KURNOOL (AP) - Rayalaseema University
KURNOOL (AP) - Rayalaseema University
KURNOOL (AP) - Rayalaseema University
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RAYALASEEMA UNIVERSITY:: <strong>KURNOOL</strong> (A.P.)M.Phil., / Ph.D., Written Examination SyllabusSub: CHEMISRYPaper –I Research MethodologyCH<strong>AP</strong>TER – 1: RESEARCH METHODOLOGY:Research Methodology:Choice of the research problem, collection of literature (Primary ad secondary sources). Basicelements of writing a scientific paper and basic principles and techniques to be adopted in thepreparation of M.Phil., dissertation or Ph.D., thesis.CH<strong>AP</strong>TER – 2: TREATMENTS OF QUANTTATIVE DATA:Errors in Chemical Analysis: Definition of terms; Systematic Errors;Random Errors in Analysis:The Nature of Random: The Statistical Treatment of Random Error; the Standard Deviation ofComputed Results; Methods for Reporting computed Data:Application of Statistics to Data Treatment and Evaluation;Confidence Limits; Statistical Aids to Hypothesis Testing; Detection of Gross Errors; Estimationof Detection limits; The Least – Squares Method for Deriving Calibration Plots; QualityAssurance and Control Charts. Significant figures.CH<strong>AP</strong>TER – 3: GAS CHROMATOGR<strong>AP</strong>HY:Instruments for Gas – Liquid Chromatography; Principles of gas chromatography; GasChromatography Columns and Stationary Phases; Application of Gas – Liquid Chromatography;Use of GCMS to identify a Drug Metabolite in Blood, High – Speed Gas Chromatography; Gas– Solid Chromatography.High – Performance Liquid Chromatography:Instrumentation; Liquid Chromatography (LC) Mass Spectrometry (MS) and LC/MS/NS; High –performance partition Chromatography; High – performance Adsorption Chromatography; Ion –Exchange Chromatography; Size – Exclusion Chromatography, Buckyballs: TheChromatographic, Separation of Fullerenes: Affinity Chromatography; Chiral Chromatography;Comparison of High – Performance Liquid Chromatography and Gas Chromatography.CH<strong>AP</strong>TER – 4: INFRARED AND RAMA SPECTROSCOPY:Theory of infra red absorption and Raman Spectroscopy, sample handling instrumentation (BasicComponents) qualitative and quantitative applications. The vibration – Rotation Spectrum ofCarbon Monoxide; Breakdown of the Born – Oppenheimer Approximation; The Interaction ofRotations and Vibrations; The Vibrations of Polyatomic Molecules; The influence of Rotation onthe spectra of polyatomic Molecules; Analysis by Infra- red Techniques; Techniques andinstrumentation; Vibrational Raman Spectra; Polarization of Light and the Raman Effect;1
55PRESENÇA DE BACTÉRIAS DA FAMÍLIA Enterobacteriaceae NASSUPERFÍCIES EXTERNA E INTERNA DE Alphitobius diaperinus (PANZER)ORIUNDOS DE GRANJAS AVÍCOLAS DOS ESTADOS DO RIO GRANDE DOSUL E SANTA CATARINA__________________________porSTEFANIE DICKEL SEGABINAZIDissertação apresentada ao Curso de Mestradodo Programa de Pós-graduação em Medicina Veterinária,Área de Concentração em Medicina Veterinária Preventiva, daUniversidade Federal de Santa Maria (UFSM, RS),como requisito parcial para a obtenção do grau deMestre em Medicina VeterináriaPPGMVSanta Maria, RS, Brasil2004
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