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Scientific Report 2007-2009<br />

Laboratories and Facilities of the Department of Physics<br />

L9. Semiconductors and Optical Properties of Solids Lab<br />

Since its foundation, the laboratory of Semiconductors and Optical Properties of Solids has been engaged in research on<br />

the electronic and optical properties of semiconductors of interest in the fields of Information and Communication Technology<br />

and renewable energies. Si and III-V compounds under different type of external perturbations (e.g. high magnetic field,<br />

stress, excitation power density) have been the main objects of investigation. Either bulk material or heterostructures grown<br />

by molecular beam epitaxy (quantum wells wires) or self assembling (quantum dots) by national or international laboratories<br />

have been investigated. In the last ten years the interest of the laboratory has been focused on dilute nitrides and on the<br />

effect hydrogen has on the electronic and structural properties of these compounds. More recently, we have shown that the<br />

hydrogen induced effects can be exploited to achieve nanostructures with shape, size, and density arbitrarily designed in<br />

the sample growth plain by a novel technique, which avoids major drawbacks typical of standard top-down or bottom-up<br />

procedures.<br />

A great variety of light sources, monochromators and detectors available in the laboratory permits to operate from the<br />

(a)<br />

(b)<br />

Figure 1: (a) Optical table with apparatus for photoluminescence and Raman measurements (both micro and macro) in the<br />

near-UV to near-IR energy range. (b) Apparatus for irradiation with low-energy atoms of samples maintained at different<br />

temperatures.<br />

near ultraviolet to mid-infrared energy range on two different optical tables.<br />

Light sources are: a 2 W Coherent Ar laser, an 8 W Coherent Verdi diode laser, a 1 W Ti-sapphire tunable laser and a<br />

Coherent MBD 266 frequency doubler pumped by the Verdi laser, high pressure Hg and Xe lamps. A 1 m McPherson single<br />

monochromator, a 0.75 m Acton double monochromator, and a 0.3 m Jobin-Yvon single monochromator are also available,<br />

together with detectors including a Princeton Si CCD and an InGaAs linear array, a Hamamatsu photomultiplier with an UV<br />

extended GaAs cathode for single photon counting, an ADC ultrapure Ge detector, GaSb, InAs, PbS detectors, and related<br />

control electronics. Eventually, samples can be cooled down to liquid helium temperatures in two closed cycle cryostats<br />

or in two exchange gas cryostats, one of which equipped with magnetic fields up to 14 T. In order to measure the optical<br />

properties of single nanostructures, the laboratory has been recently equipped with a microscope for micro-photoluminescence<br />

and micro-Raman measurements and a He continuous-flow optical-cryostat whose piezoelectric movements permit to displace<br />

samples at liquid helium temperature by 8 mm maximum in the plane perpendicular to the microscope optical axis, with a<br />

resolution of a few nanometers. Finally, samples can be irradiated at temperatures ranging from room temperature to 600<br />

C with beams of atomic hydrogen or other gases whose energy goes from a minimum of 50 eV to a maximum of 1500 eV.<br />

Related research activities: C31,C32.<br />

<strong>Sapienza</strong> Università di Roma 183 Dipartimento di Fisica

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