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Neutron Scattering

Neutron Scattering - JuSER - Forschungszentrum Jülich

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White" neutrons<br />

from reactor<br />

Sample<br />

Monochromator<br />

Crystal<br />

Figure 5 .2 : Schematic set-up of a diffraction experiment . The inset shows the relation<br />

between incident and final wave vectors k, k' and the scattering vector Q .<br />

5 .2 Experimental Examples : Static <strong>Scattering</strong><br />

5 .2 .1 Placzek corrections<br />

Figure 5 .2 shows the schematics of a scattering experiment for the determination of S(Q) .<br />

By using a monochromator the incident neutron energy or the wave vector k is fixed . After<br />

scattering the intensity is recorded as a function of the scattering angle 20 without energy<br />

discrimination . This means that the diffraction setup fixes only the direction of kf but<br />

not its magnitude . Therefore, for a given angle différent scattering vectors Q are mixed<br />

as figure 5 .3 shows .<br />

Strictly speaking, this invalidates thé relation (dQ/dÇZ) coh = IbI ZNS(Q) between (angle)<br />

differential cross section and structure factor .<br />

Nevertheless, for high incident energies it is an excellent approximation as long as thé<br />

energy transfer due to inelastic scattering is small compared to thé incident energy E .<br />

This condition is always fulfilled for x-ray scattering because thé incident energy lies in<br />

thé keV range there and thé inelasticity of scattering is limited mainly to thermal energies<br />

kBT which are of thé order of meV .<br />

5-5

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