List of used abbreviations - RosDok - Universität Rostock

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Declaration/Erklärung Here by I declare that this work has so for neither submitted to the Faculty of Mathematics and Natural Sciences at the University of Rostock nor to any other scientific Institution for the purpose of doctorate. Further more, I declare that I have written this work by myself and that I have not used any other sources, other than mentioned earlier in this work. Hiermit erkläre ich, daß diese Arbeit bisher von mir weder an der Mathematisch- Naturwissenschaftlichen Fakultät der Universität Rostock noch einer anderen wissenschaftlichen Einrichtung zum Zwecke der Promotion Eingereicht wurde. Ferner erkläre ich, dass ich diese Arbeit selbständig verfasst und keine anderen als die darin angegebenen Hilfsmittel benutzt habe I hereby apply irrevocably to take oral examination in the form of a private viva voce and a public presentation. 100 ______________ Inam Iqbal
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Synthesis of functionalized 2-(aryl
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The ink of the scholar is more holy
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Affectionately Dedicated to “All
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Table of Contents 03 List of used a
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RCM Ring Closing Metathesis TBAI Te
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humans: 1) the thiomethyl of methio
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Chart 3. Structure of sumatriptan S
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disulfide (DADS) and diallyl sulfid
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1. Synthesis of functionalized 2-(a
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3-Arylthio-1-trimethylsilyloxy-1,3-
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under kinetic reaction control, by
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l a u 4-FC6H4 H Me H 40 m a v 4-FC6
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Table 2. Synthesis of thioxanthones
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3a O OSiMe 3 O OMe + Me Me Cl 3TiO
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Table 3. Synthesis of 8a-x 3 7 8 Ar
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Cl + SPh OSiMe 3 3a 9 O OMe O O H i
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solution. The use of an excess (1.5
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Table 4. Synthesis of 12a-r 3 11 12
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2.3 Conclusion In conclusion, I hav
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aromatization). An unseparable 1:2
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Table 5. Synthesis of arenes 14a-l
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3.3 Conclusion In conclusion, I hav
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Mass Spectroscopy: AMD MS40, AMD 40
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131.0 (ArCH), 132.7, 134.0, 135.9,
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(EI, 70 eV): m/z (%): 380 (100), 21
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(m), 1490 (m), 1434 (m), 1383 (w),
Page 53 and 54: 15.4, 16.9, 18.9 (CH3), 28.3 (CH2),
Page 55 and 56: (C). IR (neat): ν̃ = 2945 (w), 29
Page 57 and 58: 948 (w) 853 (m), 803 (m), 751 (m),
Page 59 and 60: 135.4, 139.2, 143.8, 146.5, 182.2 (
Page 61 and 62: Me S O Me Ph Br Methyl 4-methyl-5-(
Page 63 and 64: 35 Cl, 37 Cl, 61), 430 (M + , 35 Cl
Page 65 and 66: ArH). 13 C NMR (62 MHz, CDCl3): δ
Page 67 and 68: Me S O Me Me Methyl 4,6-dimethyl-5-
Page 69 and 70: S Methyl 4-methyl-5-(2-bromoethyl)-
Page 71 and 72: (CH2CH3), 33.3 (CH2), 40.1 (CH2), 5
Page 73 and 74: Me 3,4-Dimethyl-2-phenylsulfanyl-be
Page 75 and 76: Me 3,4-Dimethyl-2-(p-tolylsulfanyl)
Page 77 and 78: OCH3), 7.08-7.17 (m, 7H, Ar); 13 C
Page 79 and 80: (w), 750 (s), 732 (s), 688 (s), 650
Page 81 and 82: 35 Cl 35 Cl, 100), 359 (26), 357 (3
Page 83 and 84: 2924 (w), 2853 (w), 1728 (s), 1712
Page 85 and 86: Me 3-Hydroxy-5-(4-methylphenylsulfa
Page 87 and 88: Et 3-Hydroxy-5-(4-ethylphenylsulfan
Page 89 and 90: (13), 264 (13), 262 (36) ,260 (12),
Page 91 and 92: MS (EI, 70 eV): m/z (%) = 337 (16),
Page 93 and 94: OH O 5'-Hydroxy-[1,1';3',1'']terphe
Page 95 and 96: Refrences 1. Handbook of Chemistry
Page 97 and 98: 20. For a review of [3+3] cyclizati
Page 99 and 100: Nationality Pakistan Place of Birth
Page 101 and 102: Publications 1. Inam Iqbal, Muhamma
Page 103: Tetrahedron 2007, 63, 12562-12575.
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List of used abbreviations - RosDok - Universität Rostock

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