techniques for approximating the international temperature ... - BIPM

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xiii Foreword This monograph, published by the Bureau International des Poids et Mesures (BIPM), has been compiled by the Comité Consultatif de Thermométrie, one of the eight consultative committees established by the Comité International des Poids et Mesures. The approximations to the International Temperature Scale of 1990 described here provide levels of accuracy that are adequate for the great majority of thermometric requirements, and in general do so with greater convenience or at lower cost than would be the case in realizing the ITS-90 itself. Thermometrists who do require the accuracy only available from, or the imprimatur of, the ITS-90 are referred to the text of that scale and, more particularly, to the companion monograph to this one: "Supplementary Information for the ITS-90", also published by the BIPM in 1990. The Comité Consultatif de Thermométrie expects to update both monographs periodically, probably at intervals of the order of five to eight years. H. PRESTON- THOMAS T.J. QUINN President, CCT Director, BIPM July 1990
xiv Acknowledgments This monograph has been prepared by the Working Group of the Comité Consultatif de Thermométrie (CCT) identified hereunder. Although a large part of the material originated with members of this Working Group, much also was originally contributed by colleagues, either in our laboratories, or in other National Standards Laboratories. In addition, (parts of) various drafts underwent critical review by some members of the CCT and thermometry groups. We thank all of these people for their assistance, and express special appreciation to H. Ronsin (Institut National de Métrologie, France), B. Fellmuth (Amt für Standardisierung Messwesen und Warenprüfung, German Democratic Republic), L. Crovini (Istituto di Metrologia "G. Colonnetti", Italy), R.P. Hudson (then of Bureau International des Poids et Mesures, Paris), R. Rusby (National Physical Laboratory, United Kingdom), and members of the Temperature and Pressure Section (National Bureau of Standards, United States of America). We also thank Mrs. P. Vineham (National Research Council of Canada) for having typed so excellently and so patiently the several successive drafts of this monograph. Working Group 2: R.E. Bedford, National Research Council of Canada Chairman G. Bonnier, Institut National de Métrologie, France H. Maas, Amt für Standardisierung Messwessen und Warenprüfung, German Democratic Republic F. Pavese, Istituto di Metrologia “G. Colonnetti”, Italy.
Page 1 and 2: BUREAU INTERNATIONAL DES POIDS ET M
Page 3 and 4: TECHNIQUES FOR APPROXIMATING THE IN
Page 5 and 6: iv W(100 °C) = 1.385 (exact value
Page 7 and 8: Centre for Quantum Metrology Nation
Page 9 and 10: 2. Type J viii a) temperature range
Page 11 and 12: c) temperature range from 1664.5 °
Page 13: xii
Page 17 and 18: xvi 3.3.2 Melting Points of Gold (1
Page 19 and 20: xviii 11.3 Thermal Contact 111 11.4
Page 21 and 22: 1 1. Introduction The Comité Consu
Page 23 and 24: 3 thermometers except in special ex
Page 25 and 26: 5 The accuracies with which tempera
Page 27 and 28: Table 1.1: Summary of Some Properti
Page 29 and 30: PART 1: TECHNIQUES AND THERMOMETERS
Page 31 and 32: 11 Fig. 2.1: One form of apparatus
Page 33 and 34: 13 Fig. 2.3: Flow cryostat, shown w
Page 35 and 36: 15 Fig. 2.4: Stirred liquid bath fo
Page 37 and 38: 17 contained within a cylindrical c
Page 39 and 40: 19 Fig. 2.5: Schematic drawing of a
Page 41 and 42: 21 device SRM 767 [Schooley et al.
Page 43 and 44: 23 Table 3.1 : Current Best Estimat
Page 45: 25 The widely-used, but not very re
Page 48 and 49: 28 fraction of sample melted) can g
Page 50 and 51: 30 Fig. 3.2a: Apparatus for the cal
Page 52 and 53: 32 Fig. 3.3: Sealed cell for realiz
Page 54 and 55: 34 Final readings of the thermomete
Page 56 and 57: 36 temperatures differ (usually) sy
Page 58 and 59: 38 Fig. 3.4: Cross sectional drawin
Page 60 and 61: 40 Fig. 3.5: Miniature graphite bla
Page 62 and 63: 42 4. Germanium Resistance Thermome
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44 Fig. 4.3: Example of the Π-type
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46 Fig. 4.4: Differences between dc
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48 - conversely, p-doped thermomete
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50 Fig. 4.6: Effect of a radio-freq
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52 that it will not be subject to m
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ln R n = ∑ i= 0 54 ⎛ ln T - P
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56 Fig. 5.1: Resistance (Ω) and s
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58 thermometer wires) caused a more
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60 6. Vapour Pressure Thermometry*
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62 transitions, but it could be app
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n ∑ i= 2 64 L x [ Π − k ] P =
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66 Fig. 6.3: Diagram at constant pr
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68 Fig. 6.4: Schematic construction
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70 Fig. 6.6: Use of an evacuated ja
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72 Following this, the connecting t
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74 Fig. 6.9: (c) N2, CO, Ar, O2, CH
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76 the Weber-Schmidt equation [Webe
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78 Table 6.1: Temperature values (K
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80 into the bulb (hydrous ferric ox
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82 Fig. 6.12: Effect on the vapour
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84 the remaining liquid increases.
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86 Curie constant (C⊥ is about 0.
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8.1 General Remarks 88 8. Platinum
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90 For a group of 45 thermometers h
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92 More recently, Seifert [(1980),
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94 For thermometers with W(4.2 K) <
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96 after 500 h at 1700 °C in air,
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98 normally extends about 50 cm bac
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100 inhomogeneities result from the
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9.5 Approximations to the ITS-90 10
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104 10. Infrared Radiation Thermome
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106 almost negligible. The final ac
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108 11. Carbon Resistance Thermomet
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110 Fig. 11.1: Resistance-temperatu
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112 Table 11.1: Typical Time Consta
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114 calibration after each cool-dow
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116 12. Carbon-Glass Resistance The
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118 Fig. 12.1: Resistance-temperatu
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120 14. Diode Thermometers Diodes c
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122 2 BT V = E0 − − CT ln ( DT)
Page 144 and 145:
124 Fig. 15.1: Principal features o
Page 146 and 147:
126 For a thermometer graduated abo
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128 rise decreases with time but in
Page 150 and 151:
130 Fig. 16.1: (a) Fabrication of I
Page 152 and 153:
132 capillaries of a twin- (or four
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134 advised to choose the thermomet
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136 Fig. 16.6: Distribution of the
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138 and between different thermomet
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140 therefrom) can then be used wit
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142
Page 164 and 165:
144 Fig. 16.8: Tolerances for indus
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146 Stability on thermal cycling is
Page 168 and 169:
18.2.1 Type T Thermocouple 148 With
Page 170 and 171:
150 within ± 0.5 to 0.7 percent. T
Page 172 and 173:
152 insulation even though it be af
Page 174 and 175:
154 Table 18.4: Recommended Sheath
Page 176 and 177:
156 In the case of the Types K and
Page 178 and 179:
158 temperature is measured with th
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160 19. Thermometry in Magnetic Fie
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162 Type of Sensor T(K) Magnetic Fl
Page 184 and 185:
164 be noted that these lower tempe
Page 186 and 187:
166 Fig. 19.2: The change in calibr
Page 188 and 189:
168 Carbon-glass thermometers (Chap
Page 190 and 191:
Ancsin, J. and Phillips, M.J. (1984
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172 Berry, R.J. (1972): The Influen
Page 194 and 195:
174 Brodskii, A.D. (1968): Simplifi
Page 196 and 197:
176 Crovini, L., Perissi, R., Andre
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Hudson, R.P. (1972): Principles and
Page 200 and 201:
180 Lengerer, B. (1974): Semiconduc
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182 OIML (1985): International Reco
Page 204 and 205:
184 Rusby, R.L. (1975): Resistance
Page 206 and 207:
186 Seifert, P. and Fellmuth, B. (1
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188 Ween, S. (1968): Care and Use o
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190 Fig. A.1: Differences between t
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National Institute of Metrology P.O
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194 Appendix C Some Suppliers of Va
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196 Appendix D Calculations Relativ
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198 4. The calculation of the numbe
Page 220 and 221:
200 Appendix F Interpolation Polyno
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- temperature range from 0 °C to 1
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204 where: d0 = 0; d5 = -3.17578007
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