Syllabus - The Swami Ramanand Teerth Marathwada University

Subject code : MPY - 226
Subject : LABORATORY COURSE-4
Practical 8 hrs. /week (Minimum 12 practical should be conducted)
1. Synthesis of drugs mentioned in the theory using basic operations like
molecular distillation, fractional crystallization and purification by column
chromatography, preparative TLC and structural confirmation by
spectroscopic methods. (At least 4)
2. Isolation, characterization like melting point, mixed melting point, molecular
weight determination, functional group analysis co chromatographic
techniques for identification of isolated compounds and interpretation of
UV&IR data of following (Any 8)
a. Eugenol from Clove
b. Curcumin from Turmeric
c. Sennosides from Senna
d. Hesperidine from Orange peel
e. Embelin from embela Ribes
f. Glycyrrhizin from glycyrrhiza glabra
g. Plumbigin from Plumbago Rosea
h. Solarin from potato
i. Naringen from grape fruit peel
j. Trimystin and Myristin from Nutmeg
k. Azylic acid from Castor oil
l. Pectin from Orange peel
m. Lycopene from Tomato peel
n. Epicatechin from Cashew kernel, outer kernel
o. Piperin from Black pepper
REFERENCES
1. Mann and Saunders. Practical Organic Chemistry (orient Longman)
2. A. I. Vogel, Practical Qualitative and Quantitative Organic Chemistry
3. Modern methods of plant analysis – Peech and M. V. Tracey
4. Phytochemistry Vol I & II by Miller, Jan, Nostrant, Rein Hid
5. Recent advances in Phytochemistry Vol. I & IV – Scilicet, Runeckles
6. Natural Product Chemistry “A laboratory guide” by Rapheal Ikan