OptiMelt Automated Melting Point System - Stanford Research ...

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64 Maintenance and Calibration Chapter 4Report created at the end of each melting point determination. Alternatively, the lastcalibration date, expiration date, calibration index and calibration interval aredisplayed in the Calibration menu (Figure 34) reached by touching Calibrate in theSystem menu and entering the password (“cal”).Figure 34. Calibration Menu• If the instrument’s heating block was modified in any way since the last calibrationdate, perform an Acceptability Test on the instrument following the instructions inthe next section.• If a new ramping rate, different from the one used for the last calibration, needs to beapplied to upcoming routine MP determinations, perform an Acceptability Test onthe instrument following the instructions in the next section and using the newramping rate throughout the test.OptiMelt Automated Melting Point System
Chapter 4 Maintenance and Calibration 65Does Your OptiMeltNeed Calibration?Is the current calibration trusted?NoYesIs the current calibration GLPdocumented?NoYesHas the current calibration expired?YesNoHas the heating block beenmodified since the last calibration?YesNoIs a new ramping rate required?YesNoYour unit is Acceptable formelting point determinationsPerform Acceptability Test andcalculate temperature offsetcorrections (TOCs)YesDo the TOCs meet specifications?NoUpdate the unit’s temperatureoffsets using the calculated TOCsFigure 35. Temperature Offset Calibration Protocol.OptiMelt Automated Melting Point System
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iiSafety and Preparation For Use•
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ivSafety and Preparation For UseOpt
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viContentsMelting Point Range 57Mel
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viiiFront Panel OverviewReady LEDA
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xBack Panel OverviewPrinterOptiMelt
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xiiSpecificationsOptiMelt Automated
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2 Getting Started Chapter 1• Repl
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4 Getting Started Chapter 1Ceramic
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6 Getting Started Chapter 1Principl
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8 Getting Started Chapter 1Quick St
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10 Getting Started Chapter 18. Preh
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12 Getting Started Chapter 1Touch t
Page 28 and 29: 14 Getting Started Chapter 1If none
Page 30 and 31: 16 Getting Started Chapter 1• Tou
Page 32 and 33: 18 Getting Started Chapter 1OptiMel
Page 34 and 35: 20 Displays and Menus Chapter 2Nume
Page 36: 22 Melt Screen Chapter 2Melt Screen
Page 39 and 40: Chapter 2 Melt Screen 25Touch the T
Page 41 and 42: Chapter 2 Melt Screen 27Select Newe
Page 43 and 44: Chapter 2 Melt Screen 29Select Came
Page 45 and 46: Chapter 2 Melt Screen 31Options Men
Page 47 and 48: Chapter 2 Melt Screen 33The thermod
Page 49 and 50: Chapter 2 Timer Screen 35ResetTouch
Page 51 and 52: Chapter 2 T Meter Screen 37Alarm Lo
Page 53 and 54: Chapter 2 System Screen 39System Sc
Page 55 and 56: Chapter 2 System Screen 41The Print
Page 57 and 58: Chapter 2 System Screen 43Screen Me
Page 59 and 60: Melting Point Determination 45Chapt
Page 61 and 62: Chapter 3 Melting Point Determinati
Page 77: Maintenance and Calibration 63Chapt
Page 81 and 82: Chapter 4 Maintenance and Calibrati
Page 91 and 92: Pharmacopeia vs. Thermodynamic Melt
Page 93 and 94: Appendix A Pharmacopeia vs. Thermod
Page 99 and 100: Melting Point Certified Reference S
Page 101 and 102: Appendix B Melting Point Certified
Page 103 and 104: Appendix B Melting Point Certified
Page 105 and 106: Using Melt Graphs 91Appendix CUsing
Page 107 and 108: Appendix C Using Melt Graphs 93The
Page 109 and 110: OptiMelt Remote Programming 95Appen
Page 111 and 112: Appendix D OptiMelt Remote Programm
Page 123: Appendix D OptiMelt Remote Programm
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