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THE JOURNAL OF - Dentsply

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Blunck/Zaslansky<br />

[% MQ1]<br />

100<br />

95<br />

a.<br />

90<br />

85<br />

Optibond FL<br />

80<br />

75<br />

T1 T2 T3 T4 T5 T6<br />

[% MQ1]<br />

100<br />

95<br />

b.<br />

90<br />

85<br />

Syntac<br />

80<br />

75<br />

T1 T2 T3 T4 T5 T6<br />

c.<br />

[% MQ1]<br />

100<br />

95<br />

90<br />

85<br />

80<br />

75<br />

Clearfil SE Bond<br />

T1 T2 T3 T4 T5 T6<br />

Fig 3 Median MQ1 values in % of entire margin length<br />

in dentin with error bars indicating the standard error of<br />

the mean for the multi-bottle reference materials (a) Opti<br />

Bond FL, (b) Syntac and (c) Clearfil SE Bond at the six<br />

evaluation stages T1 (after 21 days’ water storage), T2<br />

(after 1st TC), T3 (after 1 year of water storage), T4 (after<br />

2nd TC), T5 (after 3 years of water storage) and T6 (after<br />

3rd TC). Black lines: regression lines weighted by the corresponding<br />

standard error; dotted lines: 95% confidence<br />

intervals.<br />

study, but overall the scores are quite high, perhaps due to<br />

the fact that the deterioration is generally quite minimal.<br />

Further examination of the present data allows creating a<br />

quasi-dynamic perspective of the deterioration rate of the<br />

restorations (Fig 3 and Table 3). Thus it is seen that there is<br />

a general negative trend in the MQ1 values, when these are<br />

determined after water storage and/or thermocycling (TC).<br />

Clearly, the specific state of the bond between each<br />

restorative and the tooth is not easily determined by any surface-evaluation<br />

method, particularly following long-term water<br />

storage. The decision was thus made to use TC to induce<br />

mild stress to every tooth-restoration interface in order to better<br />

reveal its state as determined by the marginal quality evaluation.<br />

As can be seen in Table 3, the effect of TC is not constant<br />

during early vs late (> 1 year) water storage, and this is<br />

attributed to the differences in the adhesive stability in water.<br />

A number of publications have dealt with the effects of<br />

similar long-term water storage beyond 2 years. 2,3,7,16,22,<br />

23,27 To the best of our knowledge, however, none have managed<br />

to produce high-resolution long-term data mapping the<br />

marginal quality deterioration on the same samples.<br />

Despite the fact that the cavity dimensions were standardized,<br />

the amount of stress induced to the interface of<br />

each restoration probably varied considerably. This might<br />

be due to the large variations in the coefficients of thermal<br />

expansion of each restorative 28,29 or possibly due to tooth<br />

variability. Be that as it may, because the manufacturer-recommended<br />

composites were used, it was assumed that the<br />

conditions were optimal for each adhesive, and that the<br />

best performance was obtained. It remains to be seen if other<br />

combinations of composite/adhesive deliver improved<br />

long-term results. Possibly, a standard composite restorative<br />

should be used for such tests in the future in order to<br />

better compare the effectiveness of the investigated adhesives.<br />

The importance of the effect of the composite resins<br />

can clearly be seen in the groups of Adper Prompt L-Pop and<br />

Xeno III, where large differences in MQ1 values and slopes<br />

are seen for the same adhesive. Note however, that while<br />

Adper Prompt L-Pop in combination with Tetric Ceram<br />

showed a statistically significant decrease in MQ1 compared<br />

to the results obtained with Filtek Z250, all three<br />

combinations with Xeno III (Dyract XP, Quixfil, and Tetric Ceram)<br />

revealed no statistically significant differences in marginal<br />

integrity. We therefore conclude that these adhesives<br />

react differently to composite resins with higher polymerization<br />

shrinkage stress values.<br />

Both in vitro 6,7,10,11 and in vivo studies 8,12,13,35,37 have<br />

shown that multi-bottle multi-step adhesive systems such as<br />

236 The Journal of Adhesive Dentistry

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