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Magnetron sputtering of Superconducting Multilayer Nb3Sn Thin Film

Magnetron sputtering of Superconducting Multilayer Nb3Sn Thin Film

Magnetron sputtering of Superconducting Multilayer Nb3Sn Thin Film

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chamber which is 280 mm high and 100 mm <strong>of</strong> the diameter, we use two planarbalanced magnetrons. The Sn magnetron should be mounted at the bottom <strong>of</strong> thechamber because <strong>of</strong> the lower melting point, and the Nb magnetron is mounted at thetop <strong>of</strong> the chamber as shown in Fig. 3.2.The sample holder is in the centre <strong>of</strong> the chamber and it is an aluminium diskconnected to a rotary feed through. In this way we can rotate the samples, and every180° rotation we expose the sample to Nb plasma before, and Sn plasma after. Thedistance between targets and samples is 70 mm and during the <strong>sputtering</strong> we useArgon as process gas whose pressure is about 10 -3 mbar. No substrate heating systemswere employed.Fig. 3.3 the UHV multilayer deposition chamber3.2 Deposition on sapphireThe multilayer can be deposited on the sapphire and the Nb sample. Because <strong>of</strong>the perfect flat <strong>of</strong> the sapphire surface, all the parameters <strong>of</strong> the thin film on thesapphire can be measured, such as T c , RRR, thickness and XRD. On the other side,only T c and RRR <strong>of</strong> the thin film on the Nb sample can be measured. So, we firstinvestigate the multilayer deposited on the sapphire.3.2.1 Deposition parameterSame with the deposition <strong>of</strong> Nb thin film on the sapphire, the main parameters <strong>of</strong>the deposition multilayer are including the <strong>sputtering</strong> current, the deposition time andthe proceeding pressure. In our experiment, we fix the proceeding pressure <strong>of</strong> 5*10 -3mbar and the Sn <strong>sputtering</strong> current <strong>of</strong> 0.15mA. The deposition time is also fixed. Todeposit the buffer layer and over layer, we use the Nb <strong>sputtering</strong> current <strong>of</strong> 0.8mA for42

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