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Neutron Scattering

Neutron Scattering - JuSER - Forschungszentrum Jülich

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For a ADP-powder diffractometer the measuring time can be reduced substantially by the<br />

simultaneous use ofmany single detectors or of linear multidetector systems .<br />

As an example for a 2-axes diffractometer specially designed for the investigation of<br />

amorphous systems and liquids the 7C2-instrument installed at the hot neutron source of the<br />

ORPHEE-reactor in Saclay (F) is shown in Fig . 7 . Combined with an exchange of<br />

monochromator crystals there are there différent standard wavelengths available : A,(Ge(111))<br />

= 1 .1 A, ;,(Cu(111)) = 0 .7 A, A,(Ge(311)) = 0.57 A. The linear multidetector allows a<br />

continuous intensity measurement over a range in scattering angle of 128° . The angular<br />

resolution of this instrument is limited as there is no collimation in between the sample<br />

position and the detector. But the I (Q I -range is very large . For the shortest wavelength<br />

k(Ge(311)) = 0.57 A the accessible values extend up to (~ ,aX = 2n I H 20 A- ' .<br />

---SOI!R(:E<br />

CHAUDE<br />

3 TYPES DE COLLIMAIION (BARILLET)<br />

-z<br />

MOPI~;,~iROMA!E'~lRî i!TÎL!~ïAEiLE<br />

Ge 111 ; Cu 1 ;1 ; Ge 311<br />

~(:OLUMAfEUR SOUS VIDE<br />

-MGNITEUR<br />

-UIAF-FIP;ACME<br />

COL AAIEUR INT RNF<br />

NCEINTE A VIDE PCUR PA 'j EUR D'FCH,ANTILLON<br />

FOUR OU CRYOSTA-<br />

- ECNAN [IL ON<br />

Mlr_ IDEIECTEUR 640 CFI.ü!LES<br />

Fig . 7 . Plan of the 2-axes diffractometer 7C2 at the hot source of the ORPHEE-reactor in<br />

Saclay (F)<br />

In the case of the EDP method a polychromatic white beam is used with the scattering angle<br />

being fixed (20 = const .). The dhkl-values result from the time-of-flight measurement of the<br />

neutron velocities - converted to wavelengths - for the hkl reflections . This technique is<br />

specially suitable for pulsed neutron sources . Moreover, it offers some advantages for<br />

7- 9

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