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Study of radiation damage in silicon detectors for high ... - F9

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110 8. ConclusionsReverse anneal<strong>in</strong>g <strong>of</strong> N eff A study <strong>of</strong> the <strong>in</strong>itial phase <strong>of</strong> reverse anneal<strong>in</strong>g <strong>of</strong> N eff ona set <strong>of</strong> dedicated samples gave clear evidence <strong>for</strong> a l<strong>in</strong>ear dependence <strong>of</strong> reverse anneal<strong>in</strong>gtime constant kYl<strong>in</strong> on ir<strong>radiation</strong> uence. This means that at least at the <strong>in</strong>itial stage,relevant <strong>for</strong> the LHC experiments, the reverse anneal<strong>in</strong>g rate is governed by a rst orderprocess.Long term anneal<strong>in</strong>g <strong>of</strong> reverse current <strong>Study</strong> <strong>of</strong> the long term anneal<strong>in</strong>g <strong>of</strong> reversecurrent showed no saturation up toafewmonths at 60 C. An eective ansatz(t) = E e ;t= E ; L ln(t= L ) (8.1)was found to t the results. Lack <strong>of</strong> a natural explanation <strong>of</strong> the logarithmic behaviourhowever <strong>in</strong>dicates the need <strong>for</strong> better understand<strong>in</strong>g <strong>of</strong> the processes responsible.Eect <strong>of</strong> neutron ux Ir<strong>radiation</strong> ux was varied from a few times 10 8 n/cm 2 s to afew times 10 15 n/cm 2 s to check <strong>for</strong> the eect <strong>of</strong> neutron ux on defect generation. Nosignicant dierence among samples irradiated with dierent uxes was observed neither<strong>in</strong> <strong>radiation</strong> <strong>in</strong>duced change <strong>of</strong> N eff nor <strong>in</strong> generated reverse current [56]. The <strong>in</strong>vestigatedux range covers all presently available neutron sources and it seems safe to extrapolateresults from neutron ir<strong>radiation</strong> studies to the expected ux at LHC <strong>of</strong> about 10 6 n/cm 2 s.Eect <strong>of</strong> bias voltage Strict control <strong>of</strong> the bias<strong>in</strong>g condition both dur<strong>in</strong>g and afterir<strong>radiation</strong> lead to the discovery <strong>of</strong> bias <strong>in</strong>uence on defect development. Its orig<strong>in</strong> wasfound not to be <strong>in</strong> the creation <strong>of</strong> defects but <strong>in</strong> their anneal<strong>in</strong>g. Fully biased samplesgave about a factor <strong>of</strong> two <strong>high</strong>er N eff values at the plateau after benecial anneal<strong>in</strong>gas compared to unbiased ones. The dierence, however, annealed out if the bias voltagewas removed. Decrease <strong>of</strong> the dierence can be described by two exponentials with timeconstants at 20 C <strong>of</strong> about 40 h <strong>for</strong> the fast component ( 45%) and six weeks <strong>for</strong> theslow one ( 40%). Activation energy <strong>of</strong> both reactions is around 0.5 eV. The rema<strong>in</strong><strong>in</strong>gdierence anneals out <strong>in</strong> less than 4 hours at all measured temperatures (-7, 5 and 20 C).Few ten percent <strong>of</strong> the dierence however recovers if the sample is biased aga<strong>in</strong>. No eect<strong>of</strong> the bias voltage on time development <strong>of</strong> reverse current was observed.Comparison with previous results In all parameters, previously studied by othergroups (reverse anneal<strong>in</strong>g <strong>of</strong> N eff and long term anneal<strong>in</strong>g <strong>of</strong> reverse current), a goodagreement <strong>of</strong> our results with reported values was found. The rst systematic search <strong>for</strong>an eect <strong>of</strong> neutron ux on defect creation was per<strong>for</strong>med <strong>in</strong> this work. F<strong>in</strong>ally, <strong>in</strong> thescope <strong>of</strong> this work the eect <strong>of</strong> bias voltage on anneal<strong>in</strong>g <strong>of</strong> eective dopant concentrationwas discovered.

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