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14. DATA VERIFICATION<br />

QUALITY ASSURANCE / QUALITY CONTROL<br />

In 2007, Aval<strong>on</strong> commissi<strong>on</strong>ed CDN Laboratory from British Columbia to generate three<br />

standards called AVL-H, AVL-M or AVL-L. These standards would be inserted into <strong>the</strong> assay<br />

stream. Aval<strong>on</strong> <strong>the</strong>n commissi<strong>on</strong>ed Dr. Barry Smee to review <strong>the</strong> round robin and assess <strong>the</strong><br />

quality of <strong>the</strong> data.<br />

In 2010, Aval<strong>on</strong> commissi<strong>on</strong>ed CDN Laboratory from British Columbia to generate a fur<strong>the</strong>r<br />

standard called S-04-09. This standard would be inserted into <strong>the</strong> assay stream, alternating<br />

with <strong>the</strong> original three standards. Aval<strong>on</strong> <strong>the</strong>n commissi<strong>on</strong>ed Dr. Barry Smee to review <strong>the</strong><br />

round robin and assess <strong>the</strong> quality of <strong>the</strong> data. The Round Robin <strong>on</strong> <strong>the</strong> new standard included<br />

samples of <strong>the</strong> original three standards, rare earth certified standards, all randomized for <strong>the</strong><br />

Round Robin. When inserted into <strong>the</strong> sample database, this standard was referred to as STD-<br />

H2.<br />

The statistics of QAQC c<strong>on</strong>trol samples was presented previously in <strong>the</strong> Scott Wils<strong>on</strong> RPA<br />

(2010) and is updated here. The c<strong>on</strong>trol samples inserted into <strong>the</strong> sample stream from drill<br />

holes 137 to 311 are presented in Table 14-1.<br />

Table 14-1 Statistics of QAQC C<strong>on</strong>trol Samples, L09-137 to L10-311<br />

Samples Analyses Blanks Standard-L Standard-M Standard-H Standard-H2 Standards total<br />

Total number 10,491 15,474 417 180 162 121 306 769<br />

Percent of samples 4.0% 1.7% 1.5% 1.2% 2.9% 7.3%<br />

Percent of analyses 2.7% 1.2% 1.0% 0.8% 2.0% 5.0%<br />

As can be seen, blanks were inserted <strong>on</strong> average at <strong>the</strong> rate of 4.0%, or <strong>on</strong>e in 25 samples, and<br />

standards at <strong>the</strong> rate of 7.3%, or <strong>on</strong>e in 13 samples. The rate of inserti<strong>on</strong> of standards was<br />

varied according to whe<strong>the</strong>r <strong>the</strong> samples were from a mineralized z<strong>on</strong>e or not with a standard<br />

every 10 samples in mineralizati<strong>on</strong> and every 40 samples outside mineralizati<strong>on</strong>. Some 10,491<br />

samples were analysed by ALS method MS81 (so called “regular” analysis) and some 4,983, or<br />

47%, were re-analysed for method MS81H, for higher rare earth and Zr analytical limits. As<br />

noted elsewhere, samples were also analysed for additi<strong>on</strong>al methods such as tests of XRF<br />

analysis for Zr, Nb and Ta. These additi<strong>on</strong>al analyses are not included in <strong>the</strong> statistics above.<br />

The results of <strong>the</strong> standard analyses were checked against <strong>the</strong> certified or provisi<strong>on</strong>al means<br />

and tolerances listed in <strong>the</strong> standard certificates as well as against <strong>the</strong> lab’s (ALS) own precisi<strong>on</strong><br />

tolerance level of +/-10%. The three rare earth elements with <strong>the</strong> potential highest value (Nd,<br />

Technical Report 43-101 – March 13, 2011 Page 14-1<br />

Prepared by Aval<strong>on</strong> Rare Metals Inc.

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