OptiMelt Automated Melting Point System - Stanford Research ...
OptiMelt Automated Melting Point System - Stanford Research ...
OptiMelt Automated Melting Point System - Stanford Research ...
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viContents<strong>Melting</strong> <strong>Point</strong> Range 57<strong>Melting</strong> <strong>Point</strong> Depression 60Chapter 4 Maintenance and Calibration 63Temperature Offset Calibration 63Camera Adjustments 73Replacement of Faulty LEDs 75Broken Capillaries 75Cleaning 75Appendix A Pharmacopeia vs. Thermodynamic <strong>Melting</strong> <strong>Point</strong>Determinations 77Pharmacopeia <strong>Melting</strong> <strong>Point</strong> 77Thermodynamic <strong>Melting</strong> <strong>Point</strong> 79Thermodynamic Correction 80Thermodynamic Correction with <strong>OptiMelt</strong> 81Appendix B <strong>Melting</strong> <strong>Point</strong> Certified Reference Standards 85What is a Certified Reference Standard? 85O100MPS CRS Kit 89Substance 90Appendix C Using Melt Graphs 91Melt Graphs 91Melt Playback (MeltView Software) 93Appendix D <strong>OptiMelt</strong> Remote Programming 95Using USB 95Windows XP, 2000/98 95Using Commands 100<strong>System</strong> Commands 102Temperature and Oven Commands 103<strong>Melting</strong> <strong>Point</strong> Determination Commands 104<strong>Automated</strong> Determination Commands 105Report Generation Commands 106Backlight Commands 108<strong>OptiMelt</strong> <strong>Automated</strong> <strong>Melting</strong> <strong>Point</strong> <strong>System</strong>
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