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Appendix 7 - List of Participants at Local Quality Control & GLC Training Workshops at NEMD in Baku, Azerbaijan on 20th-21st FebruaryNo Name Position Attended training1. Ayubeniz Dushdurova Lab Monitoring Water AQC 20/2/13 & AQC Practical Training -21/2/32. Aliyeva Aytan - AQC 20/2/13 & AQC Practical Training 21/2/33. Pashayeva Resmiya - AQC 20/2/13 & AQC Practical Training 21/2/34. Madatiova Durdana Head Of Monitoring Lab On Atmosphere Precipitations AQC 20/2/13 & AQC Practical Training 21/2/35. Efendiyeva Roya Secondary Chemical Engineer AQC 20/2/13 & AQC Practical Training 21/2/36. Abdullayeva Ramina Head Of Monitoring Lab On Atmosphere Air Pollution AQC 20/2/13 & AQC Practical Training7. Aliyaeva Aytan Senior Chemical Engineer AQC 20/2/13 & AQC Practical Training 21/2/38. Ulker - AQC 20/2/139. Khalilova Aybeniz Head Of Monitoring Lab On Earth Pollution AQC 20/2/1310. Aliyeva Arzu Secondary Chemical Engineer AQC 20/2/1311. Quliyeva Sevda Secondary Chemical Engineer AQC 20/2/1312. Qasimova Ruhiyya Chemical Technique AQC 20/2/1313. Askerova Sabina Chemical Technique AQC 20/2/1314. Abulhasanova Natravan Senior Chemical Engineer AQC 20/2/1315. Latifova Shakhla Chemical Engineer AQC 20/2/1316. Allahverdiyeva Rena Senior Chemical Engineer AQC 20/2/1317. Gulkar Mammadova, Deputy Head of Laboratory AQC 20/2/13 & GLC 21/2/318. Allahverdiyeva Ragiba Secondary Chemical Engineer AQC 20/2/13 & GLC 21/2/1319. Guliyev Nizami Physical Engineer AQC 20/2/13 & GLC 21/2/1320. Mamammadova Sabina Head Of Spectrometric And Chromatography Lab AQC 20/2/13 & GLC 21/2/1321. Baghirova Gulnar Physical Engineer AQC 20/2/13 & GLC 21/2/1322. Mayilova Lala Chemical Technique AQC 20/2/13 & GLC 21/2/13KEs Mission ReportsHuman Dynamics KG ConsortiumPage 28 of 36
Appendix 8 - Main issues and recommendations for Improving the Organic Micro-pollutant Analysis at EIMC, Yerevan, ArmeniaSampling BottlesThe sampling bottles are too small, (160ml) ideally the bottles should be 2000ml amber glass with ground glass tops or caps with Teflon inserts. The reasonthese smaller bottles were used was because obtaining extraction solvents of pentane or hexane is very difficult for Armenia owing to importing problems.So it was thought that by using smaller bottles then less solvent would be required. Whilst this seems logical it must be noted that the extraction is also animportant concentrating technique. If the sample is too small then it creates a problem in being able to extract enough of the OPG from sample to be ableto detect it by GLC analysis. It is very unlikely that the current small samples with be sufficient to reach the required limit of detection (LOD).Extraction ProceduresThe extraction/concentration procedures could be a problemCurrently the liquid/liquid extractions are evaporated overnight at 60 degrees to dryness and then made up to 1ml. The extractions should not beevaporated to dryness there is a high chance that the organics will also evaporate and be lost. So the evaporation should be done to 1ml.Using this technique will also lose some of the VOCs and the aromatics. Ideally the purge and trap systems should be used – this is a GLC samplingaccessory. Also head space analysis may also be useful. Note one can use water samples and not need hexane could be useful to ArmeniaCalibration StandardsThere is one old standard for VOC (Mix of 23 parameters) which is out of date. No standard for the OCPs. Only 3 old standards for the aromatichydrocarbons. Therefore for the training new standards, are required.As there are no OCP standards available. The analyst has relied on previous calibrations obtained in 2006 by their predecessors. The only was to resolvethis, is to use fresh standards and prepare new acceptable calibration standards. It is recommended that the KE3 could train the staff to obtain suchcalibration graphs in following missions..KEs Mission ReportsHuman Dynamics KG ConsortiumPage 29 of 36
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