, free from any other<br />

scattering contributions like coherent nuclear scattering, spin-incoherent scattering and<br />

possible background . The saine is truc for the difference of non-spin flip scatterings with<br />

P Ij Q and P L Q, and Fig . 4 .10 shows such a separation of the paramagnetic scattering<br />

from MnF2 powder diffraction data . Measurements with the unpolarized beam show a<br />

background intensity decaying with Q and various Bragg peaks on top . The Bragg peaks<br />

4-14

Hooray! Your file is uploaded and ready to be published.

Saved successfully!

Ooh no, something went wrong!