instrumental techniques applied to mineralogy and geochemistry

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Analytical techniques applied to fluid inclusion studies: basics and applications 145 NONDESTRUCTIVE ANALYSIS Qualitative and semiquantitative - Visible light microscopy - Cathodoluminescence microscopy CL - Ultraviolet microscopy (Ultraviolet fluorescence microscopy) UV - Infrared microscopy IR - IR absorption spectrometry (Fourier transform IR microspectrometry) FTIR/FTIRM - Microthermometry (sometime, with infra-red microthermometry) Semiquantitative and quantitative - Laser Raman microprobe (or Laser Raman spectroscopy) LRM/LRS - Electron probes: Scanning electron microscopy and energy dispersive spectrometer SEM-EDS Electron microprobe EPMA Transmission electron microscopy TEM - Nuclear/ionic probes: Proton-induced X-ray emission (+/-Rutherford backscattering spectrometry) PIXE (RBS) Proton-induced gamma rays PIGE Elastic recoil detection analysis ERDA - X-ray probes: Synchrotron X-ray fluorescence SXRF Extended X-ray absorption fine structure EXAFS - Nuclear magnetic resonance/Proton magnetic resonance NMR/PMR TABLE 4. Different techniques used for analysis of fluid inclusions (from Roedder, 1990, and modified with data from Samsom et al. 2003 and from this summary).
146 Salvador Morales DESTRUCTIVE ANALYSIS Analysis of the gas phase - Gas chromatography (sometime, combined with mass spectrometry) GC (or GC-MS) - Laser microprobe mass analyzer or laser induced mass analyzer LAMMA/LIMA - Mass spectrometry (Quadrupole mass spectrometry) MS (QMS) Analysis of the solutes in the liquid phase - Atomic absorption spectrometry AAS - Flame-atomic emission spectroscopy FAES - Ion chromatography IC - Atomic-emission spectroscopy AES - (Laser ablation) inductively-coupled plasma mass spectrometry (LA-)ICP-MS - (Laser ablation) inductively-coupled plasma optical emission spectroscopy (LA-)ICP-OES - Instrumental neutron activation analysis INAA or NAA - SEM and cryogenic SEM (with energy dispersive analysis) (Cryo) SEM-EDS - Ion probe (secondary ion mass spectrometry) SIMS Also reported: thin-film anodic stripping voltammetry, coulometry, radiometry, emission spectroscopy, spectrophotometry, potentiometry -with ion-specific electrodes-, fluorimetry … Analysis of inclusion solids - Scanning electron microscopy and energy-dispersive spectrometry SEM-EDS - Electron diffraction ED - X-ray diffraction (+/- using the Gandolfi camera technique) XRD TABLE 4 (cont.). Different techniques used for analysis of fluid inclusions (from Roedder, 1990, and modified with data from Samsom et al. 2003 and from this summary). MgC1 2·12H 2 O; FeCl 3·6H 2 O; KCl·MgCl 2·6H 2 O) with sufficient quality in order to determine them in natural fluid inclusions (Dubessy et al., 1982). The salt hydrates can be used to determine the salinity of the solutions. Ni et al. (2006) demonstrates that hydrohalite has a positive correlation to salinity (i.e. the mass of hydrohalite increases with increasing salinities and decreasing mass of ice), being another effective way to
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INDEX Electron back-scattered diffr
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TEM in Geology. Basics and applicat
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X-ray Absorption Spectroscopy in Mi
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Raman, Conventional Infrared and Sy
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