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Influence of the Processes Parameters on the Properties of The ...

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Chapter 4.<br />

Experimental Procedures and Protocols for Analyses<br />

Figure 4.29: Set up <str<strong>on</strong>g>of</str<strong>on</strong>g> CT and flow chart <str<strong>on</strong>g>of</str<strong>on</strong>g> CT measurement process.<br />

4.4.1 Acquisiti<strong>on</strong><br />

<strong>The</strong> sample is rotated through 360 degrees <strong>on</strong> a precisi<strong>on</strong> turntable and a set <str<strong>on</strong>g>of</str<strong>on</strong>g> high resoluti<strong>on</strong><br />

digital radiographs are acquired at regular (typically 0.5 degree) increments. <strong>The</strong> accuracy <str<strong>on</strong>g>of</str<strong>on</strong>g> this data set<br />

determines <str<strong>on</strong>g>the</str<strong>on</strong>g> ultimate quality <str<strong>on</strong>g>of</str<strong>on</strong>g> <str<strong>on</strong>g>the</str<strong>on</strong>g> final 3D data.<br />

4.4.2 Correcti<strong>on</strong>s<br />

Each projected image from <str<strong>on</strong>g>the</str<strong>on</strong>g> data set undergoes geometric and shading correcti<strong>on</strong>, to remove<br />

spatial and intensity n<strong>on</strong> linearities introduced by <str<strong>on</strong>g>the</str<strong>on</strong>g> imaging device.<br />

4.4.3 Rec<strong>on</strong>structi<strong>on</strong><br />

By combining all <str<strong>on</strong>g>of</str<strong>on</strong>g> <str<strong>on</strong>g>the</str<strong>on</strong>g> individually corrected images and using a c<strong>on</strong>e beam back projecti<strong>on</strong><br />

technique, a geometrically correct, three dimensi<strong>on</strong>al data cloud is computed. <strong>The</strong> patented s<str<strong>on</strong>g>of</str<strong>on</strong>g>tware has a<br />

real-time viewer that shows <str<strong>on</strong>g>the</str<strong>on</strong>g> rec<strong>on</strong>structi<strong>on</strong> progressing in parallel with <str<strong>on</strong>g>the</str<strong>on</strong>g> x-ray images being captured.<br />

4.4.4 Viewing Results<br />

<strong>The</strong> CT data collecti<strong>on</strong>, rec<strong>on</strong>structi<strong>on</strong> and display are presented to <str<strong>on</strong>g>the</str<strong>on</strong>g> operator via <str<strong>on</strong>g>the</str<strong>on</strong>g> X-Tek<br />

graphical user interface. This has been developed to provide ease <str<strong>on</strong>g>of</str<strong>on</strong>g> use with <str<strong>on</strong>g>the</str<strong>on</strong>g> highest performance for<br />

systems to fit users’ budgets without compromise. <strong>The</strong> data cloud can be sliced open in any directi<strong>on</strong> to<br />

reveal internal detail, surface rendering s<str<strong>on</strong>g>of</str<strong>on</strong>g>tware similar to that used in 3D CAD systems is used to visualise<br />

<str<strong>on</strong>g>the</str<strong>on</strong>g> exposed features.<br />

4.4.5 Wide Variety <str<strong>on</strong>g>of</str<strong>on</strong>g> Post Processing<br />

<strong>The</strong> data cloud can be output as a stereo lithography file, a format accepted by most CAD<br />

packages. Once imported into a CAD system, <str<strong>on</strong>g>the</str<strong>on</strong>g> radiographic informati<strong>on</strong> can be compared directly with<br />

<str<strong>on</strong>g>the</str<strong>on</strong>g> original design file to highlight differences when checking first <str<strong>on</strong>g>of</str<strong>on</strong>g>f manufactured parts, or if <str<strong>on</strong>g>the</str<strong>on</strong>g> original<br />

design is not available, <str<strong>on</strong>g>the</str<strong>on</strong>g>n <str<strong>on</strong>g>the</str<strong>on</strong>g> radiographic data is used to create a new CAD file for rapid prototyping and<br />

reverse engineering.<br />

Micro CT <str<strong>on</strong>g>of</str<strong>on</strong>g> different scaffolds was taken from different angles and views. Slices were taken to<br />

observe <str<strong>on</strong>g>the</str<strong>on</strong>g> interc<strong>on</strong>nectivity and porosity <str<strong>on</strong>g>of</str<strong>on</strong>g> <str<strong>on</strong>g>the</str<strong>on</strong>g> scaffold structure. An example <str<strong>on</strong>g>of</str<strong>on</strong>g> a polymer skeletal<br />

structure al<strong>on</strong>g <str<strong>on</strong>g>the</str<strong>on</strong>g> top, fr<strong>on</strong>t and right views are taken (cf. Figure 4.30). <strong>The</strong>se images can be fur<str<strong>on</strong>g>the</str<strong>on</strong>g>r used<br />

for porosity and pore size distributi<strong>on</strong> analysis. CT can directly provide <str<strong>on</strong>g>the</str<strong>on</strong>g> porosity and interc<strong>on</strong>nectivity<br />

in tested foam. <strong>The</strong> results obtained from CT are real results compared to <str<strong>on</strong>g>the</str<strong>on</strong>g> results obtained from<br />

calculati<strong>on</strong>s and o<str<strong>on</strong>g>the</str<strong>on</strong>g>r derived analysis such as images analysis.<br />

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