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High Perfomance: AT-510 Low Cost : AT-500N-1, AT-500N-2 Multi ...

High Perfomance: AT-510 Low Cost : AT-500N-1, AT-500N-2 Multi ...

High Perfomance: AT-510 Low Cost : AT-500N-1, AT-500N-2 Multi ...

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<strong>High</strong> <strong>Perfomance</strong>: <strong>AT</strong>-<strong>510</strong><strong>Low</strong> <strong>Cost</strong> : <strong>AT</strong>-<strong>500N</strong>-1, <strong>AT</strong>-<strong>500N</strong>-2<strong>Multi</strong>-channel Software : <strong>AT</strong>-WinCEmarked forproduct safetyISO 9001for quality assuranceGLP/GMPconformedISO 14001environmentalmanagementsystemsFDA 21 CFR Part 11 Compliant Software : <strong>AT</strong>-Win/ERKYOTO ELECTRONICS


KEM Product LineA wide selection of KEM Automatic Potentiometric Titratorsmodels is available from process or quality control inproduction to research and development works in laboratory.<strong>High</strong> <strong>Perfomance</strong> : <strong>AT</strong>-<strong>510</strong>CHA-500 <strong>Multi</strong>ple Sample Changer as an option.<strong>Low</strong> <strong>Cost</strong> : <strong>AT</strong>-<strong>500N</strong>-1, <strong>AT</strong>-<strong>500N</strong>-21


KEM Product Line<strong>Multi</strong>-Channel Software : <strong>AT</strong>-WinFDA 21 CFR Part 11 Compliant Software : <strong>AT</strong>-Win/ERSecurityIntegrityAudit TrailElectronic Signatures2


Features of <strong>AT</strong> Product Line<strong>AT</strong>-<strong>510</strong> <strong>AT</strong>-<strong>500N</strong>-1 , 2 <strong>AT</strong>-Win <strong>AT</strong>-Win/ERControlling unitMain unitMain unitPCPCLanguageEnglish / JapaneseEnglishEnglish / JapaneseEnglish / JapaneseData entryKey-inKey-inKeyboard and MouseKeyboard and Mouse<strong>Multi</strong>tasking1 channel1 channel4 channels4 channelsDisplay126 x 70mm LCDwith backlight16 digits x 2 linesLCD with backlightScreen display on PCScreen display on PCReal time titration curveYesNoYes(<strong>Multi</strong>-line)Yes(<strong>Multi</strong>-line)GLP/GMP conformedYesYesYesYesConnectable number ofAPB-<strong>510</strong>10 (one built-in)No10 APB-<strong>510</strong> to<strong>AT</strong>-<strong>510</strong> (one built-in)40 APB-<strong>510</strong> to 4<strong>AT</strong>-<strong>510</strong> (4 built-in)10 APB-<strong>510</strong> to<strong>AT</strong>-<strong>510</strong> (one built-in)40 APB-<strong>510</strong> to 4<strong>AT</strong>-<strong>510</strong> (4 built-in)Burette capacity50mL, 20mL, 10mL, 5mL, 1mL--Data storage mediaPC cardNoHD and other devicesHD and other devicesSample changerYesYes--FDA 21 CFR Part 11Need <strong>AT</strong>-Win/ERNeed <strong>AT</strong>-Win/ERNoYesElectronic balanceYesYesYesYesPreamplifierSTD-<strong>510</strong>, POT-<strong>510</strong>PTA-<strong>510</strong>, CMT-<strong>510</strong>TET-<strong>510</strong>STD-<strong>510</strong>PTA-<strong>510</strong>POT-<strong>510</strong>Depending on a titratorSOFT-CAPEYesYes--3


<strong>AT</strong>-<strong>510</strong> Automatic Potentiometric TitratorThe <strong>AT</strong>-<strong>510</strong> Automatic potentiometric titrator is a new version of <strong>AT</strong> seriesoffering better operational maneuverability and compactness in size whileinheriting KEM’s many years’ advanced proven technology. This new modelcan perform potentiometric titration including acid-base, redox, precipitation,chelatometric and non-aqueous titrations. With optional peripherals, it canalso perform photometric, polarization and surfactant titrations. When themultiple sample changer CHA-500 is connected, it can automate measurementsof a number of samples unattended and save both time and man-power withreliable results and simpler operations, thus applicable to many fields wherequality and inspection control, analytical works and R&D activities aredemanded and conducted.Features1.Oversized LCD provides clearer readout ofinformation such as Titration Curve and Messages2.3.4.5.6.7.8.Increase in the types of endpoint detectionAnti-diffusion structure on titration nozzle of buretteGLP/GMP fully conformingData storing / recalling with PC cardKF (volumetric) moisture titration unit as an optionCOD titration unit as an optionPrinting on A4/Letter size paper as an option4


<strong>AT</strong>-<strong>500N</strong> Automatic Potentiometric TitratorFeatures1.2.3.4.5.6.7.8.9.<strong>Low</strong> cost but <strong>High</strong> performanceEasy-to-read LCD with a backlightAnti-diffusion titration nozzle tipSafety cover to protect buretteSelection of one or two burettesGLP/GMP fully conformingCE-marking level of safety and noise immunityEasy-to-enter colored key padThree (3) interface ports : Balance, PC and PrinterConfiguration of Function KeysExample of printoutAPBAPBUp keyEnter Purge mode of burette or dose volumeDeliver TitrantKey to enter sample number, lot numberand sample size in weightPrintStirrerMethodDown keyPurge keyPrint keyStirrer keyMethod keyFill Titrant and exchange burette unitPurge TitrantPrint outTurn on/off stirrer and select stirring speedPush this key for two seconds, and the display showssetting stirring speed.Set MethodsParameters can be set with this key.Functions include:0.Method File1.Data File2.Sample File3.Changer4.Re-Titr.5.Check Titr.6.Set Check7.Periodic8.Buret Check9.Auto Start10.Auto Statis.11.Common Blank12.pH Cal.Table13.Card Utility14.Memory ClearTitrationTitration keySet titration parametersTime and date can be set with this key.Setup items include:ControlResultSampleFunctionControl keyResult keySample keyFunction keySet control parametersSet calculation or print formatSet parameters on a sample including thenumber of sample, sample size, etc.Set up functions as below:0. Method Copy 3. Changer File 6. Memory Clear1. Data File 4. Set Check2. Sample File 5. Periodic Check0.Interface1.Date&Time2.Regist Operator3.Serial/Version No.4.LCD Contrast5.Language6.Lock7.Beep8.pH PolarityKey to return to the main screendisplay (standby state)Key to switch displays or key functionsand also used for auto input of samplesize measured by an electronic balance5


Features of KEM titrators1. An endpoint can be detected precisely.A precise endpoint, which is the most important targetin titration, can be obtained from two detecting factorsof dE (endpoint detecting potential) and dE/dmL (Maxdifferential potential) without taking undesirable noisefor endpoints.350.0mVPotentialDifferential-100.00.0000 mL 13.00002. The endpoint whether single ormultiple can be clearly indicatedand separated in titration.For example, Level Stop modecan determine the detectedsingle endpoint as EP2.350.0mV-100.00.0000 mL 13.0000350.0LevelmV-100.07.0000 mL 12.00003. EP detection range can be set.User can define titration volume and potential range,most useful in measurement under the influence ofnoise and carbon dioxide.14.00pH0.000.0000 mL 12.00004. Delivery speed in titration can be automatically controlled.Where titration potential change (differential) is smaller, the speed increases; while itbecomes larger, the speed slows down automatically. Optimal control method in chemicalreaction comes from the related combination of delivery speed and control speed : C.S.Delivery speeds/mL2100200300400500C.S.=0.5 (Slow)C.S.=4 (Fast)C.S.=2 (Medium)Fast : Control Speed (4.0)Medium : Control Speed (2.0)Slow : Control Speed (0.5)0 100 200 300 400 500 600Differential6


EP detection formsVarious detection forms can be selected suitable for users’ titration needs.320.0Full EP stop Level Stop350.0380.0mVmVmV-80.04.0000 mL 12.0000Titration will last to the presetvolume and finds endpoints. Thisis useful for a sample of whichendpoint number is unknown.Up to 3 EPs can be detected by<strong>AT</strong>-<strong>500N</strong> and 5 EPs by <strong>AT</strong>-<strong>510</strong>.-100.00.0000 mL 13.0000Titration will last until it findspreset number of endpoints definedby user on control parametersetup.Up to 3 EPs can be detected by<strong>AT</strong>-<strong>500N</strong> and 5 EPs by <strong>AT</strong>-<strong>510</strong>.-130.00.0000 mL 12.8393Titration will last up to the presetpotential level (up to 2 levels) beforestopping.12.00Auto Intersect12000Auto IntersectpH2.002.5000 mL 7.0000Two-tangent lines crossing pointis determined as the endpoint,which is adopted in photometrictitration or the like.00.0000 mL 7.4302Two-tangent lines crossing pointis determined as the endpoint,which is adopted in conductometrictitration or the like.pH Stat14.00 5.000012.00pKapHmLpH0.00 0.00000:00:00 0:30:00Reagent is dosed to maintain controlpotential in Stat titration, andtitration volume will be displayedat given interval.0.000.0000 mL 8.5000A pKa value can be determinedby finding pH at the half of titrationvolume in neutralization titration.7


Applications of Automatic TitratorsType of Industry Object of Analysis Titration Types Titrant Electrode / PreamplifierPetroleumTotal acid number of petroleum productsTotal base number of petroleum productsChlorideBromine NumberMercaptanDetermination of IodineAcid-Bass TitrationPrecipitation TitrationPolarization TitrationPrecipitation TitrationOxdation-Reduction TitrationKOHHCIO4 / HCIAgNO3NBr, KBrO3AgNO3Na2S2O398100H171&98100R172or 98100C17398100C37398100M511 or 98100M512 / POT-<strong>510</strong>98100M214&98100H17198100C272Determination of Sodium acetateHCIO498100H171&98100R172Acid-Base TitrationMedicineDetermination of Benzethonium chlorideNa(B(C6H5)4) or 98100C171FoodsCa and Mg in Dialysis solutionChloride in pharmaceutical productsAcid value of beveragesSalts in seasoning/dressingVitamin CChelatometric TitrationPrecipitation TitrationAcid-Base TitrationPrecipitation TitrationOxdation-Reduction TitrationEDTAAgNO3NaOHAgNO3indophenolPhoto Sensor / PTA-<strong>510</strong>98100C37398100C17198100C37398100C272Electronic PowerBoric acid concentration in nuclear power plantNaOH98100H171&98100R172Acid-Base TitrationTotal Acid Number of insulating oilsKOHor 98100C172Acid ValueAcid-Base TitrationKOH98100C173Peroxide ValueOxdation-Reduction Titration Na2S2O398100C272Fats and OilsSaponification valueHCIAcid-Base Titration98100C173Hydroxy ValueKOHElectronic andMetal Plating Solution NiMetal Plating Solution CuFree cyanide concentrationChelatometric TitrationPrecipitation TitrationEDTAAgNO3Photo Sensor / PTA-<strong>510</strong>98100C373Metal PlantingBoric acid in plating bathsEtching Solution H2SO4Chromic acid in chrome plating bathTotal hardnessAcid-Base TitrationOxdation-Reduction TitrationChelatometric TitrationNaOHNa2S2O3EDTA98100C17198100C272Photo Sensor / PTA-<strong>510</strong>City water/Industrial waterChlorideAlkalinityPrecipitation TitrationAcid-Base TitrationAgNO3H2SO498100C37398100C171DetergentsAnionic SurfactantsHyamineColloid TitrationCationic SurfactantsSDS98100S173Determination of IsocyanateMonomer residues in polyethyleneAcid-Base TitrationOxdation-Reduction TitrationHCINa2S2O398100C17398100C272Chemicals Carboxyl group in PET resinKOH98100C173Iron and steel/CeramicsSodium hydroxidePurity of acrylic acidFerric iron in hydrochloric acidFluoric acid and nitric acid in pickling solutionTrace chlorine in cementsAluminum oxides in cementsAcid-Base TitrationOxdation-Reduction TitrationAcid-Base TitrationPrecipitation TitrationChelatometric TitrationHCIKOHNa2S2O3NaOHAgNO3EDTA98100C17198100C17398100C27298100C17198100I271&98100R272Photo Sensor / PTA-<strong>510</strong>8


SpecificationsType and ModelTitration modeMethodType of titrationTitration formPreamplifiersDisplayDisplayed contentsExternal input/outputPrinter connectionData storageGLP/GMP conformityStructureBurettesSteps for a full strokeBurette precisionSwitching for discharge or suctionLiquid contacting materialsAmbient conditionsPower/ConsumptionDimensionWeightStandard accessories<strong>AT</strong>-<strong>510</strong> Automatic Potentiometric TitratorBlank, Auto control, Auto cut off,Continuous/Intermittent constant rate, PetroleumProducts neutralization number, KF titrationcontrol, COD titration controlSTD:7, User:38, Combined:5; Total 50Acid-base, Redox, Photometric, Polarization,Combined, pH stat, pKa, Learning, KF moistureand COD titrationAuto: Max inflection point, Level stop, IntersectionManual: EP stop, IntersectionSTD-<strong>510</strong>, (Option:TET-<strong>510</strong>, PTA-<strong>510</strong>, POT-<strong>510</strong>, CMT-<strong>510</strong>)LCD with back light, 126 x 70 mm, 30 digits by 13 linesTitration curves, Titration parameters (titer, potential,temperature, etc.), Messages, etc.RS-232C, Electronic balance, Ext. printer, <strong>Multi</strong>ple sample changerStandard accessory: Impact dot printer (Ink-ribbon Options: Impact dot printer (Ink-ribbon style), IDP-100style), IDP-100Options: A4/letter-size printersInternal: 100 samplesInternal: 100 samplesExternal: 100 samples per PC cardCalibration history for electrodes, Setting of periodic Setting of periodic inspection interval, Inspectioninspection interval, Checking of burette precision, history for titration performance (one point),Alarm for replacing electrodes, Alarm for shortage of File for operator's name (one person)titrants, Inspection history for titration performance(one point), File for operator's name (up to 10)Integrated construction of main unit and burette, Stirrer(984300018A) with a built-in preamplifierOne built-in APB-<strong>510</strong> andup to 9 external APB-<strong>510</strong> connectableBurette capacity: 20mLOptional burettes (mL): 1, 5, 10, 5020,000 steps50mL burette ±0.05mL, Repeatability20mL burette ±0.02mL, Repeatability10mL burette ±0.015mL, Repeatability5mL burette ±0.01mL, Repeatability1mL burette ±0.005mL, RepeatabilityApprox. 10kgInstruction Manual 1Rotor for stirrer(25mm) 985003141 1Piston removing stick 985515002 1Combined glass electrode 98100C171 1Temperature comp. electrode 98100T111 1Impact dot printer IDP-100 1Electrode cable 984290012 1<strong>AT</strong>-<strong>500N</strong> Automatic Potentiometric TitratorBlank, Auto control, Auto cut off,Continuous/Intermittent constant rateSTD:4, User:16; Total 20Acid-base, Redox, Photometric and PolarizationtitrationAuto: Max inflection point(Full or EP stop titration),Level stopSTD-<strong>510</strong>, (Option:PTA-<strong>510</strong>, POT-<strong>510</strong>)LCD with back light, 16 digits by 2 linesTitration parameters (titer, potential, temperature, etc.),Messages, etc.One built-in APB-<strong>510</strong> (<strong>AT</strong>-<strong>500N</strong>-1) ortwo built-in APB-<strong>510</strong> (<strong>AT</strong>-<strong>500N</strong>-2)Burette capacity: 20mLOptional burettes (mL): 1, 5, 10, 5020,000 steps±0.02mL±0.01mL±0.005mL±0.003mL±0.001mLAutomatic with ceramic cockPTFE, glass and ceramicsTemperature: 5 to 35°C; Humidity: less than 85%RH (No condensing)AC100-240 V, 50/60 Hz; approx. 30WMain unit: 288(W) x 468(D) x 481(H) mm; Stirrer unit: 118(W) x 225(D) x 336(H) mmInstruction Manual 1Rotor for stirrer(25mm) 985003141 1Piston removing stick 985515002 1Combined glass electrode 98100C171 1Temperature comp. electrode 98100T111 1Electrode cable 984290012 19


System ConfigurationTemperature compensation sensor984300054SOFT-CAPE984300036Propeller stirrerAPB-<strong>510</strong>Automatic pistonburetteMS-<strong>510</strong>Magnetic stirrerKF-<strong>510</strong>Karl Fischertitration unitStandard systemCHA-500<strong>Multi</strong>ple SampleChangerMW-<strong>510</strong>Manual washing unitAPB-<strong>510</strong>Automaticpistonburetteconnectingcable980305030COD-<strong>510</strong>COD titration unitMagnetic stirrer984300018Aconnecting cable980305030APB-<strong>510</strong>Automaticpistonburetteconnectingcable980305030MS-<strong>510</strong>Magnetic stirrerMS-<strong>510</strong>Magnetic stirrerBurette UnitsAPB-<strong>510</strong>-01B (1mL)APB-<strong>510</strong>-05B (5mL)APB-<strong>510</strong>-10B (10mL)APB-<strong>510</strong>-20B (20mL) StandardAPB-<strong>510</strong>-50B (50mL)MTA-118Microtitration cell unitSealed cell unitSCU-118PreamplifierM o d e lApplicationEquipped asDetected propertiesDetection rangeRemarks123123STD-<strong>510</strong> POT-<strong>510</strong> PTA-<strong>510</strong> CMT-<strong>510</strong> TET-<strong>510</strong>Potentiometric Polarization Photometric Conductometric 3-way titrationAcid-base titrationRedox titrationPrecipitation titrationNon-aqueous titrationPotentiometric titration at constant currentAmperometric titration at constant voltageAcid-base titrationRedox titrationNon-aqueous titrationChelate titrationAcid-base titrationRedox titrationPrecipitation titrationNon-aqueous titrationConductometric titrationAcid-base titrationRedox titrationPrecipitation titrationNon-aqueous titrationAcid-base titrationRedox titrationPrecipitation titrationNon-aqueous titrationStandard Option Option Option OptionpH pH pH pH pHmV mV mV mV mVPolar Potential/Current Transmittance Conductivity pH0 14pH 0 14pH 0 14pH 0 14pH 0 14pH2000mV2000mV 2000mV 2000mV 2000mV0 2000mV0 100 <strong>AT</strong>win Pt. electrodenot included0 120%TPhoto sensor (530nm)included0 100 S0 1000 S0 10000 SConductivity sensor includedExclusive for <strong>AT</strong>-<strong>510</strong>0 14pHExclusive for <strong>AT</strong>-<strong>510</strong>10


Options for <strong>AT</strong>-<strong>510</strong> and <strong>AT</strong>-500-1,2Automatic Piston BuretteAPB-<strong>510</strong>Features:Titration nozzle of burette is made of PTFE and twokinds of nozzle, anti-diffusion type and normal type, aregiven as standard accessories.Safety cover to protect glass burette.Easy replacement of valve with newly designed flowcontrollvalve for titrants.Specifications:Type and modelDisplayBurette capacityReagent bottlePower sourcePower consumptionDimensionWeightAPB-<strong>510</strong>, Automatic Piston BuretteLCD , capable six digits display1)20mL glass burette (standard)2)Unit with 50/10/5/1mL glass burette (option)1000mL brown glass bottle1) AC100~120 V or AC200~240 V2) 50/60 Hz20W120(W) x 365(D) x 450(H) mmApprox. 5kg<strong>Multi</strong>ple Sample ChangerCHA-500-12/CHA-500-18Features:Can select washing sequences for electrodes suitable for titration applications:1.Acid-base titration2.Precipitation titration3.Standard non-aqueous titration4.Neutralization number titration on petroleum productsOptional Power Shut-off Unit POU-310 can be connected with CHA-500.Specifications:Type and modelNumber of samplesSample vesselsRinsing methodRinsing solutionDrain capabilitiesDosing of pretreatmentsolutionCHA-500 <strong>Multi</strong>ple Sample Changer12 or 18 samplesStandard: 200mL beaker or 300mL tall beakerOptional: 50, 100mL beaker or 200mL Erlenmeyer flaskStandard: Shower (equipped with rinse pot)Optional: Dip; Dip plus showerStandard: Pure water; Ethanol or IPA (Isopropanol)Optional: Organic solvents such as toluene; Aqueous acid/alkali solutionStandard: Natural falling drain from rinsing potOptional: Mixing/Separating drain by drain pumpStandard: N/AOptional: APB-<strong>510</strong> or filling pump can be connected to CHA-500.Data Capture Software SOFT-CAPE Combination Surfactant Electrode 98100S173 Stream Potential Titration Unit PCD-500SOFT-CAPE the Data Capture Softwarefor <strong>AT</strong>-<strong>510</strong>/<strong>AT</strong>-<strong>500N</strong> Automatic titratorsData Capture Software can control Automatictitrators.Measurement results of Automatic titratorscan be downloaded directly to workbook inMicrosoft® Excel or filed in CSV format,such as Lotus1-2-3.Microsoft® Excel must be installed on theconnected personal computer.Surfactants used to be determine by the Epton'smethod with the toxic solvent of Chloroform,but with this electrode one can measure theconcentration of cationic or anionic surfactantsquickly without Chloroform.Main specificationsItemConcentration rangepH rangeTemperature rangeSpecifications1x10 -2 M 1x10 -5 MpH2 120 50 CTitration instrument for measuring on surfactantsand polymer coagulants.A number of samples can be automaticallymeasured using the <strong>Multi</strong>ple Sample Changer.Main specifications (not CE conformed)ItemSpecificationsMeasured objectsMeasuring rangeSurfactants, polymer coagulants and the colloid solutionwith dispersing charged particles in Food industry1x10 -5 M or moreOutput power -2 to +2 VDCPower source 100 to 240 VAC, 10W11


Options for <strong>AT</strong>-<strong>510</strong> and <strong>AT</strong>-<strong>500N</strong>-1,2Micro Titration AssemblyMTA-118Sealed Cell Flask Assembly SCU-118 Propeller stirrer 984300036This assembly is useful for measuring traceamount of samples by titration.The structure features the sealed jacket ofthermostatic bath.Type Cell shapeMTA-118-1 TubeMTA-118-5 ConeMTA-118-50 ConeMin. sample vol. Max. sample vol.1mL 2.5mL5mL 35mL25mL 100mLThis flask assembly with an electrode supportingholder is designed for samples that cannot bemeasured under normal ambient conditions.Titration can be performed with minimalinfluence of atmosphere by purging the inside ofthe flask with Nitrogen gas or filling thedesiccant tube with Soda lime or the like.Capacity of titration cellMinimum sample required200mLAt least 50mLThis unit features stirring titrated samplesolution with rotating propeller at the tip of amotoring rod as the substitute for a magneticstirrer. (Exclusive for <strong>AT</strong>-<strong>510</strong> and <strong>AT</strong>-<strong>500N</strong>)PC CardOptions Exclusive for <strong>AT</strong>-<strong>510</strong>The following three types of PC cards are available:1.Memory card (984340039)Can store, read and write measurement methods, titrationconditions and other parameters. Further, can performrecalculation or statistical calculations by recallingmeasured data.2.Application card (984340173)Can use 70 various measurement conditions (parametersfor such as titration, control or calculation) prepared by us.3.pH temperature compensation card (984340175)Can make temperature compensation on pH, based oninternational standards, with pH temperature compensationtables of ASTM, DIN, BS, NF and JIS.PC Card Read SoftwareSOFT-PCREFeatures:1.Can store all data in PC card for backed up on a personalcomputer. In reverse, data stored in personal computercan be transferred to Memory card, meaning that instrumentcan be easily recovered.2.Measurement results can be directly captured toMicrosoft Excel workbook.3.Measured data can be directly stored as files in CSV format.This CSV file is compatible with Microsoft ® Excelspreadsheet software package.4.Personal computer can separately store and managemeasured data, measurement conditions or sample conditionsstored in Memory card. In addition, data stored in personalcomputer can be transferred to Memory card.KF titration unit KF-<strong>510</strong> COD titration unit COD-<strong>510</strong>KF titration unit KF-<strong>510</strong>With this unit and the Karl Fischer reagents, onecan measure water in samples.COD titration unit COD-<strong>510</strong>This unit is used for the titration with Potassiumpermanganate in the last step of COD measurement.12


<strong>Multi</strong>-Channel software perfectlysupporting titrationSoftware for TitratorsCan run four measurements simultaneously and concurrently.Can display four titration curves simultaneously.<strong>AT</strong>-<strong>510</strong><strong>AT</strong>-<strong>500N</strong>-1<strong>AT</strong>-<strong>500N</strong>-2Examples of connection of <strong>AT</strong>-<strong>510</strong>/<strong>AT</strong>-<strong>500N</strong> Automatic Potentiometric TitratorsFeatures1. Auto settings of measurement conditions with the Navigating feature:Just by entering user’s intended main criteria including internationalstandard (e.g. JIS, ASTM, ISO), sample type, measured object andmeasuring range, the complete titration conditions can be set upautomatically. Additional powerful help by the Wizard enhancessetting up measurement conditions through dialogue interactions.2. Operational procedures displaying feature:Simply select what you want to do-- the necessary procedures for user’sdesired measurement will be displayed sequentially prompting the entrystep by step, allowing operators to avoid unintended or ignorant entry ofnumerical constants such as sample size and the like.3. IT Support:Details of <strong>AT</strong>-Win can be viewed at http://www.kem.jp/itsupport/,where the user can see and download data files on measurementconditions plus the up-to-date information on titration technique.13


Features4. GLP/GMP fully conforming:Electrode and sensorBurette validationCheck with standard substanceOthersNotice of periodic calibration dateDisplay of electrode calibration recordsNotice of periodic check dateDisplay of burette validation recordNotice of piston head replacement dateNotice of periodic check dateDisplay of check recordsOperational level authentication by userDisplay of operational recordsAlarm for remaining reagent volume5.Operational management with security measures:User ID and password security support operational management allowingsolely managerial person to change parameters in order to avoid illegal orunauthorized alteration of measurement conditions or the like.Create, edit, copy or delete titration conditions of Methods.GLP/GMP requirements including electrode calibration and burette validation.Analysis of measurement data like re-calculation or re-detection of endpoints.6. Standard-equipped Viewer linked to Network:Not only measurement results can be viewed, but also the simulationof measurements, recalculation or analysis can be manipulated byother computers installed with Viewer via LAN linked. Of course,the user can create report and print it out with the Microsoft Word.The Viewer can be installed on plural personal computers.7. Creating Report:Since titration data are now converted to CSV format, they can bemanipulated in other application software like Microsoft ® Excelspread sheet or Microsoft Access database software on the word-processingMicrosoft Word.Therefore, the user can create Report easily and faster than before in one'soriginal form, for example, using Microsoft Word's auto function, makinguse of its template and macro.8. Barcode reader:Sample ID or lot number can be easily input with a barcode reader sold onthe market connectable to the keyboard of user’s personal computer.14


System ConfigurationStandard componentsTitration software<strong>AT</strong>-WinKEMKey CodeWhen purchasing <strong>AT</strong>-Win/2nd software, you needRS-232C EXT. Board (984040008).CH1Key Code CardCH2CH3CH4CH5CH6CH7CH8CH9Connecting cable (2m)980300002Printer<strong>AT</strong>-Win/2nd(Add-on Set)KEMKey CodeConnecting cable (2m)980300002Key Code Card<strong>AT</strong>-<strong>510</strong>Automatic Potentiometric Titrator<strong>AT</strong>-<strong>510</strong>Automatic Potentiometric Titrator<strong>AT</strong>-<strong>500N</strong>Automatic Potentiometric TitratorAPB-<strong>510</strong>Automatic Piston BuretteAPB-<strong>510</strong>Automatic Piston Burette(Max 9 connectable)MS-<strong>510</strong>Magnetic StirrerAPB-<strong>510</strong>Automatic Piston BuretteAPB-<strong>510</strong>Automatic Piston Burette(Max 9 connectable)MS-<strong>510</strong>Magnetic Stirrer980305030connecting cable980303388connecting cableCHA-500<strong>Multi</strong>ple Sample ChangerAPB-<strong>510</strong>Automatic Piston Burette980300013connecting cableCHA-500<strong>Multi</strong>ple Sample ChangerAPB-<strong>510</strong>Automatic Piston Burette15


SpecificationsStandard components:Name of softwareCompatible modelMedia<strong>AT</strong>-WinBase set<strong>AT</strong>-<strong>510</strong>/<strong>AT</strong>-<strong>500N</strong>CD-ROM 1 pc.<strong>AT</strong>-Win/2ndAdd-on set<strong>AT</strong>-<strong>510</strong>/<strong>AT</strong>-<strong>500N</strong>NoConnecting cableConnecting cable(2m)980300002 1Connecting cable(2m)980300002 1Key Code Card1* 1*Operation manual1 copy No* For the purchase of a Key Code Card, the serial number of user's unit is required. This serial number must be notified by the user whenused in combination with the unit already in use.System requirements:DeviceDescriptionPersonal computer with CPU of 500MHz or betterComputer* Intel Pentium/Celeron family, AMD K6-2/Athlon/Duron family orIntel compatible CPU’sOperating system Windows 98SE/Me/2000/NT4.0(SP5 or later)/XPOther programsMicrosoft Internet Explorer (Version 5.01 or later)Adobe Acrobat Reader (Version 4.0 or later)RAM128MB or moreFree hard disk space 50MB or more free disk spaceDisplayResolution of 1024x768 or betterDisk driveCD-ROM or DVD-ROMSerial portRS-232C D-sub (male) 9 pin or USB port: 1 port *2*2 1) Each titrator has to have an extra serial port. Likewise, when a balance or barcode is connected to a PC, a separate serial port will berequired in the computer accordingly.2) With the optional RS-232C expanded serial port, up to four (4) titrators can be linked through the interface. Note, however, that atleast one slot must be free on PCI bus. Additionally, <strong>Low</strong> Profile type of PCI bus may not be compatible.3) If a PC has a built-in modem, one serial port may be already assigned.Options:RS-232C EXT. BoardExtension cable(For <strong>AT</strong>-<strong>510</strong>/<strong>AT</strong>-<strong>500N</strong>)Extension cable(For <strong>AT</strong>-420N)984040008 RS-232C expanded serial port (8ch, converting cable included)980080003980080004980305289983500005983500006Connecting cable set (120 VAC) 10mConnecting cable set (230 VAC) 10mTCU cable (10m)Optical cable (30m)Optical cable (50m)980305287 TCU cable (1m)980305288 TCU cable (5m)980305289 TCU cable (10m)983500005 Optical cable (30m)983500006 Optical cable (50m)16


FDA 21 CFR Part 11 Compliant SoftwareSecurity<strong>AT</strong>-Win/ER Titration Software featuring Electronic Records andSignatures compliant with FDA 21 CFR Part 11, inheritingproven user-friendly and competent features of <strong>AT</strong>-WinSoftware for titrators.IntegrityAudit TrailElectronic SignaturesSoftware specifications:Name of softwareFDA 21CFR Part 11compliant featuresItemGLP/GMP compliant featuresNetwork linkCompatible modelsUser authenticationElectronic signaturesData integrityAudit trailBackup functionDescription<strong>AT</strong>-Win/ER, FDA 21 CFR Part 11 Compliant SoftwareLogin ID and Password securityUser name and title registrationGroup management for up to 11 user groupsPassword valid periodDetection of illegal access and lockout (access number counting andits time length)Signatures according to users’ authenticationVerified data is stored in database with commentsAuto recording raw data and meta data in databaseAuto recording measurement parameters and results(Database:compatible with the Microsoft SQL Server/MSDE, Oracle)Can see stored and compressed data with ViewerRecord created or changed Methods with commentsAuto recording of results and re-evaluated data with allchanges noted.Search the recorded dataDirect backup recording in CD-R or other deviceBackup data can be viewed directly.Electrode calibration/Check with standard substances/Validation ofburette dosing volumeNotify Periodic calibration/check/validation (by setting date or its interval)Auto recording of the results of calibration/check/validation in databaseInterface to the Shimadzu CLASS-Agent System<strong>AT</strong>-<strong>510</strong> and <strong>AT</strong>-<strong>500N</strong>* “Windows, Internet Explorer, MSDE and SQL Server”, “Oracle”, “Acrobat” and “CLASS-Agent” are registered trademarks of Microsoft,Oracle, Adobe Systems and Shimadzu Ltd., respectively.Standard components:Name of softwareMediaConnecting cableKey Code CardOperation manualTitration softwareDatabase controlling software<strong>AT</strong>-Win/ERBase setCD-ROM 1 pc.CD-ROM 1 pc.980300002 1piece1*One copy<strong>AT</strong>-Win/2ndAdd-on setNoNo980300002 1piece1*No* For the issue of a Key Code Card, report of the serial number on a user’s <strong>AT</strong> unit is a must. When this software is used with the formerlydelivered <strong>AT</strong> units, be sure to let us know the serial numbers of the concerned <strong>AT</strong>’s.Note: Hardware validation is required for user’s computers on which this software is installed. For more details, please contact our localsales representatives in your country.17


Features1. Electronic signatures with ID and Password securityUser authentication is secured by login/logout with ID andpassword. The password length and validity period can beprecisely set for each user. Illegal access is prevented bylockout system which records the attempt.2. User group registrationUp to 11 separate user groups can be registered, each withits own password entry and individual level of access.3. Audit trailThe required audit trail feature is fully compliant byrecording data both before and after the change, which istraceable by the function of log file self-generation.4. Secured data integrityDatabase management of user information (name, title,e-mail address, etc.) can be secured at higher level bylinking the access-controlled database such as MicrosoftSQL Server/MSDE or Oracle.5. Electronic records and signaturesData such as measurement results or conditions, electrodecalibration or check with standard substances areautomatically recorded onto the database, which can beelectronically signed according to an approved workflow.6. Network compatibilityThe network-interfacing feature, also compatible with theLAN on Client/Server system, allows the users to controltheir login records. In addition, the feature includesthe interface to the Shimadzu LC/GC Network.Titration result7. Backup systemThe backup copies of data and log records together withthe reasons can be made on commercial media such asCD-R using a CD-R/RW drive and a CD writing software.Database18


System ConfigurationLC/GC,etc.Ethernet LAN (Labo)DatabaseWhen used as stand alone PC,the database should be installedon a local PC.DatabaseStandard componentsServer PCWhen purchasing <strong>AT</strong>-Win/2nd software, you needRS-232C EXT. Board (984040008).CH1Client PCEthernet LAN (Office)Client PCFDA21CFR Part11Compliant softwareKEMKey CodeKey Code CardCH2CH3CH4CH5CH6CH7CH8CH9DatabasemanagementsoftwareCLASS-AgentConnecting cable (2m)980300002<strong>AT</strong>-Win/2nd(Add-on Set)KEMKey CodePrinterConnecting cable (2m)980300002Key Code Card<strong>AT</strong>-<strong>510</strong>Automatic Potentiometric Titrator<strong>AT</strong>-<strong>510</strong>Automatic Potentiometric Titrator<strong>AT</strong>-<strong>500N</strong>Automatic Potentiometric TitratorAPB-<strong>510</strong>Automatic Piston BuretteAPB-<strong>510</strong>Automatic Piston Burette(Max 9 connectable)MS-<strong>510</strong>Magnetic StirrerAPB-<strong>510</strong>Automatic Piston BuretteAPB-<strong>510</strong>Automatic Piston Burette(Max 9 connectable)MS-<strong>510</strong>Magnetic Stirrer980305030connecting cable980303388connecting cableCHA-500<strong>Multi</strong>ple Sample ChangerAPB-<strong>510</strong>Automatic Piston Burette980300013connecting cableCHA-500<strong>Multi</strong>ple Sample ChangerAPB-<strong>510</strong>Automatic Piston BuretteDistributed by :KYOTO ELECTRONICSMANUFACTURING CO.,LTD.Overseas Division : 8-3 Niban-cho Chiyoda-ku TOKYO 102-0084,JAPANFax : +81-3-3237-0537, Phone : +81-3-3239-7333URL : http://www.kyoto-kem.comSpecifications and design subject to change for improvements without notice. Printed in Japan.58IK33C

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