Chemical Reference Standards AccuStandard®
Chemical Reference Standards AccuStandard®
Chemical Reference Standards AccuStandard®
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Petrochemical ASTM <strong>Standards</strong><br />
ASTM D-5769 4 Internal Standard Version (Includes Toluene-d 8 )<br />
Originally designed for D-5769-98<br />
Calibration Curve with a 4 Comp. Deuterated<br />
Internal Standard added<br />
D-5769-CAL/IS-R-SET<br />
$ 425 / 5 x 1 mL<br />
Core Calibr. Mix Std. 1 Std. 2 Std. 3 Std. 4 Std. 5<br />
24 Comps. Target Wt. % Wt. % Wt. % Wt. % Wt. %<br />
Optional Sixth Standard<br />
with a 4 Comp. Deuterated<br />
Internal Standard added<br />
D-5769-ADD/IS-R $ 100 / 1 x 1 mL<br />
Core Calibration Mix Target<br />
24 Comp. Wt. %<br />
ASTM <strong>Standards</strong><br />
Benzene 5.25 2.95 1.575 0.8144 0.4143<br />
Toluene 19.67 11.06 5.898 3.0505 1.5519<br />
Ethylbenzene 5.18 2.91 1.552 0.8026 0.4083<br />
m-Xylene 6.19 3.48 1.856 0.9598 0.4883<br />
p-Xylene 6.19 3.48 1.856 0.9598 0.4883<br />
o-Xylene 6.30 3.54 1.890 0.9776 0.4973<br />
Isopropylbenzene 3.09 1.74 0.925 0.4786 0.2435<br />
n-Propylbenzene 3.09 1.74 0.926 0.4787 0.2435<br />
3-Ethyltoluene 3.10 1.74 0.928 0.4801 0.2442<br />
4-Ethyltoluene 3.08 1.73 0.925 0.4782 0.2433<br />
1,3,5-Trimethylbenzene 3.10 1.74 0.929 0.4804 0.2444<br />
2-Ethyltoluene 3.15 1.77 0.945 0.4890 0.2488<br />
1,2,4-Trimethylbenzene 5.23 2.94 1.567 0.8104 0.4123<br />
1,2,3-Trimethylbenzene 3.20 1.80 0.960 0.4965 0.2526<br />
Indan 3.45 1.94 1.034 0.5350 0.2722<br />
1,4-Diethylbenzene 3.09 1.74 0.925 0.4786 0.2435<br />
n-Butylbenzene 3.08 1.73 0.923 0.4776 0.2430<br />
1,2-Diethylbenzene 3.15 1.77 0.945 0.4885 0.2485<br />
1,2,4,5-Tetramethylbenzene 2.12 1.19 0.635 0.3284 0.1671<br />
1,2,3,5-Tetramethylbenzene 2.12 1.19 0.637 0.3295 0.1676<br />
Naphthalene 2.37 1.34 0.712 0.3683 0.1874<br />
1-Methylnaphthalene 2.37 1.34 0.712 0.3683 0.1874<br />
2-Methylnaphthalene 2.43 1.37 0.730 0.3773 0.1919<br />
Isooctane ----- 43.77 70.015 84.4922 92.1105<br />
Internal Standard<br />
M-GRA-IS-R<br />
Wt.<br />
Compound Ratio<br />
n-Hexane 12<br />
n-Heptane 17<br />
n-Octane 17<br />
n-Decane 12<br />
n-Dodecane 5<br />
Isooctane 12<br />
Benzene 1<br />
Compound Mix ratio<br />
Benzene-d 6 2 mL<br />
Ethylbenzene-d 10 2 mL<br />
Naphthalene-d 8 1 gm<br />
Toluene-d 8 7 mL<br />
Daily Quality Control Standard<br />
(with Internal Standard)<br />
D-5769-QC/IS-R-5ML<br />
D-5769-QC/IS-R-5ML-PAK<br />
Wt.<br />
Compound<br />
Ratio<br />
Toluene 9<br />
Ethylbenzene 3<br />
m-Xylene 3<br />
o-Xylene 3<br />
1,2,4-Trimethylbenzene 3<br />
1,2,4,5-Tetramethylbenzene 2<br />
Naphthalene 1<br />
Includes M-GRA-IS-R (4 component mix)<br />
added in 12 to 100 weight ratio<br />
$ 100 / 1 x 5 mL<br />
SAVE $ 400/5 x 5 mL<br />
18 comps.<br />
100<br />
Resolution Standard<br />
M-GRA-RES<br />
M-GRA-RES-PAK<br />
Benzene 4.16<br />
Toluene 16.41<br />
Ethylbenzene 4.10<br />
m-Xylene 4.91<br />
p-Xylene 4.91<br />
o-Xylene 5.00<br />
Isopropylbenzene 2.45<br />
n-Propylbenzene 2.45<br />
3-Ethyltoluene 2.45<br />
4-Ethyltoluene 2.44<br />
1,3,5-Trimethylbenzene 2.46<br />
2-Ethyltoluene 2.50<br />
1,2,4-Trimethylbenzene 4.14<br />
1,2,3-Trimethylbenzene 2.54<br />
Indan 2.73<br />
1,4-Diethylbenzene 2.45<br />
n-Butylbenzene 2.44<br />
1,2-Diethylbenzene 2.50<br />
1,2,4,5-Tetramethylbenzene 1.68<br />
1,2,3,5-Tetramethylbenzene 1.68<br />
Naphthalene 1.88<br />
1-Methylnaphthalene 1.88<br />
2-Methylnaphthalene 1.93<br />
Isooctane 19.92<br />
The 4 Comp. Internal Standard Mix (M-GRA-IS-R) is<br />
combined with the 24 component core calibration<br />
curve mixtures above in a 12 to 100 weight ratio to<br />
formulate these 28 component calibration solutions.<br />
Sensitivity Test Solution<br />
M-GRA-ST<br />
M-GRA-ST-PAK<br />
100 µg/mL in Isooctane<br />
1,4-Diethyl benzene<br />
Compound Wt. %<br />
1,3,5-Trimethylbenzene 3.0<br />
1-Methyl-2-ethylbenzene 3.0<br />
Isooctane 94<br />
$ 10 / 1 x 1 mL<br />
SAVE $ 40 / 5 x 1 mL<br />
$ 30 / 1 x 1 mL<br />
SAVE $ 120 / 5 x 1 mL<br />
3 comps.<br />
4 Comp. Deuterated Internal Std. Mix<br />
M-GRA-IS-R-10ML<br />
$ 225 / 1 x 10 mL<br />
M-GRA-IS-R-10ML-PAK SAVE $ 900/ 5 x 10 mL<br />
Compound Mix Ratio Compound Mix Ratio<br />
Benzene-d 6 2 mL Naphthalene-d 8 1 gm<br />
Ethylbenzene-d 10 2 mL Toluene-d 8 7 mL<br />
Fragmentation Pattern Standard<br />
M-GRA-FP<br />
$ 20 / 1 x 1 mL<br />
M-GRA-FP-PAK<br />
SAVE $ 80 / 5 x 1 mL<br />
3.0 w/w in Isooctane<br />
1,2,3-Trimethylbenzene<br />
174<br />
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