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Lab 4 - Geology

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Geo 306 lab 03<br />

p. 1 of 4<br />

Name __________________________________________________<br />

Physical and Optical Properties of Sheet Silicates, Ring Silicates<br />

Goals for this lab:<br />

1. Learn essential properties for identifying these minerals in hand specimen: serpentine, kaolinite,<br />

talc, muscovite, biotite, chlorite, beryl, tourmaline.<br />

2. Learn essential properties for identifying these framework silicates in thin section: talc, muscovite,<br />

biotite, chlorite, tourmaline.<br />

<strong>Lab</strong> lecture topics<br />

1. Finding each mineral in thin section.<br />

<strong>Lab</strong> groups: You will be sharing microscopes, and can work together, but should turn in individual<br />

work on this lab.<br />

Introduction<br />

The sheet silicates are a very common and important group of crustal minerals. They all contain hydrogen<br />

(some more than others), so they are not stable at very high temperatures. These minerals are ubiquitous in<br />

many metamorphic rocks, and of course clays are extremely common in the near-surface environment.<br />

Muscovite and biotite are important components of felsic to intermediate plutonic igneous rocks, and<br />

serpentine is commonly found as an alteration product of ultramafic rocks in our area (c.f., Swift Creek<br />

Landslide).<br />

It would be wise to indicate on your notes something about the crystal structure (T-O, T-O-T, etc.).<br />

The ring silicates are not systematic in their occurrence.<br />

Serpentine<br />

Hand sample notes:<br />

•<br />

Rarely forms large or euhedral crystals. Most commonly found nearby as product of hydrothermal<br />

metamorphism of ultramafic rock.<br />

• Hardness and color are very useful, but luster is a key tool as well.<br />

• Similar: green talc, nephritic actinolite, chlorite<br />

Kaolinite<br />

Hand sample notes:<br />

•<br />

•<br />

•<br />

•<br />

Essentially never forms visible crystals.<br />

Luster is distinctive.<br />

Breathe on it, then smell it – useful.<br />

Similar: Chalk (calcite), diatomite (quartz)


Geo 306 lab 3 p. 2 of 4<br />

Talc<br />

Hand sample notes:<br />

•<br />

•<br />

•<br />

•<br />

Hardness and luster are key.<br />

Color is somewhat variable, but generally light.<br />

Often occurs mixed with other minerals, so bulk hardness can be misleading, but soapy feel is useful.<br />

Similar: serpentine, muscovite<br />

Thin section notes:<br />

•<br />

NC022E is dominated by two minerals: actinolite (an amphibole) and talc. Talc is the mineral with one<br />

cleavage. It is nearly indistinguishable from muscovite in thin section (one reason hand specimen<br />

analysis is as important as thin section).<br />

• Talc, like muscovite and biotite, has a texture in XP called “bird’s-eye extinction”. This texture is<br />

produced when the surface of the thin section is ground down. During this process, the surface get<br />

roughened, and these irregularities do not go extinct in the same orientation as the rest of the grain.<br />

What you see is a speckled appearance as the grain goes extinct.<br />

• Some of these thin sections are not the correct thickness, so be careful.<br />

• Similar: muscovite<br />

Muscovite<br />

Hand sample notes:<br />

•<br />

•<br />

Habit and cleavage, together with color, are key.<br />

Similar: biotite, talc<br />

Thin section notes:<br />

•<br />

Muscovite, together with biotite and talc, has a distinctive appearance in XP near extinction. Find a<br />

grain showing this texture, called “bird’s-eye extinction”, and sketch it.<br />

•<br />

Micas often look very different when you are looking on a cleavage plane versus looking at a cut<br />

through the cleavage planes. The bird’s-eye texture looks different as well. Find one grain of each<br />

type and describe the differences.<br />

•<br />

Muscovite and the other micas are easily deformed. Just as with quartz, this deformation causes<br />

undulatory extinction.<br />

• PM026A has lots of small muscovite grains (and a few large biotite grains). Note the bright secondorder<br />

colors.<br />

• MBr38 has some very fine muscovite grains.<br />

• Similar: talc, biotite


Geo 306 lab 3 p. 3 of 4<br />

Biotite<br />

Hand sample notes:<br />

•<br />

•<br />

Looks essentially like muscovite, but darker-colored.<br />

Similar: chlorite, hornblende, muscovite<br />

Thin section notes:<br />

•<br />

Looks essentially like muscovite, but darker-colored, and pleochroic. Note that when the biotite<br />

cleavage is oriented N-S in PP, it can looks nearly colorless.<br />

• Has bird’s-eye extinction.<br />

•<br />

•<br />

•<br />

MBr38 has lots of biotite, aligned generally parallel.<br />

PM026A has a few large biotite grains.<br />

MBr42 has large biotites with pleochroic haloes. These are small dark circles in PP light, some of<br />

which have tiny clear grains in the center. These grains have radioactive elements which, when they<br />

decay, produce damage in the surrounding biotite, disrupting the crystalline structure and turning into a<br />

semi-amorphous substance. Those without evident tiny central grains have a cut through the halo<br />

which missed the central grain. In this rock, the central grains are zircon, but other minerals can also<br />

cause these haloes. Sketch a grain with pleochroic haloes.<br />

•<br />

SN14 has two colored pleochroic minerals. Amphibole lacks bird’s-eye extinction, while biotite has<br />

bird’s-eye extinction. Be sure you can tell the difference.<br />

• Examine I-S-21 with PM026A in XP at low power. Look at the interference colors of each. Note that<br />

these minerals have similar birefringence, but they looks quite different in XP. This is because the<br />

interference color in tinted/obscured by the color of the mineral (i.e., in PP).<br />

• Similar: chlorite, hornblende, muscovite, tourmaline<br />

Chlorite<br />

Hand sample notes:<br />

•<br />

Very often too fine-grained to observe individual crystals, but color and habit/state of aggregation can<br />

often be discerned in bulk samples.<br />

• Green to very dark green colors are the rule.<br />

• Similar: biotite, talc, serpentine<br />

Thin section notes:<br />

•<br />

•<br />

•<br />

Pleochroic green colors.<br />

One cleavage plane.<br />

Very low interference colors. Note that chlorite has anomalous interference colors. This means that<br />

although the interference color maybe first-order gray, it appears brown (if Mg-rich) or blue (if Fe-rich).<br />

Generally the hue of this weird color doesn’t fit anywhere on the interference color chart, and it doesn’t<br />

decrease near the edges of the grains – that’s what makes it anomalous.<br />

• SN14 and 36AC have a very common occurrence of chlorite, as an alteration product of biotite. Look<br />

for pleochroic green layers in the brownish biotite grains. Note that the cleavage of the chlorite is<br />

parallel to that of the biotite. This alignment of crystal structures is called epitaxy<br />

• Similar: biotite, muscovite, hornblende, talc


Geo 306 lab 3 p. 4 of 4<br />

Beryl<br />

Hand sample notes:<br />

•<br />

•<br />

•<br />

Columnar hexagonal crystals with imperfect basal cleavage and conchoidal fracture otherwise.<br />

Mainly found in granitic pegmatites (intrusive rocks with very large crystals).<br />

Typical color is pale blue or blue-green, but deep green beryl is called emerald, blue is aquamarine,<br />

and other colors have other names. Makes a good gemstone due to its hardness<br />

• Similar: apatite, quartz<br />

Tourmaline<br />

Hand sample notes:<br />

•<br />

Very strongly colored; typically nearly black in hand specimen (“schorl” variety). Gem varieties can be<br />

more transparent.<br />

• If Li is dominant, then it can be pink (“rubellite” or “elbaite”).<br />

•<br />

•<br />

• Similar: hornblende, augite<br />

Always prismatic to acicular, with distinctive cross-sectional shape.<br />

Common in pegmatites and metamorphic rocks. Main residence for boron in the crust.<br />

Thin section notes:<br />

•<br />

•<br />

Strongly pleochroic in all cases.<br />

W89 is full of tourmaline. We saw this in <strong>Lab</strong> 2 – note the difference in pleochroism between cuts<br />

perpendicular to the c axis and those parallel to the c axis of this hexagonal mineral. Look for the<br />

distinctive cross-section.<br />

• Similar: hornblende, biotite, chlorite


Geo 306 lab 04<br />

Name __________________________________________________<br />

Questions for Sheet/Ring Silicates<br />

1. What is the best (although still not 100% certain) way for you to tell muscovite from talc in thin section?<br />

(Note that you cannot determine 2V until you take <strong>Geology</strong> 407) _________________________________<br />

_____________________________________________________________________________________<br />

_____________________________________________________________________________________<br />

_____________________________________________________________________________________<br />

2. Both quartz and beryl can be blue in hand specimen (although blue is pretty rare for quartz), and they<br />

occur in similar rocks. What is the best way to tell them apart in the field? (“In the field” is intended to make<br />

you think about tools for making measurements) ______________________________________________<br />

_____________________________________________________________________________________<br />

_____________________________________________________________________________________<br />

3. Muscovite, biotite, and talc share a distinctive property in thin section that no other common minerals<br />

display. Sketch it:<br />

4. There are four rocks for you to inspect. Determine which (if any) of this lab’s minerals are found in each<br />

rock:<br />

306X3<br />

306X4<br />

306X5<br />

306X6

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