Luise Strange de Soria

Luise Strange de SoriaLuise Strange de Soria'sChem-2641 Laboratory Survival GuideCHEM-2641 EXPERMENT #1 Handout developed by Luise Strange de Soria to accompany Mayo, Pike,and Trumper laboratory manualName:Lab Partner:There are four things you should complete before leaving the laboratory today. The following is a tablewhich has boxes which will be initialed by your instructor once you have completed each part of theassignment. You may turn this page in as part of your data section for your lab report. Your report shouldinclude the percent error for the melting point & boiling point, as well as your own drawings of the refluxand distillation apparati.Task # Description Temperature Reading (whenapplicable)1 Take a melting point of solid #2 Take an ultra micro boiling point of liquid #(Click here to see a description of how to make a bell)3 Build an apparatus (using your three mL conical vial) for completing a distillation4 Build an apparatus (using your five mL conical vial) for completing a refluxDiagram of a Reflux Apparatus SetupDiagram of a Distillation Apparatus Setupfile:///H|/2641lab/survivalguide/phys.htm (1 of 2) [9/1/2004 9:20:35 AM]

Luise Strange de SoriaClick here to view a Sample Lab report (many thanks to Edward Parkin) for Determinationof PhysicalProperties which describes how to take a melting point and an ultramicroboiling point(Note: the page numbers mentioned in Edward's report are from an older edition of the labtextbook!).file:///H|/2641lab/survivalguide/phys.htm (2 of 2) [9/1/2004 9:20:35 AM]