Pike Technologies Comprehensive Catalog of FTIR ... - Madatec

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NIR IntegratIR – Integrating Sphere F EATURES O F T HE NIR INTEGRATIR • Optimized 2" gold-coated integrating sphere with high signal-to-noise ratio • Fully integrated InGaAs detector, detector electronics and transfer optics • Optional automated transmission analysis stage for pharmaceutical analysis • 10 mm horizontal sampling port for easy sample placement • Excellent qualitative and quantitative NIR analysis tool • Economical alternative to dedicated near-infrared analyzers • Optional Rotating Stage for averaging of heterogeneous samples • Spectral range 12200-3850 cm -1 • In-Sample Compartment design, compatible with most commercial FTIR spectrometers The PIKE Technologies NIR IntegratIR is a near-infrared (NIR) Integrating Sphere for quantitative and qualitative measurements of a wide variety of solids and paste materials. The NIR IntegratIR collects reflected energy from a spherical perspective and thereby captures complete and quantitative response from the sample. Using near-infrared chemometrics, qualitative product identification and quantitative analysis may be performed on pharmaceutical, nutraceutical, chemical, polymer, textile, food, agricultural and other samples. The NIR IntegratIR accessory features a 2" high reflectivity gold-coated integrating sphere and a high-speed, low-noise indium-gallium-arsenide (InGaAs) detector, transfer optics and interface electronics. The NIR IntegratIR fits into the sample compartment of most commercial FTIR spectrometers and its electronics interface as an internal detector of the spectrometer. A 10 mm diameter horizontal sampling port makes the placement of samples onto the accessory very easy. An optimized borosilicate window serves as a sampling port at the top of the integrating sphere. The window is bonded and sealed to protect the sphere from corrosive materials and contamination. Sampling of tablets, packaging materials and plastics is easily accomplished by placing the sample directly on the window of the upward facing sphere. Powders, creams, pastes or liquids containing reflective particles may be placed in disposable flatbottom vials – eliminating the need for any sample cleanup. The vials may be held in place by a sample-positioning vial holder, resulting in more repeatable measurements. Qualitative analysis of steroids using the PIKE Technologies NIR IntegratIR. Samples are measured within glass vials. High quality spectra are produced quickly using the NIR IntegratIR – making qualitative and quantitative analysis of a wide variety of sample types efficient and reliable. For heterogeneous samples, PIKE Technologies offers a Rotating Stage for the NIR IntegratIR. With this option, one obtains an averaged result to eliminate variations in quantitative results for the chosen sample area. I NTEGRATING S PHERE P RODUCTS – R EFLECTANCE F ROM A LL P ERSPECTIVES 53
P IKE T ECHNOLOGIES WWW. PIKETECH. COM 608-274-2721 Quantitative measurement of active ingredient in a mixture of magnesium stearate, lactose, Emcompress, cellulose and CaboSil P ART N UMBER 048-60XX O RDERING I NFORMATION D ESCRIPTION NIR IntegratIR Integrating Sphere Accessory Includes 2" diffuse gold coated integrating sphere, InGaAs detector, detector preamplifier, cable and baseplate for the specific model spectrometer. The accessory also includes a gold reference standard, vial holder, and glass vials. Notes: Please see the FTIR instrument code sheet. Sampling Options for NIR IntegratIR P ART N UMBER D ESCRIPTION 048-2999 Glass Sample Vials (Pack of 25), 19 x 65 mm 048-3000 Diffuse Gold Reference 048-3070 NIST Traceable NIR Reference Standard 048-3071 NIST Traceable NIR Reference Standard – Recertification 044-3010 Glass Vial Holder (for 19 mm vials) 048-0150 Rotating Stage for Petri Dish (for heterogeneous samples) Includes 100 x 20 mm Petri Dish 048-0151 Rotating Stage Adapter for 500 ml beaker 048-0060 Automated Transmission Tablet Analysis Stage for NIR IntegratIR Includes 3 tablet plates for 7.5, 8.5 and 10 mm tablets Note: Please contact us for other options. NIR IntegratIR with optional transmission tablet analyzer The NIR IntegratIR comes complete with diffuse gold reference, sample holders and a removable general-purpose sample mounting plate. The NIR IntegratIR is configured for each specific FTIR spectrometer and includes a pre-aligned mount for your instrument. The NIR IntegratIR is a cost-effective, high-performance sampling option for laboratories with a standard FTIR spectrometer equipped with a near-infrared light source and beam splitter. The optional transmission tablet analysis stage for the NIR IntegratIR provides an automated tool for sampling 10 tablets of a variety of sizes. With this option you can measure formulation reproducibility or verify pharmaceutical composition. 54
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FTIR Instrument Code XX ABB Bomem F
Page 4 and 5:
TABLE O F C ONTENTS Pages 1 - 6 Pag
Page 6 and 7:
Sampling Kits If you are not sure w
Page 8 and 9: Comprehensive Transmission Sampling
Page 10 and 11: Valu-Line - High Performance Set of
Page 12 and 13: Attenuated Total Reflectance Sampli
Page 14 and 15: Table 1: MIRacle Crystal Plate Spec
Page 16 and 17: MIRacle Base Optics (must select, i
Page 18 and 19: GladiATR Base Optics (must select,
Page 20 and 21: HATR Crystal Plate Choices PIKE Tec
Page 22 and 23: HATR and HATRPlus Pressure Clamp (m
Page 24 and 25: Optimized FTIR spectrum of polymer
Page 26 and 27: VeeMAX II with ATR - Variable Angle
Page 28 and 29: Classic VATR - Variable Angle ATR f
Page 30 and 31: Table 1 ATR Sampling ZnSe, Diamond
Page 32 and 33: Diffuse Reflectance Products Diffus
Page 34 and 35: DiffusIR - Research Grade Diffuse R
Page 36 and 37: UpIR - Upward Looking Diffuse Refle
Page 38 and 39: X, Y Autosampler - Transmission and
Page 40 and 41: Diffuse Reflectance - Theory and Ap
Page 42 and 43: Specular Reflectance Products Specu
Page 44 and 45: Changing the angle of incidence wit
Page 46 and 47: 80Spec - Grazing Angle Specular Ref
Page 48 and 49: 10Spec - Measures Sample Reflectanc
Page 50 and 51: Specular Reflectance - Theory and A
Page 52 and 53: Polarization Products Polarizers ma
Page 54 and 55: Infrared Polarizers - Theory and Ap
Page 56 and 57: Integrating Sphere Products Integra
Page 60 and 61: Integrating Spheres - Introduction
Page 62 and 63: Fiber Optic Sampling Products Fiber
Page 64 and 65: FlexIR - NIR Fiber Optic Accessory
Page 66 and 67: Microsampling Products Microsamplin
Page 68 and 69: Switching from transmission to refl
Page 70 and 71: Microsampling Tools - Compression C
Page 72 and 73: Beam Condensers - 4X and 6X Version
Page 74 and 75: Transmission Sampling Products Tran
Page 76 and 77: RotatIR - Automated Rotating Sample
Page 78 and 79: X, Y Autosampler - Transmission and
Page 80 and 81: Demountable Liquid Cells - For Vers
Page 82 and 83: Long-Path Quartz Liquid Cells - For
Page 84 and 85: Demountable Liquid Cell Windows (mu
Page 86 and 87: Bolt Press & Hydraulic Die - Low-Co
Page 88 and 89: PIKE CrushIR - Digital Hydraulic Pr
Page 90 and 91: Sample Preparation Accessories - Fo
Page 92 and 93: Disks, Windows and Powders - For Tr
Page 94 and 95: Disks, 41 mm Diameter 3 mm Thicknes
Page 96 and 97: Short Path Gas Cells - For Samples
Page 98 and 99: Long-Path Gas Cells - For Measureme
Page 100 and 101: Transmission Sampling Techniques -
Page 102 and 103: An alternate method for analysis of
Page 104 and 105: Special Applications Products PIKE
Page 106 and 107: MappIR and MAP300 - For Automated A
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TGA/FTIR Accessory - Identification
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Semiconductor Applications - FTIR S
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Other Useful Products for Spectrosc
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ATR spectra are somewhat different
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ATR Spectral Data Bases - Optimize
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Alphabetical Index A 10Spec, specul
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T Teflon gaskets, demountable cell
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022-5340 HATR Liquid Jacketed Troug
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160-1007 25 x 2 mm ZnSe (6 pack) 88
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162-1130 Press-On Demountable Liqui
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We are PIKE Technologies, a small c
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Pike Technologies Comprehensive Catalog of FTIR ... - Madatec

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