Microanaliza electronica XRF - Andreescu Labor & Soft

MICRO-Standards, Serie USThese standards are designed for quality assurance of microanalysis in metallurgy,geology, ceramic and building materials industry as well as for environmentalmonitoring. They are intended to serve as a reliable standard for parameter setting,peak identification and calibration of XRF-spectrometers in electron microanalysis.Each of the candidate materials was carefully selected to be matrix-true for mostfrequent analytical tasks. They consist of pure elements, low alloy- and stainlesssteels, pig irons and cast irons, non-ferrous alloys and different mineral basedmaterials.The individual reference materials are mounted in a brass disc or in a brass ring.They are fixed into 1.5mm diameter holes by a high vacuum proof cold setting resinsystem, diamond polished and carbon coated.The concentrations stated in the certificate are based on at least two independentlaboratory means, obtained by different analytical techniques or taken from thecertificate of the particular reference material used. The candidate materials werecarefully selected and tested for homogeneity. With those materials partlyheterogeneous by nature (marked in the table of available standards) the user isrecommended to find the essential parts prior to excitation.The values of element concentrations were achieved applying the ISO-REMCOGuide 35-1985 (E)l, thus the uncertainty of values, based on materialinhomogeneity, analytical imprecision and estimate of residual systematic error isexpressed by the last significant digit, according to the above cited document , i.e. thevalue 58.3 wt% means a concentration between 58.2 - 58.4 wt%.We offer to supply your individual MICRO-Standards for SEM:MICRO-Standard 'US 57' with up to 57different reference materials mounted ina brass disc of 25mm, 5mm thick,manufactured in sets of 30, 43 or 57 samplesorMICRO-Standard 'US 72' with up to 72different reference materials mounted inbrass ring of 45/25mm, 5mm thickSelect your individual MICRO-standards as per your choice from our down mentionedstock list of approx.180 selected samples to make up your individual standard.

List of available single standards for implementation into a US-MICRO-StandardNo. Reference material Symbol Element concentration %1 Kohlenstoff C C 99.92 Magnesium Mg Mg 99.93 Aluminium Al Al 99.94 Silizium Si Si 99.95 Titan Ti Ti 99.96 Vanadium V V 99.97 Chrom Cr Cr 99.98 Mangan Mn Mn 99.99 Eisen Fe Fe 99.910 Kobalt Co Co 99.911 Nickel Ni Ni 99.912 Kupfer Cu Cu 99.913 Zink Zn Zn 99.914 Gallium Ga Ga 99.915 Germanium Ge Ge 99.916 Selenium Se Se 99.917 Zirkonium Zr Zr 99.918 Niob Nb Nb 99.919 Molybdän Mo Mo 99.920 Silber Ag Ag 99.921 Cadmium Cd Cd 99.922 Antimon Sb Sb 99.923 Tellur Te Te 99.924 Hafnium Hf Hf 99.925 Tantal Ta Ta 99.926 Wolfram W W 99.927 Blei Pb Pb 99.928 Bismut Bi Bi 99.929 Kohlenstoffstahl OC 54 C 0.55S 0.010Mn 0.60Fe 9830 Kohlenstoffstahl OC 70 C 0.74S 0.016Mn 0.52Fe 9831 Kohlenstoffstahl OC 84 C 0.83S 0.015Mn 0.45Fe 98

No. Reference materialSymbol Element concentration %32 niedrig leg. Stahl 16270 C 0.66Si 0.21P 0.019S 0.011Cr 0.33Mn 0.43Ni 1.8Cu 0.05Fe 9633 Cr-Stahl 1Cr17 C 0.05Si 0.40S 0.016Cr 16.3Mn 0.42Ni 0.15Fe 8234 Kanthal 1Cr21Al7 C 0.03Al 6.9Si 0.57Cr 21.4Mn 0.30Ni 0.09Mo 0.03Fe 7035 Edelstahl 1Cr18Ni10Mo C 0.05Si 0.32S 0.018Cr 18.5Mn 0.91Ni 9.9Mo 2.3Fe 6736 Edelstahl 1Cr18Ni10 C 0.04Si 0.45S 0.016Cr 17.6Mn 1.11Ni 9.8Fe 7037 Edelstahl 1Cr23Ni14 C 0.05Si 0.46S 0.007Cr 23.5Mn 1.61Ni 13.7Fe 60

No. Reference materialSymbol Element concentration %38 Schnellarbeitsstahl 19857 C 0.96Si 0.25P 0.015S 0.022V 2.3Cr 4.1Mn 0.17Co 10.5Mo 0.03W 9.5Fe 7239 Werkzeugstahl 1920B C 1.40S 0.017V 5.7Cr 4.7Mn 0.35Co 5.0Mo 0.12W 14.3Fe 7040 Gußeisen * 425092 C 4.1Si 1.6P 0.24S 0.019Mn 1.3Fe 9241 Gußeisen * CKD 239 C 4.2Mn 0.76Si 0.27P 0.024S 0.018Cr 0.052Ni 2.42Cu 0.085Fe 9242 Roheisen * 417111 C 4.1Si 2.3P 0.18S 0.009Cr 0.05Mn 1.02Fe 9143 Roheisen * 106074 C 4.7S 0.024Mn 0.60Cr 0.18Fe 94

No. Reference materialSymbol Element concentration %44 Roheisen * 120032 C 4.3Si 0.48S 0.034Cr 0.14Mn 0.60Zn 0.02Fe 9445 Roheisen * 414022 C 4.5Si 1.05P 0.26S 0.018Mn 1.02Fe 9346 Eisenlegierung * FeBNd B 1.24Al 0.13Si 0.05Cr 0.03Mn 0.03Pr 0.3Nd 31.2Fe 6647 Ferrolegierung * FeAl C 0.03Mg 0.2Al 48Si 1.4Fe 4948 Ferrolegierung * FeSi Al 0.5Si 46Mn 0.4Fe 5350 Ferrolegierung * FeV Al 4.4Si 0.7V 79Fe 1651 Ferrolegierung * FeCr C 0.45Si 1.2Cr 68Fe 3052 Ferrolegierung * FeMn C 7.2Si 1.5P 1.2Mn 82Fe 953 Ferrolegierung * FeMo Fe 62Mo 3854 Titanlegierung BR Ti5 Al 6.8Ti 89Fe 0.08Mo 4.0

No. Reference materialSymbol Element concentration %55 Nickellegierung Ni90Cr10 Si 0.3Cr 9.5Mn 0.04Ni 8956 Konstantan Cu55Ni45 Mn 1.3Ni 43.5Cu 55.157 Sn-Bronze Cu63Zn37 Fe 0.05Ni 0.004Cu 63.7Zn 36.258 Al-Bronze Cu84Al12Fe4 Al 11.6Fe 3.7Cu 8459 P-Bronze Cu90P10 P 10.5Cu 8960 Bronze Cu94Sn6 Cu 94.6Zn 0.004Sn 5.361 Silberlot Ag58Cu28Zn14 Cu 27.9Zn 13.6Ag 58.462 Ag-Legierung Ag63Au37 Ag 63Au 3764 Galliumarsenid GaAs Ga 51.2As 48.865 Indiumphosphid InP In 80.3P 19.766 Indiumantimonid InSb In 48.5Sb 51.569 Wolframkarbid, gesintert * WC/TiC/Co C 9Co 6.2Ti 0.9W 7770 Wolframkarbid, gesintert * WC/Co C 6Co 8.8W 8571 Bornitrid p BN B 43.6N 56.472 Siliziumkarbid p SiC C 29.9Si 70.173 Titankarbid p TiC C 20.0Ti 80.074 Fluorid CaF 2 Ca 51F 49

No. Reference materialSymbol Element concentration %75 Jadeit NaAlSi 2 O 6 Na 10.9Al 15.5Si 23.8K 1.4Ca 1.3Fe 1.2O 4676 Albit NaAlSi 3 O 8 Na 9.4Al 10.1Si 31.9O 4877 Korund Al 2 O 3 Al 53O 4778 Topaz Al 2 SiO 4 Al 32.3Si 18.2O 4979 Orthoklas KAlSi 3 O 8 Na 0.9Al 9.6Si 31.6K 10.8O 4780 Pyrop Mg 3 Al 2 Si 3 O 12 Mg 11.7Al 11.3Si 18.7Ca 2.7Ti 0.4Cr 1.0Fe 9.2O 4481 Quarz SiO 2 Si 47O 5382 Wollastonit CaSiO 3 Si 24Ca 35O 4184 CaTi-Oxid s CaTiO 3 Ca 29.5Ti 35.2O 3585 Andradit Ca 3 Fe 2 Si 3 O 12 Mg 2.4Al 5.1Si 19.5Ca 20.5Fe 11.3O 4186 Rutil TiO 2 Ti 60O 4087 Olivin MgFeSiO 4 Mg 27.2Si 20.5Fe 8.5O 44

No. Reference materialSymbol Element concentration %88 Chromit FeCr 2 O 4 Mg 8.5Al 5.3Cr 39Fe 15O 3289 Hämatit s Fe 2 O 3 Fe 69.9O 3090 Magnetit Fe 3 O 4 Fe 72O 2691 Kuprit Cu 2 O Cu 89O 1192 Zirkon ZrSiO 4 Si 14Zr 52O 3493 Rhodochrosit MnCO 3 Mn 48O 42C 1094 Magnesit MgCO 3 Mg 26.4Si 2.9Ca 2.1O 54C 1495 Calcit CaCO 3 Ca 39O 48C 1296 Anhydrit CaSO 4 S 22Ca 32O 4697 Wolframit (Mn, Fe)WO 4 Mn 8.1Fe 10.5W 60O 2198 BaTi-Oxid s BaTiO 3 Ba 58.9Ti 20.5O 2099 KTa-Oxid s KTaO 3 K 14.5Ta 67.5O 18100 Pyrit FeS 2 S 53Fe 47101 Chalcopyrit CuFeS 2 Fe 30.3Cu 36.0S 33.7102 Sphalerit ZnS S 34Zn 66103 Antimonit Sb 2 S 3 S 27Sb 73

No. Reference materialSymbol Element concentration %104 Galenit PbS S 7Pb 93105 Glas GA-11 Na 1.6Al 9.5Si 20.6K 1.1Ca 0.7Mn 21.2Zn 4.0O 41106 Glas GB-2 Al 2.9Si 27.5K 0.3Ca 14.6Fe 9.8Ni 0.3Cu 1.0Zn 0.5O 43107 Glas SD-44 Na 6.4Mg 8.1Al 14.2Si 8.0P 2.3Ca 14.9Fe 0.3Zn 4.5Pb 1.8O 40108 Glas GSI-V Na 11.3Al 1.5Si 26.1K 1.8Ca 4.4Cr 2.2Mn 4.3Zn 3.2Ba 4.3O 41109 Glas FS-23 Al 0.9Si 32.9K 19.0Ca 2.9Ti 0.6O 44

No. Reference materialSymbol Element concentration %110 Hochofenschlacke VP Mg 7.7Al 3.8Si 19.6S 0.5K 0.6Ca 25.0Mn 0.8O 41111 Indium In In 99.9112 Zinn Sn Sn 99.9113 Gold Au Au 99.9114 niedrig leg. Stahl ch 5Cr1/2Mo C 0.13Si 0.25Cr 4.3Mn 0.46Ni 0.10Cu 0.13Mo 0.46Fe 94115 niedrig leg. Stahl ch 9Cr1Mo C 0.13Si 0.38Cr 8.7Mn 0.41Ni 0.24Cu 0.15Mo 0.96Fe 89116 Cr-Stahl ch AISI 446 C 0.09Si 0.37Cr 23.8Mn 0.46Ni 0.31Cu 0.06Mo 0.05Fe 74.8117 Edelstahl ch AISI 310 C 0.07Si 0.53Cr 25.5Mn 1.7Ni 20.1Cu 0.30Mo 0.15Fe 51.7

No. Reference materialSymbol Element concentration %118 Edelstahl ch AISI 347 C 0.06Si 0.77Cr 17.4Mn 1.5Ni 9.9Cu 0.10Nb 0.70Mo 0.17Fe 69.4119 Edelstahl ch Nitronic 40 C 0.04Si 0.64Cr 20.2Mn 9.5Ni 6.6Cu 0.43Mo 0.12Fe 62.5120 Edelstahl ch Nitronic 50 C 0.05Si 0.56Cr 21.2Ni 11.9Cu 0.38Nb 0.16Mo 2.2Fe 58.9121 Edelstahl ch Nitronic 60 C 0.08Si 4.1Cr 16.4Mn 8.2Ni 8.2Cu 0.40Mo 0.23Fe 62.4122 Edelstahl ch 17-4-PH C 0.05Si 0.51Cr 15.51Mn 0.52Ni 4.4Cu 3.2Nb 0.28Mo 0.10Fe 75.5

No. Reference materialSymbol Element concentration %123 Edelstahl ch Invar 36 C 0.06Si 0.27Cr 0.17Mn 0.76Ni 36.1Cu 0.08Mo 0.01Ta 0.18Fe 62.4124 Edelstahl ch Carp20CB3 C 0.2Si 0.32Cr 19.6Ni 33.6Mn 0.48Cu 3.2Co 0.27Nb 0.51Mo 2.1Ta 0.21Fe 39.6125 Edelstahl ch Haynes 556 C 0.11Si 0.45Cr 21.8Mn 1.00Co 17.7Ni 20.2Cu 0.09Mo 2.9W 2.4Fe 33.4126 Edelstahl ch Maraging 300 C 0.01Si 0.03Ti 0.62Cr 0.16Mn 0.03Co 8.9Ni 18.6Cu 0.03Mo 4.9Fe 66.7127 Edelstahl ch BCS 467 C 0.069Mn 0.68Si 0.45P 0.015S 0.019Ni 8.95Cr 18.05Nb 1.06Fe 70.7

No. Reference materialSymbol Element concentration %128 Edelstahl ch NBS 339 C 0.052Mn 0.738Si 0.654S 0.013Cu 0.199Ni 8.89Cr 17.42V 0.058Co 0.096Mo 0.248Se 0.247Fe 71.2129 Edelstahl ch NHKG P-10 C 0.09Mn 0.44Si 1.38P 0.022Ni 10.51Cr 17.34Ti 0.84Fe 69.3130 Edelstahl ch IMZ 1.12 C 0.085Mn 1.60Si 0.56P 0.038S 0.017Ni 10.56Cr 18.63Mo 2.07Ti 0.73Fe 65.7131 Edelstahl ch CS 3/4/04 C 0.072Mn 0.66Si 0.29P 0.046S 0.007Ni 9.21Cr 18.05Cu 0.10Ti 0.63Co 0.026Fe 70.9

No. Reference materialSymbol Element concentration %132 Schnellarbeitsstahl 24/3 C 0.94Si 0.20Mn 0.44S 0.048Cu 0.20Ni 0.17Cr 4.46V 1.05Mo 9.57W 2.83Co 8.92Ti 0.22Fe 70.9133 Schnellarbeitsstahl 24/4 C 1.37Si 0.31Mn 0.58S 0.023Cu 0.34Ni 0.26Cr 3.99V 4.62Mo 1.54W 11.71Co 0.03Ti 0.02Fe 75.5134 Werkzeugstahl ch M2 C 0.86Si 0.39V 1.9Cr 4.3Mn 0.31Ni 0.20Cu 0.14Co 0.16Mo 5.1W 6.3Fe 80.5135 Werkzeugstahl ch T1 C 0.79Si 0.29V 1.1Cr 4.3Mn 0.33Co 0.39Ni 0.23Cu 0.12Mo 0.40W 18.0Fe 74.0

No. Reference materialSymbol Element concentration %136 Werkzeugstahl ch D2 C 1.49Si 0.35V 0.97Cr 12.1Mn 0.32Ni 0.23Cu 0.05Mo 0.86W 0.15Fe 83.5137 Gußeisen * KS C 1.7Si 3.2S 0.14Cr 0.7Mn 0.13Ni 0.01Mo 0.6Fe 93.5138 Gußeisen * US C 2.85Si 0.6P 0.6S 0.02Cr 1.2Mn 0.3Ni 0.04Cu 1.4Fe 93.0139 Gußeisen * RS C 2.8Si 1.6P 0.4S 0.05Cr 0.17Cu 0.06Mo 0.1Sn 0.07Sb 0.05Pb 0.015Fe 93.0140 Gußeisen * IN C 3.45Si 1.75P 0.05S 0.01Cr 0.04Mn 0.2Ni 0.7Cu 0.12Fe 93.6

No. Reference materialSymbol Element concentration %141 Gußeisen * PN C 4.0Si 0.95P 0.27S 0.2Ni 1.2Cu 0.5Fe 93.9142 Al-Legierung CKD 401 Al 85Si 6.9Ti 0.29Cr 0.26Mn 0.83Fe 1.01Cu 3.9Zn 0.99143 Al-Legierung CKD 405 Mg 1.20Al 83Si 12.2Cr 0.28Mn 0.65Fe 0.47Ni 1.37Cu 0.31Zn 0.18144 Ni-Legierung ch Inco 718 Al 0.56Ti 1.0Cr 18.5Mn 0.11Fe 18.8Co 0.25Ni 52.2Nb 5.1Mo 3.1145 Ni-Legierung ch Inco 625 Ti 0.28Cr 21.3Mn 0.22Fe 4.4Co 0.19Ni 60.9Nb 3.3Mo 8.8146 Ni-Legierung ch Haynes 214 Al 4.4Cr 16.1Mn 0.17Fe 3.6Ni 75.6

No. Reference materialSymbol Element concentration %153 Cu-Legierung ch CDA 655 Si 3.1Mn 1.02Fe 0.04Cu 96154 Cu-Legierung ch CDA 836 Fe 0.03Ni 0.78Zn 4.3Sn 4.6Sb 0.09Pb 5.4Cu 85155 Cu-Legierung ch CDA 937 Sb 0.35Ni 0.36Zn 0.27Sn 9.8Pb 9.6Cu 80156 Cu-Legierung ch CDA 955 Mn 0.16Fe 4.0Ni 4.4Zn 0.09Al 10.6Cu 81157 Cu-Legierung ch CDA 932 Fe 0.08Ni 0.09Zn 3.2Sn 6.7Sb 0.07Pb 6.4Cu 83.4158 Cu-Legierung ch CDA 863 Al 6.0Fe 2.3Mn 3.7Zn 23.3Sn 0.04Pb 0.03Cu 65159 Cu-Legierung ch CDA 642 Al 7.0Fe 0.10Si 1.97Zn 0.20Sn 0.05Cu 90.6160 Ag-Legierung P5Ag19Cu75 P 5.8Ag 18.9Cu 75

No. Reference materialSymbol Element concentration %161 Ag-Legierung Cu16Zn16Cd25Ag42 Cu 16.0Zn 16.5Cd 25.0Ag 42.3162 Ag-Legierung Cu27Zn21Ag51 Cu 27.1Zn 21.3Ag 51.6163 Ag-Legierung Cu17Ag83 Cu 17.1Ag 82.8164 Kassiterit SnO 2 Sn 78.8O 21165 Pollucit CsAl 2 Si 3 O 10 Cs 33.3Al 10.4Si 21.1O 35166 Apatit Ca 3 (PO 4 ) 2 P 19Ca 41O 40167 Celestinit SrSO 4 S 16Sr 51O 33168 Scheelit CaWO 4 Ca 15.6W 62.0O 22169 Crocoit PbCrO 4 Cr 18.7Pb 59.5O 22170 Baryt BaSO 4 S 15.0Ba 55.8O 29171 Skutterudit (Co, Ni, Fe)As 3 S 3.3Co 15.4Ni 5.0Fe 2.9As 73.3172 Titanit, brasil. CaTiSiO 5 Al 1.4Si 17.0Ca 19.2Ti 20.6O 41173 Yttriumoxid p Y 2 O 3 Y 79O 21174 Bariumcarbonat p BaCO 3 Ba 70O 24C 6175 Neodymoxid p Nd 2 O 3 Nd 79O 21

No. Reference materialSymbol Element concentration %176 Europiumoxid p Eu 2 O 3 Eu 86O 14177 Gadoliniumoxid p Gd 2 O 3 Gd 87O 13178 Dysprosiumoxid p Dy 2 O 3 Dy 87O 13179 Holmiumoxid p Ho 2 O 3 Ho 87O 13Abbreviations of material properties:* = heterogeneous materialp = powderch = chipped materials = synthetic material