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PITTCON 2015 TECHNICAL PROGRAMPOSTER SESSION Session 2530All posters are to be mounted by 10:00 AM and remain on display until 2:00 PM. Authors must be attheir posters from 10:00 AM to 12:00 PM. Location of the morning posters is on the Exposition Floor,Hall F, Aisles 3900-4500. PLEASE NOTE: You cannot get onto the Exposition Floor until after 9:00 AM.Bioanalytical Samples Using Separation TechniquesThursday Morning(2530-1 P) Removal of Cadmium (II), Cobalt (II) and Nickel (II) from Aqueous Solution UsingCorncob Waste CHIONYEDUA T ONWORDI, Lagos State University, Chinedu H Okwuolise,Olawale L Osifeko, Bukunola K Oguntade, Adedoja D Wusu(2530-2 P) Imaging Glycosphingolipid Distribution in C57BL/6NJ Mouse Brain Tissuevia-MALDI-TOFMS JENNIFER ARCEO, University of Notre Dame, Norman J Dovichi(2530-3 P) Analysis of Underivatized Steroids Using Cold EI GC/MS ADAM J PATKIN, PerkinElmer,Ruben Garnica, Andrew N Tyler, Sharanya Reddy(2530-4 P) Analysis of Subtle Changes in Biological Systems Through Use of High Resolution, HighAccuracy Vanquish UHPLC Generated Libraries with a Q-Exactive HF Mass SpectrometerDAVID A SARRACINO, Thermo Fisher Scientific BRIMS Center, Marc Plante, Keely Murphy, Ian NAcworth, Jason Neil(2530-5 P) High Fructose Feeding Induces Copper Deficiency: A Fecal Metabolomics Study XINMINYIN, University of Louisville, Xiaoli Wei, Ming Song, Craig McClain(2530-6 P) Design and Optimization of a Liquid Chromatography Method for Quantification ofSpecific Active Thiol-Molecule Reducing Agents in Protein Matrices SAM DIEP, AbbottLaboratories, Tracey Rae, Ewa Lang, Jeffrey Fishpaugh(2530-7 P) Improved Peptide Mapping Methods JEFFREY A KAKALEY, YMC America, Inc.,Ernest J Sobkow(2530-8 P) Validated HPLC-DAD and HPLC-Fluorimetric Methods for SimultaneousDetermination of Granisetron and Domperidone in Bulk Form, PharmaceuticalFormulations, and in Plasma RASHA A SHAALAN, Alexandria University, Saied F Belal,Rim S Hagag, Mahmoud A Agami(2530-9 P) In Vivo Monitoring of Branched Chain Amino Acid Dynamics Using Online Microdialysis-Capillary Electrophoresis MEGAN WEISENBERGER, University of Minnesota, Michael Bowser(2530-10 P) An Integrated Platform of LC-MS, HPAEC-PAD, and Bioinformatics for the CarbohydrateProfiling of Therapeutic Glycoproteins ANDREA GRAY, University of Maryland BaltimoreCounty, Shaunak Uplekar, Joshua Wilhide, William R LaCourse, Govind Rao(2530-11 P) Analysis of Polysorbate 80 in Protein Formulations Using 2D LCMS WILLIAM HEDGEPETH,Shimadzu Scientific Instruments, Kenichiro Tanaka, Keiko Yamabe(2530-12 P) Using Fluorescence and Mass Spectrometry to Determine Glycation Sites of HumanSerum Albumin WEIXI LIU, University of Rhode Island, Menashi A Cohenford, Leslie Frost,Joel A Dain(2530-13 P) Differentiation of Heparin and Heparin-Like Glycosaminoglycans (GAGs) viaPeroxide-Z Based Digestion with LC-MS and CE-UV Detection HONGLI LI, Food and DrugAdministration, Samanthi Wickramasekara, Peter Nemes, Rahul Kaushal(2530-14 P) An Improved Chromatographic Method for Arsenic Speciation in Urine KENNETHNEUBAUER, PerkinElmer, Wilhad M Reuter, Charles Schneider(2530-15 P) A Kinetic Study of the Maillard Reaction by On-Line Monitoring with SequentialInjection-Nuclear Magnetic Resonance Spectroscopy KELSEY A HOLBERT, University ofWisconsin Milwaukee, Marie E Nider, Joseph H Aldstadt(2530-16 P) An Automated Dual Stage Solid Phase Extraction Procedure for 15 F2t-isoprostane(8-iso Prostaglandin2a) from BSA as Lipid Markers of Oxidative Stress MARTIN CHER-RIER, Biotage, Elena Gairloch, Victor Vandell, Frank Kero(2530-17 P) Chemometric Analysis of MALDI Mass Spectrometric Images of Three-Dimensional CellCulture Systems RICHARD B KEITHLEY, Roanoke College, Eric M Weaver, Amanda B Hummon(2530-18 P) Effects of SDS and DTT in Protein Determination Using the 660 nm Protein Assay HUIXIE, Abbott Laboratories, Ewa Lang, Jeffrey Fishpaugh, Carol Ramsay(2530-19 P) Coupling Advanced Detection Techniques to Size Exclusion Chromatography XIAOLIWANG, Agilent Technologies, Andrew Coffey, Linda LloydPOSTER SESSION Session 2540All posters are to be mounted by 10:00 AM and remain on display until 2:00 PM. Authors must be attheir posters from 10:00 AM to 12:00 PM. Location of the morning posters is on the Exposition Floor,Hall F, Aisles 3900-4500. PLEASE NOTE: You cannot get onto the Exposition Floor until after 9:00 AM.Food SciencesThursday Morning(2540-1 P) Determination of Nitrite Using Captopril by UV Spectrophotometry and Flow InjectionAnalysis JONATHAN P SCAFFIDI, Miami University, Mya A Porche, Zhaowei Guo, Youxin Li, NeilD Danielson(2540-2 P) Determination of Sulfur-Containing Species in Scotch Whiskeys Using GasChromatography With Pulsed-Flame Photometric Detection J GARRETT SLATON,Xylem/OI Analytical, Cynthia Elmore(2540-3 P) Only One Platform to Approach Different Sample Preparation for the Food QualityCharacterization ILARIA FERRANTE, Dani Instruments s.p.a., Daniele Recenti, RobertaLariccia, Chiara Abate(2540-4 P) Raw Material Characterization and Comparison with Gas Chromatography withTime-of-Flight Mass Spectrometry (GC-TOFMS) ELIZABETH HUMSTON-FULMER, LECOCorporation, Joe E Binkley, Jeffrey S Patrick(2540-5 P) Determination of Hexanal in Foods Utilizing Dynamic Headspace GC/MSROGER BARDSLEY, Teledyne Tekmar, Tammy Rellar, Thomas Hartlein, Kristina Mason, Jacob ARebholz, Tyler Trent(2540-6 P) Optimization of Solid Phase Micro Extraction of Aroma Compounds in Wine ANNEJUREK, EST Analytical, Lindsey Pyron, Kelly Cravenor(2540-7 P) An Examination of Automated Sampling Techniques of Whiskey Samples ANNE JUREK,EST Analytical, Lindsey Pyron, Kelly Cravenor(2540-8 P) Advanced Alternative to SPME GCMS Sample Preparation Using Vacuum AssistedPorous Cartridge Micro Extraction (VA-PCME) THOMAS X ROBINSON, Entech Instruments,Inc., Daniel B Cardin(2540-9 P) Study of Magnetic-Bead Systems to Remove Peanut Allergens SI-YIN CHUNG, USDA,Shawndrika Reed(2540-10 P) Use of Red Chili Pepper as Natural Antioxidant for Improving the Oxidative Stability ofEdible Oil STEFANO CASIRAGHI, Velp Scientifica SRL, Stefania Corti, Claudia Mancinelli(2540-11 P) Monitoring Basmati Rice Sensory Quality Thanks to an Electronic NoseJEAN-CHRISTOPHE MIFSUD, Alpha MOS, Herve Lechat, Fatma Ayouni, Valerie Vabre, AndrewCowell, Marion Bonnefille(2540-12 P) Scale-Up of Subcritical Water Extraction of Polyphenolic Compounds from Fruit WasteMaterial ROLF SCHLAKE, Applied Separations, Al Kaziunas, Jerry King(2540-13 P) Analysis of Electronic Cigarette Liquid and Vapor JASON S HERRINGTON, Restek, AmandaRigdon, Steve Kozel, Jaap de Zeeuw, Rebecca Stevens, Linx Waclaski, Colton Myers(2540-14 P) Optimization of Type of Culture, Ripening Time, Temperature and Salt Concentration ina Model Cheese Using Response Surface Methodology: Determination of Proteolysis inCheese by Chromatographic Methods ALI A HAYALOGLU, Inonu Univeristy, Didem SahingilPOSTER SESSION Session 2550All posters are to be mounted by 10:00 AM and remain on display until 2:00 PM. Authors must be attheir posters from 10:00 AM to 12:00 PM. Location of the morning posters is on the Exposition Floor,Hall F, Aisles 3900-4500. PLEASE NOTE: You cannot get onto the Exposition Floor until after 9:00 AM.Liquid Chromatography - General InterestThursday Morning(2550-1 P) Small Scale Purification of Constituents from Complex Natural Product Extracts Usingsub-2-μm Chromatography ANDREW J AUBIN, Waters Corporation, Jo-Ann M Jablonski,Wendy Harrop(2550-2 P) How Scalable are the Dispersion Processes in Real Columns Packed with Solid CoreMaterial? TONY EDGE, Thermo Fisher Scientific, Luisa Pereira, Monica Dolci(2550-3 P) Can Core-Shell Silica Boost Efficiency of Macrocyclic Oligosaccharide Based HILICPhases? ZACHARY S BREITBACH, University of Texas at Arlington, Choyce A Weatherly,Maressa D Dolzan, Daniel A Spudeit(2550-4 P) Retention Behavior of Aromatic Compounds When Using a Fluorophenyl HPLCStationary Phase Under Highly Aqueous Mobile Phase Conditions BRITTANY GEORGE,Ursinus College, Eric Williamsen(2550-5 P) Evaluation of Monodisperse Silica for High Performance Liquid Chromatography UsingVan Deemter Plot NORIKAZU NAGAE, ChromaNik Technologies Inc., Tomoyasu Tuskamoto,Shun KojimaThursday Morning83The author list is available at www.pittcon.org