ACE C18-AR and C18-PFP - Hplc.eu

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Selectivity Changes by Changing Organic Modifier10,12mAU0 100 2005768,11916ACE C18‐AR13 1415MeOH/0.1% HCOOHmAU0 100 2004,569ACE C18‐PFP10,12,13157,8 11 1614MeOH/0.1% HCOOH3.0 4.0 5.0 6.05) benzoic acid, 6) myrecetin, 7) p‐cresol, 8) propranolol, 9) ethylparaben, 10) furosemide, 11) anisole,12) 1,3,5‐trinitrobenzene, 13) toluene, 14) nimesulide, 15) mefenamic acid, 16) 1,2,3‐trichlorobenzene10ACE C18‐AR4.0 5.04) phenacetin, 5) p‐cresol, 6) acetophenone, 7) quercetin, 8) carvedilol, 9) 1,3‐dinitrobenzene,10) tolmetin 11) 3,4‐dichlorobenzoic acid, 12) ethyl benzoate 13) toluene 14) ibuprofen 15)indomethacin, 16) 1,2‐dichlorobenzene4ACE C18‐PFP0 100 2005678 9 111213141516ACN/0.1% HCOOHmAU0 100 2005678910 1113 141215162.1 x 50 mm, 3µm columnsACN/0.1% HCOOH3.0 4.0 5.03.0 4.0 5.0
Gradient Column Phase Screening:Optimum selectivity + UHPLC efficiencyAmbien Tablet, H 2O 2degradedTrazodone Tablet, H 2O 2degradedmAU0 2 4ACE Excel C18mAU0 2 418 8ACE Excel C18# Peaks4.0 5.0 6.0 7.0 8.0Time (min)4.0 5.0 6.0 7.0 8.0Time (min)mAU0 2 418ACE Excel C18‐ARmAU0 2 414ACE Excel C18‐AR4.0 5.0 6.0 7.0 8.0Time (min)mAU0 2 414ACE Excel C18‐PFPmAU0 2 44.0 5.0 6.0 7.0 8.0Time (min)Agilent 1200SL 600 bar systemoptimized ECV, 2 µL flow cell8ACE Excel C18‐PFP4.0 5.0 6.0 7.0 8.0Time (min)4.0 5.0 6.0 7.0 8.0Time (min)0–80% ACN/0.1% HCOOH, 10 mM NH 4 COO, 12‐minutes
Page 1 and 2: Exploiting Selectivity in HPLCand U
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Page 5 and 6: ®ACEHPLC / UHPLC ColumnsThe Import
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Page 9 and 10: ®ACEHPLC / UHPLC ColumnsWhich Fact
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Page 25 and 26: ®ACEHPLC / UHPLC ColumnsWhat Do I
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