Zebron™ Inferno™ - Phenomenex

Petrochemical ApplicationsMotor OilParaffin Wax16071Column: Zebron ZB -1HT Inferno Dimensions: 30 meter x 0.25 mm x 0.10 µmPart No.: 7HG-G014-02Injection: On-Column @ 153 °C, 1 µLCarrier Gas: Helium @ 1 mL/min (constant flow)Oven Program: 150 °C to 400 °C at 14 °C/min for 6 minDetector: FID @ 400 °CNote: Sample was 1 % in dichloromethaneSample: Mobil ® 1 10W-30 Fully Synthetic Motor OilColumn: Zebron ZB-5HT Inferno Dimensions: 15 meter x 0.32 mm x 0.10 μmPart No.: 7EM-G015-02Injection: Direct on column @ 43 °C, 0.01 µLCarrier Gas: Helium @ 1.9 mL/min (35 cm/sec)(constant flow)Oven Program: 40 °C for 2 min to 430 °C @ 20 °Cfor 10 minDetector: FID @ 430 °CSample: Paraffin WaxApp ID 16071Only 1.5 %retention differenceafter 23 hours inextreme conditions4 th injection136 th injectionApp ID 160890510 1520 min8 10 12 14 16 18 20 22minASTM Methods D2887 and D6352 on One ColumnASTM D2887 and D6352 both set standard test methods for boilingrange determination of petroleum fractions by GC. While ASTM D2887is used for products having a final boiling point of 538 °C or lower,ASTM D6352 is used for determining petroleum distillate fractions witha boiling point (BP) up to 700 °C. The Zebron Inferno columns makesimulated distillation analysis easier and less expensive. Typically youwould have to use a traditional fused silica column for ASTM D2887 anda metal column for ASTM D6352. Zebron Inferno columns provide arobust solution for both analyses.ASTM Method D635216148ASTM Method D2887-971235 6 7 931 338 10 1211 13414 1527 291617 18 19 21232520 2224262830323435 36 373839 40414243444546474849 56 585051 52 54 5753 5516217App ID 161481 23456 78910Stable analysis for standardhigh temperature simulateddistillation analysis11 1213 14 15 16 17App ID 16217010 20 minColumn: Zebron ZB-1HT Inferno Dimensions: 5 meter x 0.53 mm x 0.10 μmPart No.: 7AK-G014-02Injection: On-Column @ 43 °C, 0.1 μLCarrier Gas: Helium @ 4.4 mL/min (constant flow)Oven Program: 40 °C for 0.5 min to 430 °C @ 20 °C/min for 10 minDetector: FID @ 430 °CNote: Sample was a combination of PolyWax 655 and retention time markers C8-C40 in CS2/Chloroform.Sample:1. C102. C113. C124. C135. C146. C157. C168. C179. Pristane10. C1811. Phytane12. C1913. C2014. C2115. C2216. C2317. C2418. C2519. C2620. C2721. C2822. C2923. C3024. C3125. C3226. C3327. C3428. C3529. C3630. C3731. C3832. C3933. C4034. C4235. C4436. C4637. C4838. C5039. C5240. C5441. C5642. C5843. C6044. C6245. C6446. C6647. C6848. C7049. C7250. C7451. C7652. C7853. C8054. C8255. C8456. C8657. C8858. C902 4 6 8 10 12 minColumn: Zebron ZB-1HT Inferno Dimensions: 15 meter x 0.53 mm x 0.15 μmPart No.: 7EK-G014-05Injection: On-Column @ 38 ºC, 0.1 μLCarrier Gas: Helium @ 10 mL/min(constant flow)Oven Program: 35 ºC for 1 min to 360 ºC @25 ºC/minDetector: FID @ 375 ºCSample:1. Hexane2. Heptane3. Octane4. Nonane5. Decane6. Undecane7. Dodecane8. Tetradecane9. Hexadecane10. Octadecane11. Eicosane12. Tetracosane13. Octacosane14. n-Dotriacontane15. n-Hexatriacontane16. Tetracontane17. TetratetracontanePhenomenex | Tel: 310-212-0555 | Fax: 310-328-7768 | Email: info@phenomenex.com | Web: www.phenomenex.com21