PITTCON 2015 TECHNICAL PROGRAMTuesday AfternoonPOSTER SESSION Session 1530All posters are to be mounted by 10:00 AM and remain on display until 4:00 PM. Authors must be attheir posters from 1:00 PM to 3:00 PM. Location of the afternoon posters is on the Exposition Floor,Hall F, Aisles 3900-4500. PLEASE NOTE: You cannot get onto the Exposition Floor until after 9:00 AM.Environmental Samples - Sampling, Detection and Water/Soil SamplesTuesday Afternoon(1530-1 P) Automation of a Solid Phase Extraction (SPE) Fractionation Step for Aliphatics andAromatics in Oil Fingerprinting Analysis MICHAEL J TANNER, J2 Scientific(1530-2 P) Alternative Approaches to the Gel Permeation Chromatography Clean-up Step whenUsing CLP Method SOM01.1 and EPA Method 3640A MICHAEL J TANNER, J2 Scientific(1530-3 P) Novel Method for the Detection of Arsenic Using a Bare Glassy Carbon ElectrodeTHOMAS CARPENTER, Uninversity of Tennessee, Knoxville, Carlos W Lee, James Q Chambers,Zi-Ling Xue(1530-4 P) Wetland Drying and Wetting Impacts on Greenhouse Gas (GHG) Fluxes DALE LECAPTAIN,Central Michigan University, Johann Britting, Taylor West(1530-5 P) Real-Time Voltammetric Characterization of Metal Complexation THUSHANI MSIRIWARDHANE, Wayne State University, Audrey Sulkanen, Annette Tremonti, PavithraPathirathna, Shawn P McElmurry, Parastoo Hashemi(1530-6 P) Covalent Scaffolding Functionalization of Carbon Fiber Microelectrodes (CFMs) forHigh-Selectivity Trace Metal Detection YUANYUAN YANG, Wayne State University, Ahmad AIbrahim, Jennifer Stockdill, Parastoo Hashemi(1530-7 P) Color Measuring in Industrial Wastewater MARÍA I TABARES BERNAL, UniversidadPontificia Bolivariana, Beatriz E Gómez Hoyos , Jose A Ríos Arango, Erwin Ramírez Muñoz,Faber E Peñaloza Anaya, Francisco J Jiménez García, Viviana A Martínez(1530-8 P) Aptamer-Based Electrochemical Biosensing Platform for Detection of HormonalPollutants in Water GASTON CONTRERAS, UQAM, Shimaa Eissa, Andy Ng, MohammedZourob, Mohamed Siaj(1530-9 P) Layered Double Hydroxide Membranes as Phosphate Sensitive Electrodes MARTIN EENEMCHUKWU, University of South Africa(1530-10 P) Analysis of Arsenic in Aqueous Solutions Using Cyclic Voltammetric DeterminationSEUNG MOK LEE, Catholic Kwandong University(1530-11 P) Development of Electron Tracking Compton Camera for Fine Imaging andQuantitatively Dose-Monitoring to Environmental Gamma-Ray DAI TOMONO, KyotoUniversity, Tetsuya Mizumoto, Atsushi Takada, Toru Tanimori, Shotaro Komura, Hidetoshi Kubo,Yoshihiro Matsuoka, Yoshitaka Mizumura, Kiseki Nakamura, Shogo Nakamura, Makoto Oda,Joseph D Parker, Tatsuya Sawano, Naoto Bando, Akira Nabetani(1530-12 P) Determination of Veterinary Antibiotics Found Within the Soil and Groundwater ofFarmlands ALEX MESSUR, St. John Fisher College, Kimberly Chichester(1530-13 P) Evaluation of the Waste Generated in Wastewater Treatment as Energy’s CogeneratorMARISA S CRESPI, Chemistry Institute/UNESP, Weverton C Nozela, Sandra I Maintinguer,Clovis A Ribeiro(1530-14 P) Development of Test Paper for Fluoride Ion with ON-OFF Color Change Reaction SHOHEIFUKIAGE, Institute of National College of Technology , Atsushi Manaka, Shukuro Igarashi(1530-15 P) Analyzing Total Organic Carbon in Sea Water KRISTINA MASON, Teledyne Tekmar, TammyRellar, Thomas Hartlein, Jacob A Rebholz, Tyler Trent, Roger Bardsley(1530-16 P) Biosorption of 2-nitrophenol and 4-nitrophenol from Aqueous Solutions UsingActivated Charcoal of Grape (Vitis Vinifera) Leaf Litter BEATRICE O OPEOLU, CapePeninsula University of Technology, W O Afolabi, Olalekan Siyanbola Fatoki, B J Ximba,Olatunde S Olatunji(1530-17 P) Removal and Decolorization of Dye Bearing Textile Effluents by Urea-FormaldehydeResins HASUKH S PATEL, SP University(1530-18 P) The Application of Infrared Microspectroscopy for the Analysis of Microplastics inWater-Borne Environmental Samples IAN ROBERTSON, PerkinElmer Limited, GuidoLohkamp-Schmitz, Justin Lang(1530-19 P) Light Weight Evaporation Vessel for the Determination of Dissolved Solids DAVIDSMITH, Environmental Express, Joe Boyd, Edward Kim(1530-20 P) Soil Respiration and Its Analytical Use for Rating Contaminated Soil FRANK HONOLD,Xylem - WTW, Klaus ReithmayerPOSTER SESSION Session 1540All posters are to be mounted by 10:00 AM and remain on display until 4:00 PM. Authors must be attheir posters from 1:00 PM to 3:00 PM. Location of the afternoon posters is on the Exposition Floor,Hall F, Aisles 3900-4500. PLEASE NOTE: You cannot get onto the Exposition Floor until after 9:00 AM.Environmental Samples - Separation TechniquesTuesday Afternoon(1540-1 P) Extending Hexavalent Chromium Stability in Industrial Hygiene Applications ANITAHSOUNA, High-Purity Standards, Svetlana Uzunova(1540-2 P) Simultaneous Analysis of Isocyanate Monomers and Oligomers as Urea DerivativesUsing UHPLC-MS-MS/MS EMILY R BARREY, Supelco/Sigma-Aldrich, Olga I Shimelis, KristenSchultz, Michael Ye, Jamie L Brown, Gaurang Parmar(1540-3 P) Quantitative Analysis of Isocyanates During Spray Painting Using Dry Air Sampler andLC-MS/MS Analysis EMILY R BARREY, Supelco/Sigma-Aldrich, Olga I Shimelis, Michael RHalpenny, Jamie L Brown, Michael Ye(1540-4 P) Mercury Speciation by Selective Pre-Concentration and Liquid Chromatography ColdVapour Atomic Fluorescence Spectrometry (Prec HPLC-CV-AFS) - An Efficient Method forMany Sample Matrices CORNELIUS C BROMBACH, University of Aberdeen, Bin Chen, Warren TCorns, Jorg Feldmann, Eva Krupp(1540-5 P) Online Monitoring of Hg, Se and As in FGD Wastewater Treatment Plants WARREN TCORNS, P S Analytical, Bin Chen(1540-6 P) Improved Quantification Method of Organic Toxins for Human Health Assessment UsingDirect Isotope Dilution Mass Spectrometry Gas Chromatography MICHAEL MILES,Duquesne University, Elizabeth Clouser, Andrew Boggess, Logan T Miller, HM Skip Kingston,Scott Faber(1540-7 P) Removal of Cr(VI) from Aqueous Solutions Using the Polyurethane Foam LikeAdsorbent HIROAKI MINAMISAWA, Nihon University, Hiromichi Asamoto, MinamisawaMayumi, Saitoh Kazunori, Tatsuro Nakagama(1540-8 P) Determination of Selected Metals in Rice by Inductively Coupled Plasma OpticalEmission Spectrometry and Anodic Stripping Voltammetry JOSEPH SNEDDON, McNeeseState University, Joel Richert, Carey J Hardaway(1540-9 P) Irrigation of Selected Crops with Abandoned Mine Drainage: Preliminary Results andEvaluation of Uptake of Selected Metal Analytes MARK THOMAS STAUFFER, University ofPittsburgh Greensburg, Eric D Deihl(1540-10 P) Application of the Leaching Environmental Assessment Framework and VapourGeneration Atomic Fluorescence Spectroscopy to Investigate the Fate of Mercury andArsenic Species after Smouldering Remediation of Contaminated Soils CHRISTINESWITZER, University of Strathclyde, Mara L Knapp, Warren T Corns, Andrew Robson, Rossane CDeLapp, David S Kosson(1540-11 P) Solid Phase Extraction and Analysis for Polychlorinated Biphenyls (PCBs) andOrganochlorine Pesticides (OCPs) in Plasma Samples of Humans Resident in Lagos,Nigeria ADEYEMI DAVID KEHINDE, University of Lagos, Adeyao Adeleye, Godfred Darko(1540-12 P) Revisions to EPA Method 624 for Analysis of VOCs by GC/MS BRAHM PRAKASH, ShimadzuScientific Instruments, Inc., William Lipps, Laura Chambers, Di Wang(1540-13 P) Parts-per-Trillion SVOC Air Analysis with Novel Optical GC Detector MARTIN L SPARTZ,Prism Analytical Technologies, Inc., Anthony S Bonanno, Stacey E Beyer, Alice E Delia(1540-14 P) Formation of Disinfection Byproducts and Associated Bromine Substitution FactorsUpon Chlorination/Chloramination of Seawater HAITING ZHANG, Missouri University ofScience and Technology, Huiyu Dong, Honglan Shi, Yinfa Ma, Zhimin Qiang(1540-15 P) Determination of Endocrine Disrupting Chemicals in Ground Water in Herkimer CountyELAINA ZITO, St. John Fisher College, Kimberly Chichester(1540-16 P) Characterization of Microbial Transformation Products of Persistent Organic Pollutantsby GC×GC and High Performance Mass Spectrometry CHRISTINE GALLAMPOIS, UmeaUniversity, Peter Haglund, Jonathan Byer, Elizabeth Humston-Fulmer, Joe E Binkley,Lorne M Fell(1540-17 P) Application of Newly Developed Inert GC Columns for Analysis of ComplexEnvironmental Samples Using GC and GC/MS KRISHNAT P NAIKWADI, J & K Scientific Inc.,Allen J Britten(1540-18 P) Validation of Environmental Water Methods on One System: Considerations for SampleVolume, Purge Parameters and Quality Control Parameters JACOB A REBHOLZ, TeledyneTekmar, Thomas Hartlein, Roger Bardsley, Tyler Trent, Kristina Mason, Tammy Rellar(1540-19 P) Improved Siloxane Measurement in Air Using Ultra Inert Stainless Steel VacuumSampling Canisters THOMAS X ROBINSON, Entech Instruments, Inc., Daniel B CardinThe author list is available at www.pittcon.org58
(1540-20 P) Identification of Biomarkers of Exposure to Emerging Environmental Chemicals UsingHPLC and Mass Spectrometry MANORI SILVA, Centers for Disease Control and Prevention,James Preau, Ella Samandar, Donald Hilton, Antonia Calafat, Xiaoyun Ye, Johnathan Furr, LEarl Gray(1540-21 P) A Comparative Study of TOC and THM Analysis of Municipal Drinking Water UsingHeated Sodium Persulfate Oxidation and a Novel Approach to EPA Method 524.4 JOHNF WELSH, Xylem/OI Analytical, Cynthia Elmore, Steven J Skalski(1540-22 P) Screening for Pesticides in Medical Marijuana Using Triple-Quadrupole GC-MS/MS DIWANG, Shimadzu Scientific Instrument, Laura Chambers, William Lipps, Zhuangzhi ‘Max’Wang, Robert Clifford(1540-23 P) Cadmium Isotopic Composition Indicates Multiple Geological Sources in CadmiumAnomaly in Jamaican Soils ADRIAN SPENCE, University of the West Indies, Johann MAntoine, Charles G Grant(1540-24 P) Determination of Ni2+ by Dispersive Micro Solid Phase Extraction-Flame AtomicAbsorption Using Multi-Wall Carbon Nanotubes Coated by Electro-Reduction Product of4-Nitrophenol as an Adsorbent MEHDI JALALI, University of Guilan, Alirez Aliakbar, NargesLarki, Ghahraman Afshar MajidPOSTER SESSION Session 1550All posters are to be mounted by 10:00 AM and remain on display until 4:00 PM. Authors must be attheir posters from 1:00 PM to 3:00 PM. Location of the afternoon posters is on the Exposition Floor,Hall F, Aisles 3900-4500. PLEASE NOTE: You cannot get onto the Exposition Floor until after 9:00 AM.Liquid Chromatography - Food Science, Bioanalytical and BiomedicalTuesday Afternoon(1550-1 P) Separation of Lactose, Lactulose and Epilactose by a New HILIC Column SATOKO SAKAI,Showa Denko K.K., Naoya Nakajima, Mellissa Turcotte, Ronald Benson(1550-2 P) An Abnormal Retention Behavior of Pyrazines with Acetonitrile-Based Mobile Phasesin Reversed-Phase Liquid Chromatography HAYATO TAKEUCHI, Toyohashi University ofTechnology, Akira Kobayashi, Ikuo Ueta, Yoshihiro Saito(1550-3 P) Simultaneous Analysis of Water- and Fat-Soluble Vitamins in Beverages Using anODS-Modified and Metal-Doped Column KENICHIRO TANAKA, Shimadzu ScientificInstruments, Inc., William Hedgepeth(1550-4 P) Determination of Amyloid Fibrils by High-Performance Liquid Chromatography-Fluorescence Detection With Post Column Labeling ASAMOTO HIROMICHI, NihonUniversity, Nakagama Tatsuro, Saitoh Kazunori, Minamisawa Hiroaki(1550-5 P) Determination of p-Toluidine, Sulfonated p-Toluidines, 1-Hydroxyanthraquinone,1, 4-Dihydroxyanthraquinone, and Subsidiary Colors in Ext. D&C Violet No. 2 UsingUltra-Performance Liquid Chromatography HUEIHSUAN W YANG, Food and DrugAdministration, Julie Barrows(1550-6 P) Direct Carbohydrate Analysis in Beverages and Food Using Pulsed Amperometric andCharged Aerosol Detection BRUCE BAILEY, Thermo Fisher Scientific, Qi Zhang, Marc Plante,Ian N Acworth(1550-7 P) Improved Throughput and Resolution of Xanthones in Mangosteen PericarpBRUCE BAILEY, Thermo Fisher Scientific, Qi Zhang, Marc Plante, Ian N Acworth(1550-8 P) Determination of A-Type and B-Type Procyanidins in Apple, Cocoa and CinnamonExtracts DAVID H THOMAS, Thermo Fisher Scientific, Ian N Acworth, Jan Glinsky, Alan Wong,Glinsky B Vitold(1550-9 P) Novel Method for Identification of Deinococcus and Hymenobacter Using HighPerformance Liquid Chromatography THOMAS KUBORN, University of Wisconsin Oshkosh,Patrick Klepp, Kevin Crawford, Sabrina Mueller-Spitz(1550-10 P) Portable Medium Pressure Capillary Liquid Chromatography based on a ModularMicrofluidic System Using Off-the-Shelf Components YAN LI, University of Tasmania,Miloš Dvo ák, Nantana Nuchtavorn, Pavel N Nesterenko, Roger Stanley, Jana Aufartová, LenkaKujovská Kr mová, Mirek Macka(1550-11 P) Characterization of Binding by Second Generation Sulfonylurea Drugs to GlycatedHuman Serum Albumin by Using High-Performance Affinity Chromatography RYANMATSUDA, University of Nebraska-Lincoln, Jeanethe Anguizola, KS Joseph, Zhao Li, XiweiZheng, David S Hage(1550-12 P) Site-Directed Immobilization of Genetically Engineered Single-Domain AntibodiesSignificantly Increases the Efficiency of Immunoaffinity Columns KAITLYNN R DAVEN-PORT, Northern Illinois University, Chris Smith, James Horn, Oliver Hofstetter(1550-13 P) Separation of Heparin and Other Glycosaminoglycans Using Weak Anion ExchangeChromatography YOUXIN LI, Tianjin University, Jennifer M Fasciano, Ying Zhang, Richard TTaylor, James J Bao, Neil D DanielsonPITTCON 2015 TECHNICAL PROGRAMPOSTER SESSION Session 1560All posters are to be mounted by 10:00 AM and remain on display until 4:00 PM. Authors must be attheir posters from 1:00 PM to 3:00 PM. Location of the afternoon posters is on the Exposition Floor,Hall F, Aisles 3900-4500. PLEASE NOTE: You cannot get onto the Exposition Floor until after 9:00 AM.Sampling and Sample Preparation TechniquesTuesday Afternoon(1560-1 P) Evaluation of a Novel 96-Well Filter Plate for the Effective Removal of Serum Proteinand Phospholipids Prior to LC-MS/MS Analysis ELENA GAIRLOCH, Biotage, Lee Williams,Martin Cherrier, Victor Vandell, Frank Kero(1560-2 P) A Novel Approach to Low Volume Sample Preparation JON BARDSLEY, Thermo FisherScientific, Ken Meadows(1560-3 P) Using SPE to Achieve a Twenty Fold Pre-Concentration without the Need forEvaporation and Reconstitution KEN MEADOWS, Thermo Fisher Scientific(1560-4 P) Use of Unique Retention Properties of Graphitized Carbon Toward Passive Sampling of1,3-Butadiene and Other Hazardous Pollutants in Air JAMIE L BROWN, Supelco/Sigma-Aldrich, Olga I Shimelis, Kristen Schultz, Daniel Vitkuske, Michael Ye(1560-5 P) Semi-Automated Large Volume Sample Extraction for Detection of Pharmaceuticalsand Personal Care Products KEVIN CRAWFORD, University of Wisconsin Oshkosh(1560-6 P) Fast Analysis of Volatile Organic Compounds in Water in Compliance With EPAMethod 8260 ILARIA FERRANTE, Dani Instruments s.p.a., Abate Chiara, Roberta Lariccia,Daniele Recenti(1560-7 P) Automated Liquid-Liquid Extraction of PAH Compounds in Water ANNE JUREK, ESTAnalytical, Lindsey Pyron, Kelly Cravenor(1560-8 P) The Use of Thermal Extraction to Investigate Hazardous Chemicals in ConsumerProducts KAREN SAM, CDS Analytical, Stephen Wesson, Gary Deger, Chris Dwyer(1560-9 P) Passive Monitoring – A Guide to Sorbent Tube Sampling for EPA Method 325 NICOLAWATSON, Markes International, David Wevill, Peter Grosshans, Vanessa Frost-Barnes(1560-10 P) Understanding the Health Safety and Environmental Implication of FormulatingSolutions in the Laboratory Environment ANTHONY R KEMPERMAN, Honeywell, Burdickand Jackson(1560-11 P) New Selective SPE Clean-Up Method Based on Molecularly Imprinted Polymers forGlyphosate and AMPA Analysis with and without Derivatization for Water, Food andFeed SAMI BAYOUDH, Polyintell, Kaynoush Naraghi, Delphine Derrien, Berengere Claude,Philippe Morin, Kinga Puzio, Catherine Berho, Laurence Amallric, Emeline Grellet(1560-12 P) Improvement in Extraction Efficiency of Existing Pesticide Residues in Food ThroughIntroduction of Simple Automated Vortexer During QuEChERS Procedure OLGA ISHIMELIS, Supelco/Sigma-Aldrich, Ken G Espenschied, Michael Ye, Katherine K Stenerson,Jennifer Claus, Daniel Vitkuske(1560-13 P) An Update on the QuEChERS Tablet JULIE KOWALSKI, Restek, Rebecca Stevens, JackCochran, Jaap de Zeeuw, Linx Waclaski, Mike Chang(1560-14 P) The Use of QuEChERS and IL-SDME for the Extraction of Drugs of Abuse from UrineUsing Gas Chromatography-Mass Spectrometry MICHELLE L SCHMIDT, Seton HallUniversity, Leanne Mocniak, Nicholas H Snow(1560-15 P) Application of Extraction Induced by Emulsion Breaking in the Determinationof Chloride in Brazilian Crude Oils by Ion Chromatography RICARDO J CASSELLA,Universidade Federal Fluminense, Fernanda N Feiteira, Nicolle F Robaina, AlessandraR Cassella(1560-16 P) High-Throughput Clean-Up for Drugs of Abuse in Urine Using a Liquid Handling SystemJASON WEISENSEEL, PerkinElmer, Amanda Prior, Wilhad M Reuter(1560-17 P) Automating Liquid-Liquid Extractions Using a Bench-Top Workstation EDWARDPFANNKOCH, GERSTEL, Inc., Fredrick Foster, Jacqueline Whitecavage, John Stuff(1560-18 P) Performance Update and Review of Coatings used to Improve Reliability and Accuracyfor Sulfur, Mercury and NH 3 Samples LUKE PATTERSON, SilcoTek Corporation, Gary BaroneTuesday Afternoon59The author list is available at www.pittcon.org