Ordinance and Syllabus - Bhagat Phool Singh Mahila ...

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Paper Code: BPL 203 Pharmaceutical Chemistry-IV (Pharmaceutical Analysis-I)L -- T -- P Total Credits: 044 -- -- Total Marks: 100External Marks: 50Internal Marks: 50Paper Objectives: Analysis of Pharmaceuticals play a very important role in industry as itrelies upon both qualitative and quantitative chemical analysis to ensure that the raw materialused meets Pharmacopoeial specifications and also ensures a quality of finished product inTerms of proportion of components.UNIT IIntroduction: Significance of quantitative analysis in quality control, differenttechniques of analysis, significant figures, rules for retaining significant digits, typesof errors, mean deviation and standard deviation, precision and accuracy,fundamentals of volumetric analysis: law of mass action, activity and activitycoefficient, pH, buffers, method of expressing concentration, primary and secondarystandards.Neutralization Titrations: Acid base concepts, strength of acids and bases,hydrolysis of salts, ionic product of water, neutralization curves, neutralizationindicators, theory of indicators, choice of indicators, mixed indicators. Analysis ofboric acid, mixture of sodium carbonate and bicarbonate.UNIT IINon-aqueous Titrations: Theory of non-aqueous titrations, titration of alkali metalsalts of organic acids, titration of amines and amine salts of organic acids, titration ofhalogen acid salts of bases and titration of acidic substances.Oxidation Reduction Titrations: Concepts of oxidation and reduction, redoxreactions, strength and equivalent weights of oxidizing and reducing agents. Theoryof redox titrations, General principles of potassium permanganate titrations,potassium dichromate titrations potassium iodate titrations, potassium bromatetitrations, cerric sulphate titrations and iodometric titrations. Analysis of ferroussulphate, hydrogen peroxide, potassium bromide, ascorbic acid, sodium thiosulphate,copper sulphate, phenol, sodium sulphite.UNIT IIIPrecipitations Titrations: Precipitation reactions, common ion effect, solubilityproduct, effects of acids, temperature and solvent upon the solubility of a precipitate.Determination of end points in precipitation titrations by Mohr’s method, Volhardsmethod and Fajans method.Gravimetry: Introduction, precipitation methods, the colloidal state, supersaturation,co-precipitation, post-precipitation, conditions of precipitation, precipitation fromhomogeneous solution, precipitation reagents, washing and ignition of the precipitate.Determination of nickel as dimethylglyoximate and aluminium as 8-hydroxyquinolate.48
UNIT IVComplexometric Titrations: Complex ions, complexation, stability of complexes,factors influencing the stability of complexes, Warner’s co-ordination number,complexones, titration curves, types of EDTA titrations, titrations of mixturesincluding use of masking and demasking agents, metal ion indicators. Analysis ofmagnesium and calcium.Miscellaneous methods of analysis: Diazotization titration, Kjeldahl nitrogendetermination, Karl Fischer titration, determination of alcohol in liquid galenicals,oxygen flask combustion.Note: Instruction for Examiner:The Semester examination in each theory subject shall be of 50 marks. The examiner will setnine questions. Student will attempt five questions. First question would be of short answertype question covering all four Units (2.5 Marks per Unit) & it would be compulsory. Twoquestions will be set from each unit & out of which candidate will attempt one question. EachQuestion shall be of 10 marks.Suggested Readings (Latest Editions):1. A. I. Vogel, “Vogel’s Textbook of Quantitative Inorganic Analysis”, London: ELBS/Longman.2. I. M. Kolthoff and V. A. Stenger, “Volumetric Analysis, Vol. II Titration Methods”,New York: Interscience Publishers, Inc.3. K. A. Connors, “A Textbook of Pharmaceutical Analysis”, New York: WileyInterscience.4. Skoog, Hollar and Nieman, “Principles of Instrumental Analysis”, Philadelphia:Harcourt College Publishers.5. T. Higchi, “Pharmaceutical Analysis”, New Delhi: CBS Publishers.6. A. H. Beckett and J. B. Stenlake, “Practical Pharmaceutical Chemistry, Vol. I andII”,London: The Athlon Press of the University of London.49
Page 1 and 2: BPS Mahila Vishwavidyalaya, Khanpur
Page 3 and 4: 7.2 The examination in each semeste
Page 5 and 6: 9.4 Adhoc Grace:If there is any dis
Page 7 and 8: 10. Promotion:11. Division:WhereCi
Page 9 and 10: 16. General Guidelines:16.1 Where t
Page 11 and 12: Drug chargesPre-packagingCentral st
Page 13 and 14: Note: Instruction for Examiner:The
Page 15 and 16: Autonomic nervous system: Physiolog
Page 17 and 18: Paper Code: BPL-107 REMEDIAL BIOLOG
Page 19 and 20: Suggested Readings (Latest Editions
Page 21 and 22: Paper Code: BPP-113Pharmaceutical C
Page 23 and 24: Paper Code: BPP-117REMEDIAL BIOLOGY
Page 25 and 26: products i.e. PVP, Dextran, absorba
Page 33 and 34: Paper Code: BPP-112 Pharmaceutical
Page 37: measurement, large-scale equipment
Page 41 and 42: Pyridine-piperidine: tobacco, areca
Page 45 and 46: nuclear hazards, Solid waste manage
Page 47 and 48: NOTE:Types of listeningStrategies f
Page 51 and 52: Paper Code: BPL-202Pharmaceutical C
Page 53 and 54: Paper Code: BPL-204Pharmaceutical C
Page 55 and 56: Paper Code: BPL-206Pharmaceutics-V
Page 57 and 58: Paper Code: BPL-208Computer Science
Page 59 and 60: Paper Code: BPL-210Pharmaceutical M
Page 63 and 64: Paper Code: BPP-216Pharmaceutics-V
Page 65 and 66: Paper Code: BPL-301 Pharmaceutical
Page 67 and 68: Paper Code: BPL-303 Pharmaceutics-V
Page 69 and 70: Paper Code: BPL-305Pharmaceutics-VI
Page 71 and 72: Paper Code: BPL-307Pharmacology-II
Page 73 and 74: Paper Code: ENG-301Communication Sk
Page 75 and 76: Paper Code: FFA-100Communicative Fr
Page 77 and 78: Paper Code: LAW- 001Legal LiteracyL
Page 81 and 82: Paper Code: BPP-313Pharmaceutics-VI
Page 83 and 84: Propanthaline bromide, Benzhexol, O
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Note: Instruction for Examiner:The
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Suggested Readings (Latest Editions
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Paper Code: BPP-314Pharmaceutics-VI
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Paper Code: BPP-318Pharmacology-III
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Nifedipine, Procainamide, Verapamil
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Packaging of Pharmaceutical Product
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Note: Instruction for Examiner:The
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UNIT IVAnti-epileptics drugs.Anti-P
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Types of closures used for the ster
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Paper Code: BPP-417Pharmaceutics -X
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Paper Code: BPP-421Pharmacology-IV
Page 115 and 116:
Paper Code: BPL-402Pharmaceutical C
Page 117 and 118:
Paper Code: BPL-404Pharmaceutical C
Page 119 and 120:
Paper Code: BPL-406Pharmaceutics -X
Page 121 and 122:
Paper Code: BPL-408Pharmacology-V (
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Paper Code: BPL-410Pharmacology-VI
Page 125 and 126:
Paper Code: BPP-412Pharmaceutical C
Page 127 and 128:
Paper Code: BPP-416Pharmaceutics -X
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