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Neutron Scattering

Neutron Scattering - JuSER - Forschungszentrum Jülich

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tribution of bisecting planes (ntosaic) which spans the hatched area being proportional to<br />

k 2 cot0, . Together with the vertical divergence iß delivering a contribution of ßk there results<br />

a resolution volume being proportional to k' cot 0,,, . The variance ofthe scattering angle<br />

AO in eq . (12) follows to (without derivation) :<br />

a 2 a 2 + a 2 2 + a2 172<br />

2 2 2<br />

ao+a, +41<br />

(13)<br />

This dependence shows that the gain in intensity by the mosaic crystal is not to be "paid" by a<br />

worse energy resolution for ao = a, ! Generally, the influence of ri on AO is weak . (Fig . 9)<br />

Which crystals should now be used as monochromators for neutron? Apart front the lattice parameters<br />

further criteria are to be considered : those are the reflectivity, the suppression of<br />

A,/2-contamination, and last not least the availability as given by the technical and fmancial effort<br />

for their production in suitable quality and size . For example, for the saine reflected<br />

wavelength, Cu bas a better resolution as graphite (PG means pyrolytic deposited graphite),<br />

however, an appreciably lower reflectivity (see table 1) and Fig . 7)) . The elastic form factor of<br />

the crystal<br />

plays an important role saine it represents the coherent scattering length and the extinction<br />

cules . Eq . (14) delivers for the diamond lattice the form factors :<br />

2 h+k+1= 4n<br />

F(Q)=_b 1±i = 2n + 1<br />

0 = 2(2n + 1) !!<br />

Thus Ge and Si have the desired property to suppress the ~,/2-contamination of the reflected<br />

beam by means ofthe forbidden (222)-reflection when using the (111)-reflection.<br />

1 .0<br />

Fig . 10) transmission of<br />

PG-filters [4]<br />

0.8<br />

a .s<br />

0.4<br />

0.2<br />

0.5 1 .0 1 .5 2.0 2.5<br />

wavelength ~ iA<br />

9-9

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